US4234627A — Fabric conditioning compositions

Claim 1

Independent Claim 159 words

A granular laundry presoaking/washing composition comprising: (A) from about 3% to 20% by weight of a granular fabric treatment mixture, the granules within said mixture comprising (i) water-insoluble, friable microcapsules varying in size from about 5 to 500 microns, each microcapsule consisting essentially of (a) a liquid core containing fabric conditioning agent; and (b) a solid thin polymeric shell completely surrounding said core; said shell having an average thickness ranging between about 0.1 and 50 microns; and (ii) a substantially water-insoluble, fabric substantive capsule transfer agent having a melting point between about 40° C. and 150° C.; said capsule transfer agent surrounding each microcapsule; the weight ratio of microcapsules to capsule transfer agent within each granule of the fabric treatment mixture between about 0.002:1 and 2000:1; and (B) from about 5% to 90% by weight of a presoaking/washing adjuvant selected from the group consisting of water-soluble detersive surfactants, detergency builders and mixtures of water-soluble detersive surfactants and detergency builders.

Claim 2

Dependent Claim 159 words

A granular laundry presoaking/washing composition comprising: (A) from about 3% to 20% by weight of a granular fabric treatment mixture, the granules within said mixture comprising (i) water-insoluble, friable microcapsules varying in size from about 5 to 500 microns, each microcapsule consisting essentially of (a) a liquid core containing fabric conditioning agent; and (b) a solid thin polymeric shell completely surrounding said core; said shell having an average thickness ranging between about 0.1 and 50 microns; and (ii) a substantially water-insoluble, fabric substantive capsule transfer agent having a melting point between about 40° C. and 150° C.; said capsule transfer agent surrounding each microcapsule; the weight ratio of microcapsules to capsule transfer agent within each granule of the fabric treatment mixture between about 0.002:1 and 2000:1; and (B) from about 5% to 90% by weight of a presoaking/washing adjuvant selected from the group consisting of water-soluble detersive surfactants, detergency builders and mixtures of water-soluble detersive surfactants and detergency builders.

Claim 3

Dependent Claim 67 words

A composition in accordance with claim 1 wherein (A) the microcapsule shell wall material is selected from the group consisting of polyurethanes, polyolefins, polyamides, polyesters, polysaccharides, silicone resins, epoxy resins and aminoplast polymers derived from urea and aldehydes; (B) the fabric conditioning agent is a perfume; and (C) the capsule transfer agent is selected from the group consisting of cationic and nonionic organic materials and mixtures thereof.

Claim 4

Dependent Claim 42 words

A composition in accordance with claim 2 wherein the presoaking/washing adjuvant comprises from about 5% to 25% by weight of the composition of a water-soluble detersive surfactant and from about 30% to 50% by weight of the composition of a detergency builder.

Claim 5

Dependent Claim 149 words

A composition in accordance with claim 2 wherein the presoaking/washing adjuvant comprises (A) from about 0% to 7% by weight of the composition of a detersive surfactant selected from the group consisting of linear alkyl benzene sulfonates having from 11 to 14 carbon atoms in the alkyl group, alkylsulfates having from 12 to 20 carbon atoms in the alkyl group, alkyl glyceryl sulfonates having from 8 to 18 carbon atoms in the alkyl group, alkyl ether sulfates having from 14 to 18 carbon atoms in the alkyl group and an average degree of ethoxylation between 1 and 6, the water-soluble ethoxylates of aliphatic alcohols containing from 10 to 20 carbon atoms and mixtures of these surfactants; and (B) from about 30% to 90% by weight of a detergency builder selected from the group consisting of water-soluble phosphates, pyrophosphates, orthophosphates, polyphosphates, carbonates, bicarbonates, borates, silicates, polyacetates, carboxylates, polycarboxylates and succinates.

Claim 6

Dependent Claim 35 words

A composition in accordance with claim 4 wherein the capsule transfer agent is a nonionic fabric softening agent selected from the group consisting of the C 14 to C 18 alkyl sorbitan tri- and tetra-esters.

Claim 7

Dependent Claim 111 words

A composition in accordance with claim 4 wherein the capsule transfer agent is a water-insoluble mixture of nonionic and cationic fabric softeners, said mixtures being selected from the group consisting of (a) mixtures of C 10 to C 22 alkyl sorbitan tri- and tetra-esters with C 12 to C 22 dialkyl, dimethylammonium salts in a sorbitan ester/quaternary salt weight ratio of from about 1:4 to 4:1, and (b) mixtures of C 10 to C 22 alkyl sorbitan tri- and tetra-esters and C 14 to C 20 fatty alcohols with C 12 to C 20 dialkyl, dimethyl ammonium salts in a total nonionic/quaternary salt weight ratio of from about 1:4 to 4:1.

Claim 8

Dependent Claim 38 words

A composition in accordance with claim 4 wherein the capsule transfer agent is selected from the group consisting of 2:1 mixtures of sorbitan tristearate with ditallowdimethylammonium methylsulfate and 1:1:1 mixtures of sorbitan tristearate, tallow alcohol and ditallowdimethylammonium methylsulfate.

