US4239833A
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US
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Grid of precious metals for the recovery of platinum metals escaping from a catalyst during the reaction, and especially of platinum during oxidation of ammonia
Abstract The subject of the invention is a grid of precious metals for the recovery of platinum metals escaping from a catalyst during the reaction of oxidation of ammonia in the production process of nitric oxide. In the reactions conducted in the presence of the catalysts containing platinum metals at the incandesence temperature a loss in the mass of precious metals occurs, which disadvantageously effects the economy of the process. For the recovery of platinum escaping from a catalyst during the reaction of oxidation of ammonia the grids mainly used are those made of palladium-gold alloy, which, in order to increase their strength, are spot-welded into packs, or the separating grids of heat-resisting materials are used. The known methods of increasing the strength and the durability of the recovery grids are disadvantageous, as the flow of reactants through a pack of grids meets additional resistance, which causes a decrease of the process effectiveness. The grid according to the invention is characterized by a different thickness of wires in the weave of the grid made of the same precious metals which are used for the recovery of platinum metals. The wires of various thickness are applied, depending on the type of the catalytic process.
In a grid of precious metals for the recovery of platinum metals escaping from a catalyst during the reaction, especially of platinum during oxidation of ammonia, wherein the grid contains wires of different thickness in the weave which are made of the known precious metals used for the recovery, the improvements which are characterized in that for pressureless catalytic processes the difference in the thickness of wires in the weave is from 30% to 400%, for medium-pressure catalytic processes the difference in the thickness of the wires is from 60% to 600%, for high-pressure catalytic processes the difference in the thickness of the wires is from 100% to 1000%, and in that the thicker wires in the weave are arranged between every 10 to 200 of the thinner wires.
Claim 2
Dependent Claim
129 words
In a grid of precious metals for the recovery of platinum metals escaping from a catalyst during the reaction, especially of platinum during oxidation of ammonia, wherein the grid contains wires of different thickness in the weave which are made of the known precious metals used for the recovery, the improvements which are characterized in that for pressureless catalytic processes the difference in the thickness of wires in the weave is from 30% to 400%, for medium-pressure catalytic processes the difference in the thickness of the wires is from 60% to 600%, for high-pressure catalytic processes the difference in the thickness of the wires is from 100% to 1000%, and in that the thicker wires in the weave are arranged between every 10 to 200 of the thinner wires.
Claim 3
Dependent Claim
26 words
The grid according to claim 1, characterized in that the thicker wires in the weave are arranged in the warp and the weft of the grid.
Claim 4
Dependent Claim
24 words
The grid according to claim 1, characterized in that the thicker wires in the weave are arranged unidirectionally in the warp or the weft.