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US4187322A Expired / Lapsed US ⏱️ 0.0 years remaining

Powder compositions containing vitamin C active component

Assignee: Hoffmann La Roche Inc
•
Filing: 1976-11-08
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Granted: 1980-02-05
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Expires: 1996-11-08
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Abstract

Abstract Stable, dry, free-flowing powder compositions containing ascorbic acid or salts thereof, methods for their preparation and feedstuff containing the powder compositions are disclosed.

Inventors

  • 👤 Rene Josse
  • 👤 Heinrich Klaui

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 15:54
CPC Classifications
A; A61; A61K; A61K31/00; A61K31/33; A61K31/335; A61K31/365; A61K31/375; A23; A23K; A23K20/00; A23K20/10; A23K20/174

Claims Analysis

Total Claims: 20
Claim 1
Independent Claim 76 words
A dry, stable, free-flowing powder composition which comprises pre-swollen cereal grain having absorbed therein from about 15% to about 45% by weight, based on the total weight of the powder composition, of a vitamin C active component selected from the group consisting of ascorbic acid, an alkali metal salt thereof and an alkaline earth metal salt thereof and wherein said vitamin C active component is obtained from an aqueous solution of said acid or said salts.
Claim 2
Dependent Claim 76 words
A dry, stable, free-flowing powder composition which comprises pre-swollen cereal grain having absorbed therein from about 15% to about 45% by weight, based on the total weight of the powder composition, of a vitamin C active component selected from the group consisting of ascorbic acid, an alkali metal salt thereof and an alkaline earth metal salt thereof and wherein said vitamin C active component is obtained from an aqueous solution of said acid or said salts.
Claim 3
Dependent Claim 25 words
The powder composition of claim 1 which comprises from about 15% to about 25% by weight of ascorbic acid as the vitamin C active component.
Claim 4
Dependent Claim 21 words
The powder composition of claim 2 which comprises about 18% by weight of ascorbic acid as the vitamin C active component.
Claim 5
Dependent Claim 25 words
The powder composition of claim 1 which comprises from about 25% to about 45% by weight of sodium ascorbate as the vitamin C active component.
Claim 6
Dependent Claim 25 words
The powder composition of claim 4 which comprises from about 30% to about 40% by weight of sodium ascorbate as the vitamin C active component.
Claim 7
Dependent Claim 25 words
The powder composition of claim 5 which comprises from about 35% to about 38% by weight of sodium ascorbate as the vitamin C active component.
Claim 8
Dependent Claim 18 words
The powder composition of claim 1 having a particle size range of from about 250μ to about 2000μ.
Claim 9
Independent Claim 91 words
A method for preparing a dry, stable, free-flowing powder composition containing a vitamin C active component which comprises (a) preparing an aqueous mixture of a cereal grain; (b) processing the aqueous mixture of step (a) to form a pre-swollen, non-agglutinating cereal grain in the aqueous mixture; (c) admixing, under an inert atmosphere, the aqueous pre-swollen, non-agglutinating cereal grain mixture of step (b) with a saturated aqueous solution of a vitamin C active component; (d) drying the resulting admixture in an inert gas atmosphere to prepare the dry, stable, free-flowing powder composition.
Claim 10
Independent Claim 91 words
A method for preparing a dry, stable, free-flowing powder composition containing a vitamin C active component which comprises (a) preparing an aqueous mixture of a cereal grain; (b) processing the aqueous mixture of step (a) to form a pre-swollen, non-agglutinating cereal grain in the aqueous mixture; (c) admixing, under an inert atmosphere, the aqueous pre-swollen, non-agglutinating cereal grain mixture of step (b) with a saturated aqueous solution of a vitamin C active component; (d) drying the resulting admixture in an inert gas atmosphere to prepare the dry, stable, free-flowing powder composition.
Claim 11
Dependent Claim 26 words
The method of claim 8 wherein the dried mixture of step (d) is comminuted to a particle size range of from about 250μ to about 2000μ.
Claim 12
Dependent Claim 153 words
The method of claim 8 wherein the aqueous mixture of pre-swollen, non-agglutinating cereal grain of step (b) is prepared by (i) preparing an admixture of from about 40% to about 70% by weight of cereal grain with from about 60% by weight to about 30% by weight of water, all percents by weight based on the weight of the resulting admixture; (ii) heating the mixture of step (i) in an autoclave for from about 3 minutes to about 8 minutes at a temperature of from about 100° to about 140° C.; (iii) removing the mixture from the autoclave; and (iv) drying the mixture in an oven at a temperature of from about 60° C. to about 100° C. until there is a water loss of from about 10% to about 30% by weight based on the total weight of the initial admixture. to thus form the aqueous mixture of pre-swollen, non-agglutinating cereal grain.
Claim 13
Dependent Claim 32 words
The method of claim 8 wherein the aqueous solution of step (c) comprises from about 25% to about 35% on a weight/volume basis of ascorbic acid as the vitamin C active component.
Claim 14
Dependent Claim 32 words
The method of claim 8 wherein the aqueous solution of step (c) comprises from about 40% to about 70% on a weight/volume basis of sodium ascorbate as the vitamin C active component.
Claim 15
Dependent Claim 27 words
The method of claim 8 wherein the drying procedure of step (d) is carried out at a temperature of from about 50° C. to about 80° C.
Claim 16
Dependent Claim 94 words
A stable, vitamin C fortified animal feedstuff which comprises an admixture of (a) an animal feedstuff and (b) a dry, stable, free-flowing powder composition which comprises pre-swollen cereal grain having absorbed therein from about 15% to about 45% by weight, based on the total weight of the powder composition, of a vitamin C active component selected from the group consisting of ascorbic acid, an alkali metal salt thereof and an alkaline earth metal salt thereof and wherein said vitamin C active component is obtained from an aqueous solution of said acid or said salts.
Claim 17
Dependent Claim 94 words
A stable, vitamin C fortified animal feedstuff which comprises an admixture of (a) an animal feedstuff and (b) a dry, stable, free-flowing powder composition which comprises pre-swollen cereal grain having absorbed therein from about 15% to about 45% by weight, based on the total weight of the powder composition, of a vitamin C active component selected from the group consisting of ascorbic acid, an alkali metal salt thereof and an alkaline earth metal salt thereof and wherein said vitamin C active component is obtained from an aqueous solution of said acid or said salts.
Claim 18
Dependent Claim 44 words
The stable, vitamin C fortified animal feedstuff of claim 14 wherein the vitamin C active component of the powder composition is present in a concentration range of from about 100 milligrams to about 200 milligrams of the component per kilogram of the animal feedstuff.
Claim 19
Dependent Claim 19 words
The stable, vitamin C fortified animal feedstuff of claim 15 wherein the vitamin C active component is ascorbic acid.
Claim 20
Dependent Claim 19 words
The stable, vitamin C fortified animal feedstuff of claim 15 wherein the vitamin C active component is sodium ascorbate.

References Cited (Backward Citations)

US2775521A Cited
US3247065A Cited
US3767824A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1983-02-04 1983-08-06 1984-02-05 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1987-02-04 1987-08-06 1988-02-05 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1991-02-04 1991-08-06 1992-02-05 $7700.00 Window Closed / Lapsed

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