Claim 9

Dependent Claim 58 words

A composition in accordance with claim 2 wherein (A) the microcapsule shell wall material is a urea-formaldehyde polymer having an average shell wall thickness of from about 0.4 to 4.0 microns; (B) the microcapsules vary in size between 10 and 100 microns; and (C) the weight ratio of microcapsules to capsules transfer agent varies between 0.008:1 and 3:1.

Claim 10

Dependent Claim 60 words

A composition in accordance with claim 2 which additionally contains a detergent adjuvant selected from the group consisting of a peroxygen bleaching agent present to the extent of from about 1% to 45% by weight a detergency enzyme component present to the extent of from about 0.1% to 1% by weight and mixtures of said bleaching agent and enzyme components.

Claim 11

Dependent Claim 147 words

A process for conditioning fabrics comprising the steps of: (A) contacting said fabrics in an aqueous bath with an effective amount of a composition comprising: 1. from about 3% to 20% by weight of a granular fabric treatment mixture, the granules within said mixture comprising (i) water-insoluble; friable microcapsules varying in size from about 5 to 500 microns, each microcapsule consisting essentially of (a) a liquid core containing fabric conditioning agent; and (b) a solid thin polymeric shell completely surrounding said core; said shell having an average thickness ranging between about 0.1 and 50 microns; and (ii) a substantially water-insoluble, fabric substantive capsule transfer agent having a melting point between about 40° C. and 150° C.; said capsule transfer agent surrounding each microcapsule; the weight ratio of microcapsules to capsule transfer agent within each granule of the fabric treatment mixture ranging between about 0.002:1 and 2000:1; and

Claim 12

Dependent Claim 147 words

A process for conditioning fabrics comprising the steps of: (A) contacting said fabrics in an aqueous bath with an effective amount of a composition comprising: 1. from about 3% to 20% by weight of a granular fabric treatment mixture, the granules within said mixture comprising (i) water-insoluble; friable microcapsules varying in size from about 5 to 500 microns, each microcapsule consisting essentially of (a) a liquid core containing fabric conditioning agent; and (b) a solid thin polymeric shell completely surrounding said core; said shell having an average thickness ranging between about 0.1 and 50 microns; and (ii) a substantially water-insoluble, fabric substantive capsule transfer agent having a melting point between about 40° C. and 150° C.; said capsule transfer agent surrounding each microcapsule; the weight ratio of microcapsules to capsule transfer agent within each granule of the fabric treatment mixture ranging between about 0.002:1 and 2000:1; and

Claim 13

Dependent Claim 53 words

from about 5% to 90% by weight of a presoaking/washing adjuvant selected from the group consisting of water-soluble detersive surfactants, detergency builders and mixtures of water-soluble detersive surfactants and detergency builders; and (B) manipulating said fabrics in an automatic clothes dryer at a temperature of from about 38° C. to about 100° C.

Claim 14

Dependent Claim 53 words

from about 5% to 90% by weight of a presoaking/washing adjuvant selected from the group consisting of water-soluble detersive surfactants, detergency builders and mixtures of water-soluble detersive surfactants and detergency builders; and (B) manipulating said fabrics in an automatic clothes dryer at a temperature of from about 38° C. to about 100° C.

Claim 15

Dependent Claim 14 words

A process according to claim 10 wherein the fabric conditioning agent is a perfume.

Claim 16

Dependent Claim 34 words

A process according to claim 11 wherein the capsule transfer agent is a nonionic fabric softening agent selected from the group consisting of the C 14 to C 18 alkyl sorbitan tri- and tetra-esters.

Claim 17

Dependent Claim 148 words

A process according to claim 11 wherein the presoaking/washing adjuvant comprises: (A) from about 0% to 7% by weight of the composition of a detersive surfactant selected from the group consisting of linear alkyl benzene sulfonates having from 11 to 14 carbon atoms in the alkyl group, alkylsulfates having from 12 to 20 carbon atoms in the alkyl group, alkyl glyceryl sulfonates having from 8 to 18 carbon atoms in the alkyl group, alkyl ether sulfates having from 14 to 18 carbon atoms in the alkyl group and an average degree of ethoxylation between 1 and 6, the water-soluble ethoxylates of aliphatic alcohols containing from 10 to 20 carbon atoms and mixtures of these surfactants; and (B) from about 30% to 90% by weight of a detergency builder selected from the group consisting of water-soluble phosphates, pyrophosphates, orthophosphates, polyphosphates, carbonates, bicarbonates, borates, silicates, polyacetates, carboxylates, polycarboxylates and succinates.

Annuity Stage	Window Opens	Payment Deadline	Surcharge Period Until	Estimated Fee	Status
3.5 Years (Year 4)	1983-11-18	1984-05-19	1984-11-18	$2000.00	Window Closed / Lapsed
7.5 Years (Year 8)	1987-11-18	1988-05-19	1988-11-18	$3760.00	Window Closed / Lapsed
11.5 Years (Year 12)	1991-11-18	1992-05-19	1992-11-18	$7700.00	Window Closed / Lapsed

Fabric conditioning compositions

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