Abstract Flocculent furnace carbon black is produced by contacting a feed hydrocarbon with hot combustion gases to pyrolyze the feed hydrocarbon. The hot combustion products produced by pyrolyzing include flocculent carbon black suspended in gases and are quenched to form a cooled effluent. The effluent is subjected to separation to separate the flocculent carbon black from the gases. The combustion products are cooled by quenching in a manner to maintain a photelometer value of the flocculent carbon black in predetermined range such that when the separated flocculent carbon black is subsequently pelleted a minimum loss of modulus results in the rubber into which the pelleted carbon black is compounded. The flocculent carbon black is pelleted under prescribed pelleting conditions and is dried under prescribed drying conditions to help achieve minimum modulus loss in the end product.
A method of producing pelleted carbon black to reduce modulus loss comprising: providing flocculent carbon black having a toluene photelometer of between about 45 and 65 or a chloroform photelometer of between about 78 and about 90, an N 2 SA-CTAB value of less than about 10 m 2 /gm, an N 2 SA-I 2 adsorption number of between about 6 and about 20, and a nitrogen surface area of between about 75 m 2 /gm and about 140 m 2 /gm; pelleting said flocculent carbon black using an aqueous pelleting liquid substantially free of additives to form carbon black pellets; drying said carbon black pellets at a temperature of less than about 300° F. in an environment containing less than about 8 volume percent free oxygen; and recovering the thus dried pellets.
Claim 2
Independent Claim
133 words
A method of producing pelleted carbon black to reduce modulus loss comprising: providing flocculent carbon black having a toluene photelometer of between about 45 and 65 or a chloroform photelometer of between about 78 and about 90, an N 2 SA-CTAB value of less than about 10 m 2 /gm, an N 2 SA-I 2 adsorption number of between about 6 and about 20, and a nitrogen surface area of between about 75 m 2 /gm and about 140 m 2 /gm; pelleting said flocculent carbon black using an aqueous pelleting liquid substantially free of additives to form carbon black pellets; drying said carbon black pellets at a temperature of less than about 300° F. in an environment containing less than about 8 volume percent free oxygen; and recovering the thus dried pellets.
Claim 3
Dependent Claim
29 words
A method as set forth in claim 1 wherein: said pellets are dried to a moisture content of less than about 0.5 percent by weight of the dried pellets.