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US4207397A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for recovering and treating brine from water softener regeneration

Assignee: Water Refining Co Inc
•
Filing: 1978-09-15
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Granted: 1980-06-10
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Expires: 1998-09-15
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Abstract

Abstract Cation exchange water softeners may be regenerated and, then, the regenerant wastes (brine) recovered, treated, and recycled. The result is a closed system which is ecologically beneficial. The regenerant brine is captured in as concentrated a form as possible and then treated with a precipitant such as sodium or potassium carbonate or mixtures of sodium or potassium carbonate with sodium or potassium hydroxide. Calcium and magnesium compounds are precipitated and the supernatant contains sodium or potassium chloride. These are separated within the brine treatment tank, the precipitate being disposed of as a sludge or sludge cake and the supernatant being recycled to the water softener at the time of further regeneration.

Inventors

  • 👤 Stephen H. Davis
  • 👤 James E. Etzel

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 07:05
CPC Classifications
B; B01; B01J; B01J49/00; B01J49/50; B01J49/53; B01J49/75

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 223 words
A closed-mode method for regenerating a water softener having a cation exchange resin bed located therein and for recovering and treating the regenerant brine from the water softener regeneration, comprising: (a) backwashing said cation exchange resin bed, (b) evacuating the liquid from said water softener, (c) introducing a saturated brine of regenerating material selected from the group consisting of potassium chloride and sodium chloride into said water softener to a level of approximately 150% or greater of said cation exchange resin bed depth to produce regenerant wastes in the form of a calcium chloride and magnesium chloride containing regenerant brine, (d) evacuating said regenerant brine from said resin bed and recovering a concentrated portion of said regenerant brine for further treatment, (e) treating said regenerant brine with a treatment chemical selected from the group consisting of sodium carbonate, potassium carbonate, a mixture of potassium carbonate and potassium hydroxide, and a mixture of sodium carbonate and sodium hydroxide to produce a calcium and magnesium containing precipitate and a potassium chloride or sodium chloride containing supernatant, (f) separating said precipitate from said supernatant, (g) resaturating said supernatant with additional potassium chloride or sodium chloride regenerating material, and (h) recycling said resaturated supernatant to said water softener at the time of further regeneration, whereby a closed system for water softening and water softener regenerating is achieved.
Claim 2
Dependent Claim 223 words
A closed-mode method for regenerating a water softener having a cation exchange resin bed located therein and for recovering and treating the regenerant brine from the water softener regeneration, comprising: (a) backwashing said cation exchange resin bed, (b) evacuating the liquid from said water softener, (c) introducing a saturated brine of regenerating material selected from the group consisting of potassium chloride and sodium chloride into said water softener to a level of approximately 150% or greater of said cation exchange resin bed depth to produce regenerant wastes in the form of a calcium chloride and magnesium chloride containing regenerant brine, (d) evacuating said regenerant brine from said resin bed and recovering a concentrated portion of said regenerant brine for further treatment, (e) treating said regenerant brine with a treatment chemical selected from the group consisting of sodium carbonate, potassium carbonate, a mixture of potassium carbonate and potassium hydroxide, and a mixture of sodium carbonate and sodium hydroxide to produce a calcium and magnesium containing precipitate and a potassium chloride or sodium chloride containing supernatant, (f) separating said precipitate from said supernatant, (g) resaturating said supernatant with additional potassium chloride or sodium chloride regenerating material, and (h) recycling said resaturated supernatant to said water softener at the time of further regeneration, whereby a closed system for water softening and water softener regenerating is achieved.
Claim 3
Dependent Claim 36 words
The method of claim 1 wherein said calcium and magnesium containing precipitate is separated from said potassium chloride or sodium chloride supernatant by decanting said supernatant from said precipitate as it settles within a separation unit.
Claim 4
Dependent Claim 14 words
The method of claim 2 wherein filtration is used to further dewater said precipitate.
Claim 5
Dependent Claim 46 words
The method of claim 1 wherein said regenerating material is sodium chloride and said treatment chemical is sodium carbonate which is added to said recovered regenerant brine, then, thoroughly blended with said regenerant brine to rapidly and effectively produce said calcium carbonate and magnesium carbonate precipitate.

References Cited (Backward Citations)

US3101316A Cited
US3350292A Cited
US3528912A Cited
US3977968A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1983-06-10 1983-12-10 1984-06-10 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1987-06-10 1987-12-10 1988-06-10 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1991-06-10 1991-12-10 1992-06-10 $7700.00 Window Closed / Lapsed

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