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US4172828A
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Method for processing soy protein and composition of matter
Assignee: CHEESE ANALOG CORP 345 MERCHANDISE MART CHICAGO ILLINOIS 60654 A CORP OF DE
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Filing: 1978-04-27
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Granted: 1979-10-30
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Expires: 1998-04-27
Abstract
Abstract A method for processing soy protein from defatted soybean flakes. Flakes are mixed with water and heated to an elevated temperature of from about 55° C. to about 70° C. to extract solubles therefrom. The extract liquor is cooled over a period of time of from at least one to three hours to a temperature of from about 5° C. to about 10° C. resulting in curd and whey. The curd is separated from the whey and is preserved preferably by either freeze-drying or spray-drying. The curd can be redissolved in water, precipitated by addition of acid, followed by washing of the curd precipitate, adjustment of pH of the washed curd precipitate and drying thereof. The whey from which the curd of the initial extract was separated may be processed by a series of steps generally involving precipitation of additional curd, washing or redissolution of the curd, adjustment of pH, and drying the curd. Four distinct protein fractions result, each having differing and unique physical and/or functional properties.
Inventors
- 👤 Ronald M. Davidson
- 👤 Ralph E. Sand
- 👤 Richard E. Johnson
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-07 21:26
CPC Classifications
A; A23; A23J; A23J1/00; A23J1/14
Claims Analysis
Total Claims: 32
Claim 1
Independent Claim
99 words
A method for processing soy protein from defatted soybean flakes, comprising, (a) mixing the flakes with water and maintaining said mixture at an elevated temperature for a time sufficient to solubilize substantial portion of the protein in the flakes, (b) removing a substantial portion of any insolubles from the mixture of step (a), (c) cooling the liquor of step (b), over a time of at least one to three hours to a temperature of from about 5° C. to about 10° C. resulting in curd and whey, (d) separating the curd from the whey, and (e) preserving the curd.
Claim 2
Independent Claim
99 words
A method for processing soy protein from defatted soybean flakes, comprising, (a) mixing the flakes with water and maintaining said mixture at an elevated temperature for a time sufficient to solubilize substantial portion of the protein in the flakes, (b) removing a substantial portion of any insolubles from the mixture of step (a), (c) cooling the liquor of step (b), over a time of at least one to three hours to a temperature of from about 5° C. to about 10° C. resulting in curd and whey, (d) separating the curd from the whey, and (e) preserving the curd.
Claim 3
Dependent Claim
15 words
The method of claim 1 wherein the curd of step (e) is preserved by freezing.
Claim 4
Dependent Claim
15 words
The method of claim 1 wherein the curd of step (e) is preserved by drying.
Claim 5
Dependent Claim
19 words
The method of claim 3 wherein the drying of the curd is effected by one of freeze-drying or spray-drying.
Claim 6
Dependent Claim
73 words
The method of claim 1 wherein the curd of step (e) is preserved by the additional steps of, (i) mixing the curd with water, (ii) adjusting pH of the resulting mixture to about 5.3 so as to form a curd precipitate, (iii) washing the curd precipitate of step (ii) with water, (iv) adjusting the pH of the washed curd precipitate to from about 6.3 to about 6.8, and (v) drying said curd precipitate.
Claim 7
Dependent Claim
37 words
The method of claim 5 wherein in step (iv) the pH of the washed curd precipitate is adjusted by the addition of a base selected from the group consisting of calcium hydroxide, potassium hydroxide or sodium hydroxide.
Claim 8
Dependent Claim
16 words
The method of claim 1 wherein the defatted soybean flakes have an NSI of about 60.
Claim 9
Dependent Claim
43 words
The method of claim 1 wherein the mixture of step (a) is formed of at least about 5 parts by weight of water to about 1 part by weight of flakes at a temperature of from about 55° C. to about 70° C.
Claim 10
Dependent Claim
20 words
The method of claim 8 wherein the mixture of claim 8 has a pH of about 6.2 to about 6.8.
