Patent US4168996A successfully refreshed from Google Patents.
← Back to Patent Explorer
US4168996A Expired / Lapsed US ⏱️ 0.0 years remaining

Soldering flux

Assignee: AT&T Inc
•
Filing: 1977-10-28
•
Granted: 1979-09-25
•
Expires: 1997-10-28
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract A soldering flux is disclosed. The soldering flux comprises a mixture comprising rosin, an activator having at least one halogen atom and at least one destabilizing substituent and an acid solder surfactant selected from a polybasic carboxylic acid, a hydroxyl substituent thereof, a keto acid and a mixture of any of the foregoing surfactants.

Inventors

  • 👤 Frank M. Zado

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-02 18:40
CPC Classifications
B; B23; B23K; B23K35/00; B23K35/22; B23K35/36; B23K35/3612; B23K35/3613

Claims Analysis

Total Claims: 39
Claim 1
Independent Claim 92 words
A solder flux which comprises: (a) rosin; (b) an activator having at least one halogen atom and at least one destabilizing substituent; and (c) a surfactant selected from the group consisting of (a") a polycarboxylic acid, (b") a hydroxyl substituent of (a"), (c") a keto acid and (d") a mixture of any of the foregoing surfactants wherein said activator is present in an amount of from 0.3 to 7 weight percent and said surfactant is present in an amount of at least one weight percent of the components (a), (b) and (c).
Claim 2
Dependent Claim 92 words
A solder flux which comprises: (a) rosin; (b) an activator having at least one halogen atom and at least one destabilizing substituent; and (c) a surfactant selected from the group consisting of (a") a polycarboxylic acid, (b") a hydroxyl substituent of (a"), (c") a keto acid and (d") a mixture of any of the foregoing surfactants wherein said activator is present in an amount of from 0.3 to 7 weight percent and said surfactant is present in an amount of at least one weight percent of the components (a), (b) and (c).
Claim 3
Dependent Claim 13 words
The flux as defined in claim 1 which further comprises a flux vehicle.
Claim 4
Dependent Claim 16 words
The flux as defined in claim 1 which further comprises a secondary activator comprising an organohydrohalide.
Claim 5
Dependent Claim 29 words
The flux as defined in claim 1 which further comprises a foaming expedient selected from the group of expedients consisting of a surface active agent and a stabilizer solvent.
Claim 6
Dependent Claim 16 words
The flux as defined in claim 1 wherein said activator comprises a halogen substituted carboxylic acid.
Claim 7
Dependent Claim 41 words
The flux as defined in claim 1 wherein said surfactant comprises a polycarboxylic acid selected from the group consisting of dicarboxylic acid having at least 4 carbon atoms, a tricarboxylic acid having 6 to 7 carbon atoms and a mixture thereof.
Claim 8
Dependent Claim 16 words
The flux as defined in claim 1 which comprises rosin, a dibromosuccinic acid and adipic acid.
Claim 9
Dependent Claim 12 words
The flux as defined in claim 7 which further comprises levulinic acid.
Claim 10
Dependent Claim 16 words
The flux as defined in claim 1 which comprises rosin, azelaic acid and a dibromostyrene activator.
Claim 11
Dependent Claim 16 words
The flux as defined in claim 9 which further comprises a secondary activator comprising diethylamine hydrochloride.
Claim 12
Dependent Claim 55 words
The flux as defined in claim 1 wherein said rosin is present in an amount ranging from about 50 to about 96 weight percent, said activator is present in an amount ranging from about 0.3 to about 7 weight percent and said surfactant is present in a remainder amount of at least one weight percent.
Claim 13
Dependent Claim 37 words
The flux as defined in claim 11 wherein said rosin, said activator and said surfactant are dissolved in a solvent vehicle in an amount ranging from about 9.7 to about 80 weight percent of the resultant solution.
Claim 14
Dependent Claim 135 words
A soldering flux comprising: a rosin mixture which comprises (a) rosin; (b) an activator comprising an organic acid selected from the group consisting of a monocarboxylic acid having at least 12 carbon atoms, a dicarboxylic acid having at least 4 carbon atoms and a mixture thereof, said organic acid having at least one halogen atom; and (c) a surfactant comprising an organic acid selected from the group consisting of (a') a dicarboxylic acid having at least 4 carbon atoms, (b') a hydroxyl substituent of (a'), (c') a keto acid and (d') a mixture of any of the foregoing acids wherein said activator is present in an amount of from 0.3 to 7 weight percent and said surfactant is present in an amount of at least one weight percent of the components (a), (b) and (c).
Claim 15
Dependent Claim 135 words
A soldering flux comprising: a rosin mixture which comprises (a) rosin; (b) an activator comprising an organic acid selected from the group consisting of a monocarboxylic acid having at least 12 carbon atoms, a dicarboxylic acid having at least 4 carbon atoms and a mixture thereof, said organic acid having at least one halogen atom; and (c) a surfactant comprising an organic acid selected from the group consisting of (a') a dicarboxylic acid having at least 4 carbon atoms, (b') a hydroxyl substituent of (a'), (c') a keto acid and (d') a mixture of any of the foregoing acids wherein said activator is present in an amount of from 0.3 to 7 weight percent and said surfactant is present in an amount of at least one weight percent of the components (a), (b) and (c).
Claim 16
Dependent Claim 12 words
The flux as defined in claim 13 which further comprises a vehicle.
Claim 17
Dependent Claim 36 words
The flux as defined in claim 14 wherein said vehicle comprises a solvent selected from the group consisting of an aliphatic alcohol, an alkanolamine, a chlorinated hydrocarbon and a mixture of any of the foregoing solvents.
Claim 18
