Patent US4218262A successfully refreshed from Google Patents.
US4218262A
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US
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Nonclumping, delayed action viscosity increasing agent
Assignee: Balchem Corp
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Filing: 1978-11-02
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Granted: 1980-08-19
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Expires: 1998-11-02
Abstract
Abstract A nonclumping, delayed action viscosity increasing agent comprising core particles of xanthan gum and an encapsulating coating of a fat derivative selected from the group consisting of fatty acids and mono and diglycerides of fatty acids and a surfactant wherein the coating has a hydrophilic/lipophilic balance from 3.5 to 10. Methods of forming the encapsulated particles are also disclosed.
Inventors
- 👤 Charlotte L. Warren
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 21:38
CPC Classifications
C; C08; C08L; C08L5/00; A; A23; A23L; A23L29/00; A23L29/20; A23L29/269; A23L29/27
Claims Analysis
Total Claims: 22
Claim 1
Independent Claim
94 words
A nonclumping, delayed action viscosity increasing agent comprising (a) 90 to 10% core particles of xanthan gum, and (b) 10 to 90% encapsulating coating on said particles comprising: (i) 90 to 99.5% of a fat derivative selected from the group consisting of fatty acids having from 12 to 22 carbon atoms, monoglycerides of fatty acids having from 12 to 22 carbon atoms, diglycerides of fatty acids having from 12 to 22 carbon atoms and mixtures thereof; and (ii) 0.5 to 10% of a surfactant; said coating having a hydrophilic/lipophilic balance from 3.5 to 10.
Claim 2
Dependent Claim
94 words
A nonclumping, delayed action viscosity increasing agent comprising (a) 90 to 10% core particles of xanthan gum, and (b) 10 to 90% encapsulating coating on said particles comprising: (i) 90 to 99.5% of a fat derivative selected from the group consisting of fatty acids having from 12 to 22 carbon atoms, monoglycerides of fatty acids having from 12 to 22 carbon atoms, diglycerides of fatty acids having from 12 to 22 carbon atoms and mixtures thereof; and (ii) 0.5 to 10% of a surfactant; said coating having a hydrophilic/lipophilic balance from 3.5 to 10.
Claim 3
Dependent Claim
20 words
A viscosity increasing agent according to claim 1 wherein the hydrophilic/lipophilic balance of said coating is from 3.5 to 6.
Claim 4
Dependent Claim
21 words
A viscosity increasing agent according to claim 1 wherein the size of the core particles ranges between 325 and 20 mesh.
Claim 5
Dependent Claim
26 words
A viscosity increasing agent according to claim 3 wherein the average size of the core particles lies in the range from 140 mesh to 200 mesh.
Claim 6
Dependent Claim
20 words
A viscosity increasing agent according to claim 1 wherein said coating has a melting point of at least 40° C.
Claim 7
Dependent Claim
25 words
A viscosity increasing agent according to claim 5 wherein the melting point of the coating lies in the range from 45° C. to 80° C.
Claim 8
Dependent Claim
20 words
A viscosity increasing agent according to claim 1 wherein the gum core comprises from 25 to 60% of each particle.
Claim 9
Dependent Claim
35 words
A viscosity increasing agent according to claim 1 wherein said fat derivative is selected from the group consisting of saturated fatty acids, monoglycerides of saturated fatty acids, diglycerides of saturated fatty acids and mixtures thereof.
Claim 10
Dependent Claim
30 words
A viscosity increasing agent according to claim 8 wherein said fat derivative comprises a mixture of mono and diglycerides of saturated fatty acids having from 12 to 22 carbon atoms.
Claim 11
Dependent Claim
18 words
A viscosity increasing agent according to claim 9 wherein said fat derivative comprises at least 30% alpha monoglyceride.
Claim 12
Dependent Claim
18 words
A viscosity increasing agent according to claim 10 wherein said fat derivative comprises at least 90% alpha monoglyceride.
Claim 13
Dependent Claim
53 words
A viscosity increasing agent according to claim 2 wherein the coating has a retarding effect on the dissolution of the gum particles such that when the coated particles are added to an aqueous medium at a temperature between 10° and 30° C., none of the gum dissolves within a period of two minutes.
Claim 14
Dependent Claim
19 words
A viscosity increasing agent according to claim 12 wherein all of the gum core particles dissolve within 24 hours.
Claim 15
Dependent Claim
56 words
A viscosity increasing agent according to claim 1 wherein the surfactant is selected from the group consisting of alkali metal salts of fatty acids, sorbitan fatty acid esters, polyoxyethylene modified sorbitan fatty acid esters, polyethylene glycol monoesters, polypropylene glycol monoesters, linear alcohol ethoxylates, alkyl aryl polyethylene glycol ethers, fatty acid esters of sucrose and mixtures thereof.
Claim 16
Independent Claim
87 words
A method of producing a nonclumping, delayed action viscosity increasing agent comprising coating xanthan gum particles with an encapsulating coating comprising (i) 90 to 99.5% of a fat derivative selected from the group consisting of fatty acids having from 12 to 22 carbon atoms, monoglycerides of fatty acids having from 12 to 22 carbon atoms, diglycerides of fatty acids having from 12 to 22 carbon atoms and mixtures thereof and (ii) 0.5 to 10% of a surfactant; said coating having a hydrophilic/lipophilic balance from 3.5 to 10.
Claim 17
Independent Claim
87 words
A method of producing a nonclumping, delayed action viscosity increasing agent comprising coating xanthan gum particles with an encapsulating coating comprising (i) 90 to 99.5% of a fat derivative selected from the group consisting of fatty acids having from 12 to 22 carbon atoms, monoglycerides of fatty acids having from 12 to 22 carbon atoms, diglycerides of fatty acids having from 12 to 22 carbon atoms and mixtures thereof and (ii) 0.5 to 10% of a surfactant; said coating having a hydrophilic/lipophilic balance from 3.5 to 10.
Claim 18
Dependent Claim
18 words
A method according to claim 15 wherein the hydrophilic/lipophilic balance of said coating is from 3.5 to 6.
Claim 19
Dependent Claim
43 words
A method according to claim 15 comprising the steps of melting the fat derivative; mixing the surfactant with the molten fat derivative; suspending the gum particles in the molten fat derivative, and spray chilling the thusly formed suspension to produce encapsulated gum particles.
Claim 20
Dependent Claim
37 words
A method according to claim 15 comprising the steps of dissolving the fat derivative and surfactant in a volatile solvent and spraying the resulting solution onto an agitated bed of gum particles to produce encapsulated gum particles.
Claim 21
Dependent Claim
12 words
A method as recited in claim 18 wherein said solvent is ethanol.
Claim 22
Dependent Claim
54 words
A method according to claim 15 wherein the surfactant is selected from the group consisting of alkali metal salts of fatty acids, sorbitan fatty acid esters, polyoxyethylene modified sorbitan fatty acid esters, polyethylene glycol monoesters, polypropylene glycol monoesters, linear alcohol ethoxylates, alkyl aryl polyethylene glycol ethers, fatty acid esters of sucrose and mixtures thereof.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1983-08-19 | 1984-02-18 | 1984-08-19 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1987-08-19 | 1988-02-18 | 1988-08-19 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1991-08-19 | 1992-02-18 | 1992-08-19 | $7700.00 | Window Closed / Lapsed |