Claim 11
Dependent Claim
68 words
The method of claim 1 wherein in the cooling step (c), the temperature of the liquor is reduced from an elevated temperature of from about 55° C. to about 70° C. to a temperature of about 20° C. over a period of approximately 30 minutes and is further reduced to from about 5° C. to about 10° C. and is maintained at said temperature for a holding period.
Claim 12
Dependent Claim
13 words
The method of claim 10 wherein the liquor is cooled with slow agitation.
Claim 13
Dependent Claim
56 words
The method of claim 1 wherein the whey of step (d) is further treated to recover protein therein by the steps of, (i) adjusting the pH of the whey to about 4.5 so as to form a curd precipitate, (ii) separating the curd precipitate formed in step (i), and (iii) preserving the curd of step (ii).
Claim 14
Dependent Claim
36 words
The method of claim 12 wherein the curd of step (iii) is preserved by the additional steps of, (i) washing said curd with water, (ii) separating the water from the curd, and (iii) drying the curd.
Claim 15
Dependent Claim
75 words
The method of claim 1 wherein the whey of step (d) is further treated to recover protein therein by the steps of, (i) heating the whey to a temperature of from about 32° C. to about 38° C., (ii) adjusting the pH of the whey to about 5.3 so as to form a curd precipitate and a second whey solution, (iii) separating the curd precipitate from the second whey solution, and (iv) preserving said curd.
Claim 16
Dependent Claim
46 words
The method of claim 14 wherein the curd of step (iv) is preserved by the additional steps of, (i) washing the curd with water, (ii) separating the water from the curd, (iii) adjusting the pH of the curd to about 6.5, and (iv) drying the curd.
Claim 17
Dependent Claim
72 words
The method of claim 14 wherein the second whey solution of step (iii) is further treated to recover protein therein by the steps of, (i) cooling the second whey solution to a temperature of from about 10° C. to about 16° C., (ii) adjusting the pH of the second whey solution to about 4.5 so as to form a curd precipitate, (iii) separating the curd precipitate, and (iv) preserving the curd precipitate.
Claim 18
Dependent Claim
16 words
The method of claim 16 where in the curd of step (iv) is preserved by freeze-drying.
Claim 19
Dependent Claim
44 words
The method of claim 16 wherein the curd of step (iv) is preserved by the additional steps of, (i) placing the curd in water, (ii) adjusting pH of the curd to about 6.8, and (iii) drying the curd by one of freeze-drying or spray-drying.
Claim 20
Dependent Claim
9 words
The product produced by the method of claim 5.
Claim 21
Dependent Claim
9 words
The product produced by the method of claim 13.
Claim 22
Dependent Claim
9 words
The product produced by the method of claim 15.
Claim 23
Dependent Claim
9 words
The product produced by the method of claim 18.
Claim 24
Independent Claim
205 words
A method for processing soy protein from defatted soybean flakes comprising, (a) mixing at least about five parts by weight of water with about one part by weight of flakes at a temperature of from about 55° C. to about 70° C. for from about 15 to about 50 minutes, the aqueous mixture having a pH of about 6.2 to about 6.8, and maintaining said mixture at said temperature for a time sufficient to solubilize a substantial portion of the protein and the flakes, (b) removing a substantial portion of any insolubles from the mixture of step (a) so as to provide a clarified liquor, (c) cooling the liquor of step (b) over a time of at least one to three hours to a temperature of from about 5° C. to about 10° C. resulting in curd and whey, (d) separating the curd from the whey, (e) mixing the curd with water and adjusting the pH of the resulting mixture to about 5.3 so as to form a curd precipitate, (f) washing the curd precipitate of step (e) with water and adjusting the pH of the washed curd precipitate to from about 6.3 to about 6.8, and (g) drying the curd precipitate of step (f).
