Patent US4238295A successfully refreshed from Google Patents.
US4238295A
Expired / Lapsed
US
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Energy efficient recovery of acrylonitrile
Assignee: Standard Oil Co
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Filing: 1978-12-04
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Granted: 1980-12-09
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Expires: 1998-12-04
Abstract
Abstract Substantial operating cost savings are realized in the recovery of acrylonitrile from an aqueous solution containing acrylonitrile by using the recovery column bottoms stream to provide heat to one or more distillation columns in the process.
Inventors
- 👤 Paul S. Odom
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 11:56
CPC Classifications
C; C07; C07C; C07C253/00; C07C253/32; C07C253/34; Y; Y02; Y02P; Y02P20/00; Y02P20/50; Y10; Y10S; Y10S203/00; Y10S203/03
Claims Analysis
Total Claims: 3
Claim 1
Independent Claim
144 words
In the process for the recovery and purification of acrylonitrile from an aqueous solution of acrylonitrile, acetonitrile, HCN and impurities consisting of the steps of: (a) distilling said aqueous solution in an extractive distillation column with solvent water to produce an overhead stream of acrylonitrile, HCN and water, and a bottoms stream of water and impurities; (b) distilling in a second distillation column the overhead stream of (a) to produce a second overhead stream of HCN and water, and a second bottoms stream of acrylonitrile and impurities; (c) distilling in a product column the second bottoms stream of (b) to recover product quality acrylonitrile, the improvement comprising; passing said bottoms stream of (a) in indirect heat exchange relationship with liquid from the second distillation column of (b) followed by the liquid from the product column of (c) to provide heat to the respective columns.
Claim 2
Dependent Claim
144 words
In the process for the recovery and purification of acrylonitrile from an aqueous solution of acrylonitrile, acetonitrile, HCN and impurities consisting of the steps of: (a) distilling said aqueous solution in an extractive distillation column with solvent water to produce an overhead stream of acrylonitrile, HCN and water, and a bottoms stream of water and impurities; (b) distilling in a second distillation column the overhead stream of (a) to produce a second overhead stream of HCN and water, and a second bottoms stream of acrylonitrile and impurities; (c) distilling in a product column the second bottoms stream of (b) to recover product quality acrylonitrile, the improvement comprising; passing said bottoms stream of (a) in indirect heat exchange relationship with liquid from the second distillation column of (b) followed by the liquid from the product column of (c) to provide heat to the respective columns.
Claim 3
Dependent Claim
39 words
The process of claim 1 including the additional step of passing said bottoms stream of (a), after providing heat to said distillation columns, in indirect heat exchange relationship with the aqueous solution of step (a) prior to extractive distillation.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1983-12-09 | 1984-06-09 | 1984-12-09 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1987-12-09 | 1988-06-09 | 1988-12-09 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1991-12-09 | 1992-06-09 | 1992-12-09 | $7700.00 | Window Closed / Lapsed |