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US4238295A Expired / Lapsed US ⏱️ 0.0 years remaining

Energy efficient recovery of acrylonitrile

Assignee: Standard Oil Co
•
Filing: 1978-12-04
•
Granted: 1980-12-09
•
Expires: 1998-12-04
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Abstract

Abstract Substantial operating cost savings are realized in the recovery of acrylonitrile from an aqueous solution containing acrylonitrile by using the recovery column bottoms stream to provide heat to one or more distillation columns in the process.

Inventors

  • 👤 Paul S. Odom

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 01:01
CPC Classifications
C; C07; C07C; C07C253/00; C07C253/32; C07C253/34; Y; Y02; Y02P; Y02P20/00; Y02P20/50; Y10; Y10S; Y10S203/00; Y10S203/03

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 144 words
In the process for the recovery and purification of acrylonitrile from an aqueous solution of acrylonitrile, acetonitrile, HCN and impurities consisting of the steps of: (a) distilling said aqueous solution in an extractive distillation column with solvent water to produce an overhead stream of acrylonitrile, HCN and water, and a bottoms stream of water and impurities; (b) distilling in a second distillation column the overhead stream of (a) to produce a second overhead stream of HCN and water, and a second bottoms stream of acrylonitrile and impurities; (c) distilling in a product column the second bottoms stream of (b) to recover product quality acrylonitrile, the improvement comprising; passing said bottoms stream of (a) in indirect heat exchange relationship with liquid from the second distillation column of (b) followed by the liquid from the product column of (c) to provide heat to the respective columns.
Claim 2
Dependent Claim 144 words
In the process for the recovery and purification of acrylonitrile from an aqueous solution of acrylonitrile, acetonitrile, HCN and impurities consisting of the steps of: (a) distilling said aqueous solution in an extractive distillation column with solvent water to produce an overhead stream of acrylonitrile, HCN and water, and a bottoms stream of water and impurities; (b) distilling in a second distillation column the overhead stream of (a) to produce a second overhead stream of HCN and water, and a second bottoms stream of acrylonitrile and impurities; (c) distilling in a product column the second bottoms stream of (b) to recover product quality acrylonitrile, the improvement comprising; passing said bottoms stream of (a) in indirect heat exchange relationship with liquid from the second distillation column of (b) followed by the liquid from the product column of (c) to provide heat to the respective columns.
Claim 3
Dependent Claim 39 words
The process of claim 1 including the additional step of passing said bottoms stream of (a), after providing heat to said distillation columns, in indirect heat exchange relationship with the aqueous solution of step (a) prior to extractive distillation.

References Cited (Backward Citations)

US3328266A Cited
US3073753A Cited
US3462477A Cited
US3936360A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1983-12-09 1984-06-09 1984-12-09 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1987-12-09 1988-06-09 1988-12-09 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1991-12-09 1992-06-09 1992-12-09 $7700.00 Window Closed / Lapsed

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