Claims Analysis
Total Claims: 11
Claim 1
Independent Claim
254 words
A process for the manufacture of coarse aluminum hydroxide having a maximum of 15 weight percent of particles with a diameter less than 45 micrometers by a two stage decomposition of a supersaturated alkaline aluminate solution, by the addition of aluminum hydroxide seed material of different quality to said aluminate solution in each of said two stages, which comprises (a) distributing the quantity of aluminum hydroxide seed material as follows: adding to said aluminate solution a first addition of fine seed material (primary seed material) in a first stage of the decomposition, where the quantity thereof is so calculated that the ratio between the supersaturation in grams of Al 2 O 3 per liter of aluminate liquor and the surface area of said seed material expressed in square meters per liter of aluminate liquor lies between 7 and 25 grams per square meter; and adding to said aluminate solution a second addition of coarse seed material (secondary seed material) in a second stage of the decomposition after an interval of approximately two hours after the first addition such that the total amount of seed material (primary and secondary seed material) is at least 130 grams Al(OH) 3 per liter of aluminate liquor; and (b) regulating the temperature of the decomposition in the following manner: conducting said first stage of the decomposition in a temperature range of 77 degrees Celsius to 66 degrees Celsius; and conducting said second stage of the decomposition at a reduced temperature which can be down to approximately 40 degrees Celsius.
Claim 2
Dependent Claim
254 words
A process for the manufacture of coarse aluminum hydroxide having a maximum of 15 weight percent of particles with a diameter less than 45 micrometers by a two stage decomposition of a supersaturated alkaline aluminate solution, by the addition of aluminum hydroxide seed material of different quality to said aluminate solution in each of said two stages, which comprises (a) distributing the quantity of aluminum hydroxide seed material as follows: adding to said aluminate solution a first addition of fine seed material (primary seed material) in a first stage of the decomposition, where the quantity thereof is so calculated that the ratio between the supersaturation in grams of Al 2 O 3 per liter of aluminate liquor and the surface area of said seed material expressed in square meters per liter of aluminate liquor lies between 7 and 25 grams per square meter; and adding to said aluminate solution a second addition of coarse seed material (secondary seed material) in a second stage of the decomposition after an interval of approximately two hours after the first addition such that the total amount of seed material (primary and secondary seed material) is at least 130 grams Al(OH) 3 per liter of aluminate liquor; and (b) regulating the temperature of the decomposition in the following manner: conducting said first stage of the decomposition in a temperature range of 77 degrees Celsius to 66 degrees Celsius; and conducting said second stage of the decomposition at a reduced temperature which can be down to approximately 40 degrees Celsius.
Claim 3
Dependent Claim
18 words
A process according to claim 1 wherein the time of the first decomposition stage is about six hours.
Claim 4
Dependent Claim
28 words
A process according to claim 1 wherein the caustic liquor concentration expressed in grams of Na 2 O caustic per liter is at least 100 grams per liter.
Claim 5
Dependent Claim
20 words
A process according to claim 1 including the step of continuously applying cooling at said second stage of the decomposition.
Claim 6
Dependent Claim
24 words
A process according to claim 1 including the step of applying cooling at the second stage of the decomposition in one or more steps.
Claim 7
Dependent Claim
30 words
A process according to claim 1 including applying cooling at said second stage of the decomposition and adding said coarse seed material immediately before, during, or immediately after said cooling.
Claim 8
Dependent Claim
32 words
A process according to claim 1 wherein the ratio of supersaturation of the liquor to the surface area of the primary seed material is between 7 and 16 grams per square meter.
Claim 9
Dependent Claim
23 words
A process according to claim 1 wherein the total amount of seed in said second stage does not exceed 400 grams per liter.
Claim 10
Dependent Claim
16 words
A process according to claim 1 wherein said secondary seed material is added at one time.
Claim 11
Dependent Claim
19 words
A process according to claim 1 including the step of applying cooling following said first stage of the decomposition.