US4243512A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for preparation of pitch for producing carbon fiber
Assignee: Kureha Corp
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Filing: 1979-06-19
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Granted: 1981-01-06
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Expires: 1999-06-19
Abstract
Abstract A process for preparing a pitch for carbon fiber by filtering a heavy pitch having a softening point of 150°-200° C. at a temperature of 250°-300° C. and further treating at the same temperature under reduced pressure.
Inventors
- 👤 Ikuo Seo
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 02:50
CPC Classifications
C; C10; C10C; C10C3/00
Claims Analysis
Total Claims: 3
Claim 1
Independent Claim
184 words
A process for preparing a pitch suitable for use in producing carbon fibers comprising: filtering at a temperature of 250° to 300° C. a heavy petroleum pitch, containing 20 to 45% by weight of compounds insoluble in benzene and having a softening point of 150° to 200° C., to remove fractions non-liquefying or infusible at a temperature higher than 250° to 300° C. therefrom using more than one filter net of meshes finer than 200 mesh at a rate of 0.5 to 2 g/min/cm 2 , introducing the thus filtered pitch at a temperature of 250° to 300° C. in the form of laminar flow of 1 to 30 mm in thickness into a vessel at a reduced pressure of 300 to 500 mm Hg of an inert gas to remove volatile fractions and bubbles from said filtered pitch in the laminar flow, thereby obtaining a treated pitch containing substantially no bubbles and no components non-liquefying or infusible at a temperature of 250° to 300° C., containing less than 5% by weight of low-molecular weight fractions boiling at a temperature lower than 500° C.
Claim 2
Dependent Claim
184 words
A process for preparing a pitch suitable for use in producing carbon fibers comprising: filtering at a temperature of 250° to 300° C. a heavy petroleum pitch, containing 20 to 45% by weight of compounds insoluble in benzene and having a softening point of 150° to 200° C., to remove fractions non-liquefying or infusible at a temperature higher than 250° to 300° C. therefrom using more than one filter net of meshes finer than 200 mesh at a rate of 0.5 to 2 g/min/cm 2 , introducing the thus filtered pitch at a temperature of 250° to 300° C. in the form of laminar flow of 1 to 30 mm in thickness into a vessel at a reduced pressure of 300 to 500 mm Hg of an inert gas to remove volatile fractions and bubbles from said filtered pitch in the laminar flow, thereby obtaining a treated pitch containing substantially no bubbles and no components non-liquefying or infusible at a temperature of 250° to 300° C., containing less than 5% by weight of low-molecular weight fractions boiling at a temperature lower than 500° C.
Claim 3
Dependent Claim
13 words
The process according to claim 1, wherein said inert gas is gaseous nitrogen.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-01-06 | 1984-07-07 | 1985-01-06 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-01-06 | 1988-07-07 | 1989-01-06 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-01-06 | 1992-07-07 | 1993-01-06 | $7700.00 | Window Closed / Lapsed |