Dependent Claim 13 words
The flux as defined in claim 15 which further comprises a foaming expedient.
Claim 19
Dependent Claim 16 words
The flux as defined in claim 13 which further comprises a secondary activator comprising an organohydrohalide.
Claim 20
Dependent Claim 18 words
The flux as defined in claim 13 wherein said monocarboxylic acid activator comprises 12 to 18 carbon atoms.
Claim 21
Dependent Claim 28 words
The flux as defined in claim 13 wherein said dicarboxylic acid activator, said dicarboxylic acid surfactant and said hydroxyl substituent thereof each comprise 4 to 10 carbon atoms.
Claim 22
Dependent Claim 16 words
The flux as defined in claim 13 which comprises rosin, a dibromosuccinic acid and adipic acid.
Claim 23
Dependent Claim 12 words
The flux as defined in claim 20 which further comprises levulinic acid.
Claim 24
Dependent Claim 59 words
The flux as defined in claim 13 wherein, in said rosin mixture, said rosin is present in an amount ranging from about 50 to about 96 weight percent, said activator is present in an amount ranging from about 0.3 to about 7 weight percent and said surfactant is present in a remainder amount of at least one weight percent.
Claim 25
Dependent Claim 39 words
The flux as defined in claim 22 which further comprises a secondary activator comprising an organohydrohalide combined with said rosin mixture in an amount ranging from 0.17 to about 0.28 weight percent of the total weight of combined components.
Claim 26
Dependent Claim 36 words
The flux as defined in claim 22 which further comprises a solvent vehicle in which said rosin mixture is dissolved in an amount ranging from about 9.7 to about 80 weight percent of the resultant flux.
Claim 27
Dependent Claim 13 words
The flux as defined in claim 24 which further comprises a foaming expedient.
Claim 28
Dependent Claim 123 words
A soldering composition comprising: a rosin mixture which comprises (a) rosin; (b) an activator having at least one halogen atom and at least one destabilizing substituent selected from the group consisting of (a') the carboxyl group, (b') the aryl group, (c') the carbonyl group and (d') the halogen atom; (c) a surfactant selected from the group consisting of (a") a polycarboxylic acid, (b") a hydroxyl substituent of (a"), (c") a keto acid and (d") a mixture of any of the foregoing surfactants wherein said activator is present in an amount of from 0.3 to 7 weight percent and said surfactant is present in an amount of at least one weight percent of the components (a), (b) and (c); and a metal solder alloy.
Claim 29
Dependent Claim 123 words
A soldering composition comprising: a rosin mixture which comprises (a) rosin; (b) an activator having at least one halogen atom and at least one destabilizing substituent selected from the group consisting of (a') the carboxyl group, (b') the aryl group, (c') the carbonyl group and (d') the halogen atom; (c) a surfactant selected from the group consisting of (a") a polycarboxylic acid, (b") a hydroxyl substituent of (a"), (c") a keto acid and (d") a mixture of any of the foregoing surfactants wherein said activator is present in an amount of from 0.3 to 7 weight percent and said surfactant is present in an amount of at least one weight percent of the components (a), (b) and (c); and a metal solder alloy.
Claim 30
Dependent Claim 17 words
The soldering composition as defined in claim 26 which further comprises a secondary activator comprising an organohydrohalide.
Claim 31
Dependent Claim 13 words
The soldering composition as defined in claim 26 which further comprises a vehicle.
Claim 32
Dependent Claim 29 words
The composition as defined in claim 26 wherein said activator comprises a halogen substituted carboxylic acid selected from the group consisting of a monobasic acid and a polybasic acid.
Claim 33
Dependent Claim 41 words
The composition as defined in claim 29 wherein said surfactant comprises a polycarboxylic acid selected from the group consisting of a dicarboxylic acid having 4 to 10 carbon atoms, a tricarboxylic acid having 6 to 7 atoms and a mixture thereof.
Claim 34
Dependent Claim 44 words
The composition as defined in claim 30 wherein said activator comprises a halogen substituted carboxylic acid selected from the group consisting of a monocarboxylic acid having 12 to 18 carbon atoms, a dicarboxylic acid having 4 to 10 carbon atoms and a mixture thereof.
Claim 35
Dependent Claim 19 words
The composition as defined in claim 26 wherein said rosin mixture comprises rosin, a dibromosuccinic acid and adipic acid.
Claim 36
Dependent Claim 12 words
The composition as defined in claim 32 which further comprises levulinic acid.
Claim 37
Dependent Claim 27 words
The composition as defined in claim 26 wherein said rosin mixture comprises rosin, azelaic acid, and a dibromostyrene activator combined with a secondary activator comprising diethylamine hydrochloride.
Claim 38
Dependent Claim 53 words
The composition as defined in claim 26 wherein, in said rosin mixture, said activator is present in an amount ranging from about 0.3 to about 7 weight percent, said surfactant is present in an amount ranging from about 1 to about 49.7 weight percent and said rosin is present in a remainder amount.
Claim 39
Dependent Claim 41 words
The composition as defined in claim 35 wherein said rosin mixture is combined with a secondary activator comprising an organohydrohalide which is present in an amount of 0.17 to about 0.28 weight percent of the total weight of the combined components.

References Cited (Backward Citations)

US3577284A Cited
US3734791A Cited
US3837932A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1982-09-24 1983-03-26 1983-09-25 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1986-09-24 1987-03-26 1987-09-25 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1990-09-24 1991-03-26 1991-09-25 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag