Patent US4234698A successfully refreshed from Google Patents.
US4234698A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method of making cured aminoplast foam
Assignee: British Industrial Plastics Ltd
•
Filing: 1978-12-04
•
Granted: 1980-11-18
•
Expires: 1998-12-04
Abstract
Abstract A method of making a cured foamed amino formaldehyde product utilizes an amino formaldehyde precondensate of water content below 20% by weight in order to obtain a less brittle product. A liquid foamable composition is made by dispersing a curing catalyst and a blowing agent in the precondensate and the composition is heated to cause the blowing agent to form a foam and the precondensate to cure.
Inventors
- 👤 George Inverarity
- 👤 Dennis H. Ogden
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 18:22
CPC Classifications
C; C08; C08J; C08J9/00; C08J9/04; C08J9/12; C08J9/14; C08J9/141; C08L; C08L61/00; C08L61/20; C08J2361/00; C08J2361/20
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
171 words
In a method of making a cured foamed aminoformaldehyde product by (a) dispersing a curing catalyst and a blowing agent in a liquid aminoformaldehyde precondensate to obtain a liquid foamable composition, and (b) heating the composition to a temperature such as to cause the flowing agent to form a foam and the aminoformaldehyde precondensate to cure, the improvement which consists in (1) employing as the aminoformaldehyde precondensate one that has a water content less than 20% by weight and a viscosity in the range of about 400 to about 1300 poise at 25° C., and is obtained from a reaction mixture which consists essentially of urea, a source of formaldehyde selected from paraformaldehyde and hexamine, and a reaction modifier to maintain the reaction mixture in the liquid phase, said modifier being selected from ethylene urea, a melamine-formaldehyde precondensate, melamine, diethylene glycol, polyvinyl alcohol, a water-soluble carbohydrate, and dicyandiamide, and (2) formulating the foamable composition so that, at the temperature at which foaming begins, its viscosity is in the range 100-1000 poise.
Claim 2
Dependent Claim
171 words
In a method of making a cured foamed aminoformaldehyde product by (a) dispersing a curing catalyst and a blowing agent in a liquid aminoformaldehyde precondensate to obtain a liquid foamable composition, and (b) heating the composition to a temperature such as to cause the flowing agent to form a foam and the aminoformaldehyde precondensate to cure, the improvement which consists in (1) employing as the aminoformaldehyde precondensate one that has a water content less than 20% by weight and a viscosity in the range of about 400 to about 1300 poise at 25° C., and is obtained from a reaction mixture which consists essentially of urea, a source of formaldehyde selected from paraformaldehyde and hexamine, and a reaction modifier to maintain the reaction mixture in the liquid phase, said modifier being selected from ethylene urea, a melamine-formaldehyde precondensate, melamine, diethylene glycol, polyvinyl alcohol, a water-soluble carbohydrate, and dicyandiamide, and (2) formulating the foamable composition so that, at the temperature at which foaming begins, its viscosity is in the range 100-1000 poise.
Claim 3
Dependent Claim
28 words
A method according to claim 1, in which the aminoformaldehyde precondensate is brought to a pH in the range 7-8.5 before the curing catalyst is dispersed in it.
Claim 4
Dependent Claim
20 words
A method according to claim 1 in which the viscosity of the foamable composition is in the range 100-200 poise.
Claim 5
Dependent Claim
29 words
A method according to claim 1 in which the precondensate of water content less than 20% by weight is one obtained from urea, paraformaldehyde, hexamine, and a melamine-formldehyde precondensate.
Claim 6
Dependent Claim
27 words
A method according to claim 1, in which the precondensate of water less than 20% by weight is one obtained from urea, paraformaldehyde, hexamine and ethylene urea.
References Cited (Backward Citations)
GB586199A
Cited
US2789095A
Cited
US2807595A
Cited
US4026980A
Cited
US3975318A
Cited
US3975319A
Cited
US4035456A
Cited
US4069175A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1983-11-18 | 1984-05-19 | 1984-11-18 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1987-11-18 | 1988-05-19 | 1988-11-18 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1991-11-18 | 1992-05-19 | 1992-11-18 | $7700.00 | Window Closed / Lapsed |