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US4182676A Expired / Lapsed US ⏱️ 0.0 years remaining

Method and system for purifying liquid

Assignee: Almag Chemical Corp
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Filing: 1976-08-03
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Granted: 1980-01-08
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Expires: 1996-08-03
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Abstract

Abstract A method and system combining filtration and ion-exchange structures for removing contaminants from liquids. In overall concept, contaminated liquid is passed through filtering mediums to remove particulate matter from the incoming contaminated liquid. Organics are removed from the liquid by passage through adsorbent non-ionic type resins. The liquid is then passed through strong acid cation exchange resins, weak base anion exchange resins, weak acid cation exchange resins, and strong base anion exchange resins arranged in a predetermined location in the liquid flow path to provide optimized contaminant removal. One of the optimization techniques is through the pH adjustment of the liquid at predetermined points in the flow path. Additionally, the liquid to be purified is passed through mixed bed polisher resins as well as chelation resins to provide a final substantially contaminant free liquid which is returned to use in a closed loop fashion.

Inventors

  • 👤 Angelo J. Casolo

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 07:07
CPC Classifications
C; C02; C02F; C02F9/00; B; B01; B01J; B01J39/00; B01J39/04; B01J39/05; B01J45/00; B01J47/00; B01J47/02; B01J47/04; C02F1/00; C02F1/001; C02F1/28; C02F1/283; C02F1/66; C02F1/42; C02F2001/422; C02F2001/425; C02F2101/00; C02F2101/10; C02F2101/105; C02F2101/16; C02F2101/18; C02F2101/20; C02F2101/203; C02F2101/22; C02F2301/00; C02F2301/04; C02F2301/043

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 214 words
A method of purifying mineral contaminated water, said water including mineral contaminants of copper, cadmium, chromium (Cr +6 ), iron, cyanide, and phosphate, including the steps of: (a) dividing said mineral contaminated water from a storage tank into a first stream and a second stream; (b) transporting said first stream through a first plurality of ion exchange resins connected in series flow each to the other including series passage through a strong acid cation exchange resin in the hydrogen form to provide an efflux having a pH value within the range of 1.0 and 5.0, and a weak base anion exchange resin in the hydroxyl form to provide an efflux having a pH value within the range of 7.0 and 10.0, (c) simultaneously passing said second stream through a second plurality of ion exchange resins coupled each to the other in series flow including consecutive series flow through a strong base anion exchange resin in the hydroxyl form to provide an efflux pH value within the range of 7.0-10.0, and a weak acid cation exchange resin in the hydrogen form to provide an efflux having a pH value within the range of 3.0-7.0; and (d) combining liquid efflux of said first and second plurality of ion exchange resins for return to said storage tank.
Claim 2
Independent Claim 214 words
A method of purifying mineral contaminated water, said water including mineral contaminants of copper, cadmium, chromium (Cr +6 ), iron, cyanide, and phosphate, including the steps of: (a) dividing said mineral contaminated water from a storage tank into a first stream and a second stream; (b) transporting said first stream through a first plurality of ion exchange resins connected in series flow each to the other including series passage through a strong acid cation exchange resin in the hydrogen form to provide an efflux having a pH value within the range of 1.0 and 5.0, and a weak base anion exchange resin in the hydroxyl form to provide an efflux having a pH value within the range of 7.0 and 10.0, (c) simultaneously passing said second stream through a second plurality of ion exchange resins coupled each to the other in series flow including consecutive series flow through a strong base anion exchange resin in the hydroxyl form to provide an efflux pH value within the range of 7.0-10.0, and a weak acid cation exchange resin in the hydrogen form to provide an efflux having a pH value within the range of 3.0-7.0; and (d) combining liquid efflux of said first and second plurality of ion exchange resins for return to said storage tank.
Claim 3
Dependent Claim 35 words
The method of purifying contaminated liquid as recited in claim 1 including the step of transporting each of said first and second streams through a plurality of filtering mediums for removing particulates or predetermined size.
Claim 4
Dependent Claim 44 words
The method of purifying contaminated liquid as recited in claim 2 where the step of transporting each of said first and second streams includes the step of passing each of said streams through a coarse filtration medium, said coarse filtration medium being sand particles.
Claim 5
Dependent Claim 54 words
The method of purifying contaminated liquid as recited in claim 3 including the step of filtering each of said first and second streams through a fine filter medium after each of said first and second streams has passed through said coarse filter mediums, said coarse and fine filter mediums being connected in series flow.
Claim 6
Dependent Claim 39 words
The method of purifying contaminated liquid as recited in claim 1 where the step of transporting said first stream includes the step of displacing said first stream through an adsorbent medium for removing organic contaminants from said contaminated liquid.
Claim 7
Dependent Claim 18 words
The method of purifying contaminated liquid as recited in claim 5 where said adsorbent medium is activated carbon.
Claim 8
Dependent Claim 42 words
The method of purifying contaminated liquid as recited in claim 5 where the step of transporting said first stream includes the step of displacing said liquid through said strong acid cation exchange resin after said liquid has passed through said adsorbent medium.
Claim 9
Dependent Claim 49 words
The method of purifying contaminated liquid as recited in claim 1 where the step of passing said stream through said weak acid cation exchange resin is followed by the step of passing said second stream through a mixture of anionic and cationic resins, each being intermixed with the other.
Claim 10
Dependent Claim 27 words
The method of purifying contaminated liquid as recited in claim 8 where said anionic and cationic resin mixture includes approximately 50.0% by volume of said anionic resin.
Claim 11
Dependent Claim 34 words
The method of purifying contaminated liquid as recited in claim 8 where said second stream passes from said weak acid cation exchange resin to said mixture of anionic and cationic resins in series flow.

References Cited (Backward Citations)

US3408289A Cited
US3697419A Cited
US3618589A Cited
US3758405A Cited
US3753899A Cited
US3985648A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1983-01-07 1983-07-09 1984-01-08 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1987-01-07 1987-07-09 1988-01-08 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1991-01-07 1991-07-09 1992-01-08 $7700.00 Window Closed / Lapsed

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