Patent US4202909A successfully refreshed from Google Patents.
US4202909A
Expired / Lapsed
US
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Treatment of whey
Assignee: Foremost Farms USA Cooperative
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Filing: 1978-05-19
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Granted: 1980-05-13
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Expires: 1998-05-19
Abstract
Abstract A high yield of relatively pure lactose and salt products are produced from a permeate resulting from ultrafiltration of whey by precipitating calcium and citrate salts from the permeate without substantial precipitation of phosphate salts by concentrating the permeate to a solids content of about 40 to 45% and holding at about 180° to 200° F. for 30 to 90 minutes, removing precipitated solids from the permeate and then further concentrating the permeate and crystallizing and removing lactose.
Inventors
- 👤 Harold T. Pederson, Jr.
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-09 09:57
CPC Classifications
C; C13; C13K; C13K5/00; A; A23; A23C; A23C9/00; A23C9/14; A23C9/142; A23C9/1425
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
182 words
A process for the treatment of whey derived from the manufacture of cheese and having titratable acidity, the steps of subjecting the whey to membrane ultrafiltration to form a protein-rich fraction and a permeate fraction having a solids content of the order of 5.0 to 7.5% and having a lactose content of about 68 to 87%, a protein content of not more than about 6% and a mineral salt content, the mineral salt content including calcium and citrate salts together with phosphate and monovalent salts, precipitating calcium and citrate salts of the permeate without substantial precipitation of phosphate salts by concentrating the unneutralized permeate to a solids content of about 40 to 45%, and by holding the concentrate at a temperature level of about 180° to 200° F. for about 30 to 90 minutes to effect precipitation of calcium and citrate salts without substantial precipitation of phosphate salts, the precipitated salts being about 5.0 to 15.0% of the total mineral salts, removing the precpitated solids from the permeate, and then further concentrating the permeate and crystallizing and removing lactose from the same.
Claim 2
Dependent Claim
182 words
A process for the treatment of whey derived from the manufacture of cheese and having titratable acidity, the steps of subjecting the whey to membrane ultrafiltration to form a protein-rich fraction and a permeate fraction having a solids content of the order of 5.0 to 7.5% and having a lactose content of about 68 to 87%, a protein content of not more than about 6% and a mineral salt content, the mineral salt content including calcium and citrate salts together with phosphate and monovalent salts, precipitating calcium and citrate salts of the permeate without substantial precipitation of phosphate salts by concentrating the unneutralized permeate to a solids content of about 40 to 45%, and by holding the concentrate at a temperature level of about 180° to 200° F. for about 30 to 90 minutes to effect precipitation of calcium and citrate salts without substantial precipitation of phosphate salts, the precipitated salts being about 5.0 to 15.0% of the total mineral salts, removing the precpitated solids from the permeate, and then further concentrating the permeate and crystallizing and removing lactose from the same.
Claim 3
Dependent Claim
18 words
A process as in claim 1 in which the removed lactose is subjected to washing with acidulated water.
Claim 4
Dependent Claim
52 words
A process as in claim 2 in which the permeate after crystallization and removal of lactose is combined with wash effluent and is subjected to a second precipitating operation to precipitate a substantial amount of mineral salts, removing the mineral salts so precipitated, and then crystallizing and removing lactose from the liquor.
Claim 5
Dependent Claim
53 words
A process as in claim 3 in which the second precipitating operation is carried out by adjusting the pH to 7-10 by addition of a neutralizing agent and by holding at a temperature of about 140° to 150° F. for a time sufficient to effect precipitation of a substantial amount of mineral salts.
Claim 6
Dependent Claim
25 words
A process as in claim 1 in which some of the mineral salts of the whey are removed by electrodialysis before removal of crystallized lactose.
Claim 7
Dependent Claim
34 words
A process as in claim 5 in which some of the mineral salts of the permeate are removed by electrodialysis after removal of the precipitated solids and before said further concentrating of the permeate.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1983-05-13 | 1983-11-12 | 1984-05-13 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1987-05-13 | 1987-11-12 | 1988-05-13 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1991-05-13 | 1991-11-12 | 1992-05-13 | $7700.00 | Window Closed / Lapsed |