Claim 25
Independent Claim
205 words
A method for processing soy protein from defatted soybean flakes comprising, (a) mixing at least about five parts by weight of water with about one part by weight of flakes at a temperature of from about 55° C. to about 70° C. for from about 15 to about 50 minutes, the aqueous mixture having a pH of about 6.2 to about 6.8, and maintaining said mixture at said temperature for a time sufficient to solubilize a substantial portion of the protein and the flakes, (b) removing a substantial portion of any insolubles from the mixture of step (a) so as to provide a clarified liquor, (c) cooling the liquor of step (b) over a time of at least one to three hours to a temperature of from about 5° C. to about 10° C. resulting in curd and whey, (d) separating the curd from the whey, (e) mixing the curd with water and adjusting the pH of the resulting mixture to about 5.3 so as to form a curd precipitate, (f) washing the curd precipitate of step (e) with water and adjusting the pH of the washed curd precipitate to from about 6.3 to about 6.8, and (g) drying the curd precipitate of step (f).
Claim 26
Dependent Claim
37 words
The method of claim 23 wherein in step (f), the pH of the washed curd precipitate is adjusted by the addition of a base selected from the group consisting of calcium hydroxide, potassium hydroxide or sodium hydroxide.
Claim 27
Dependent Claim
63 words
The method of claim 23 wherein in the cooling step of step (c), the temperature of the liquor is reduced from an elevated temperature of about 65° C. to a temperature of about 20° C. over a period of approximately 30 minutes and is then further reduced to from about 5° C. to about 10° C., the liquor being agitated slowly during cooling.
Claim 28
Dependent Claim
66 words
The method of claim 23 wherein the whey of step (d) is further treated to recover protein therein by the steps of, (i) adjusting the pH of the whey to about 4.5 so as to form a curd precipitate, (ii) separating the curd precipitate formed in step (i), (iii) washing said curd with water, (iv) separating the water from the curd, and (v) drying the curd.
Claim 29
Dependent Claim
103 words
The method of claim 23 wherein the whey of step (d) is further treated to recover protein thereby by the steps of, (i) heating the whey to a termperature of from about 32° C. to about 38° C., (ii) adjusting the pH of the whey to about 5.3 so as to form a curd precipitate and a second whey solution, (iii) separating the curd precipitate from the second whey solution, (iv) washing said curd precipitate with water, (v) separating the water from said curd precipitate, and (vi) adjusting the pH of the washed curd precipitate to about 6.5, and (vii) drying said curd.
Claim 30
Dependent Claim
95 words
The method of claim 27 wherein the second whey solution of step (ii) is further treated so as to recover protein therein by the steps of, (i) cooling the second whey solution to a temperature of from about 10° C. to about 16° C., (ii) adjusting the pH of the second whey solution to about 4.5 so as to form a curd precipitate, (iii) separating said curd precipitate, (iv) placing said curd precipitate in water and adjusting the pH thereof to from about 6.8, and (v) drying the curd by one of freeze-drying or spray-drying.
Claim 31
Dependent Claim
142 words
The method of claim 23 wherein the whey of step (d) is further treated to recover protein therein by the steps of, (i) heating the whey to a temperature of from about 32° C. to about 38° C., (ii) adjusting pH of the whey to about 5.3 so as to form a curd precipitate and a second whey solution, (iii) separating the curd precipitate from the second whey solution, (iv) washing said curd with water, (v) adjusting pH of the curd to about 6.5 and drying said curd, (vi) cooling the second whey solution of step (ii) to a temperature of from about 10° C. to about 16° C., (vii) adjusting the pH of the second whey solution to about 4.5 so as to form a curd precipitate, (viii) separating the curd precipitate of step (vii), and (ix) preserving said curd precipitate.
Claim 32
Dependent Claim
45 words
The method of claim 29 wherein the curd of step (ix) is preserved by the additional steps of, (i) placing the curd in water, (ii) adjusting pH of the curd to from about 6.8, and (iii) drying said curd by one of freeze-drying or spray-drying.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1982-10-29 | 1983-04-30 | 1983-10-30 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1986-10-29 | 1987-04-30 | 1987-10-30 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1990-10-29 | 1991-04-30 | 1991-10-30 | $7700.00 | Window Closed / Lapsed |