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US4243512A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for preparation of pitch for producing carbon fiber

Assignee: Kureha Corp
•
Filing: 1979-06-19
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Granted: 1981-01-06
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Expires: 1999-06-19
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Abstract

Abstract A process for preparing a pitch for carbon fiber by filtering a heavy pitch having a softening point of 150°-200° C. at a temperature of 250°-300° C. and further treating at the same temperature under reduced pressure.

Inventors

  • 👤 Ikuo Seo

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 20:26
CPC Classifications
C; C10; C10C; C10C3/00

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 184 words
A process for preparing a pitch suitable for use in producing carbon fibers comprising: filtering at a temperature of 250° to 300° C. a heavy petroleum pitch, containing 20 to 45% by weight of compounds insoluble in benzene and having a softening point of 150° to 200° C., to remove fractions non-liquefying or infusible at a temperature higher than 250° to 300° C. therefrom using more than one filter net of meshes finer than 200 mesh at a rate of 0.5 to 2 g/min/cm 2 , introducing the thus filtered pitch at a temperature of 250° to 300° C. in the form of laminar flow of 1 to 30 mm in thickness into a vessel at a reduced pressure of 300 to 500 mm Hg of an inert gas to remove volatile fractions and bubbles from said filtered pitch in the laminar flow, thereby obtaining a treated pitch containing substantially no bubbles and no components non-liquefying or infusible at a temperature of 250° to 300° C., containing less than 5% by weight of low-molecular weight fractions boiling at a temperature lower than 500° C.
Claim 2
Dependent Claim 184 words
A process for preparing a pitch suitable for use in producing carbon fibers comprising: filtering at a temperature of 250° to 300° C. a heavy petroleum pitch, containing 20 to 45% by weight of compounds insoluble in benzene and having a softening point of 150° to 200° C., to remove fractions non-liquefying or infusible at a temperature higher than 250° to 300° C. therefrom using more than one filter net of meshes finer than 200 mesh at a rate of 0.5 to 2 g/min/cm 2 , introducing the thus filtered pitch at a temperature of 250° to 300° C. in the form of laminar flow of 1 to 30 mm in thickness into a vessel at a reduced pressure of 300 to 500 mm Hg of an inert gas to remove volatile fractions and bubbles from said filtered pitch in the laminar flow, thereby obtaining a treated pitch containing substantially no bubbles and no components non-liquefying or infusible at a temperature of 250° to 300° C., containing less than 5% by weight of low-molecular weight fractions boiling at a temperature lower than 500° C.
Claim 3
Dependent Claim 13 words
The process according to claim 1, wherein said inert gas is gaseous nitrogen.

References Cited (Backward Citations)

GB1155448A Cited
US3718493A Cited
US4026788A Cited
US4032430A Cited
US3997654A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-01-06 1984-07-07 1985-01-06 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-01-06 1988-07-07 1989-01-06 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-01-06 1992-07-07 1993-01-06 $7700.00 Window Closed / Lapsed

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