Patent US4168171A successfully refreshed from Google Patents.
US4168171A
Expired / Lapsed
US
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Light-sensitive thermal developable diazotype sheets with imidazoles
Assignee: 3M Co
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Filing: 1977-08-05
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Granted: 1979-09-18
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Expires: 1997-08-05
Abstract
Abstract A heat-developable diazotype sheet containing an acid-stabilized diazonium salt in one layer thereof and an acid-neutralizing component in another layer thereof is shown wherein at least 25% by weight of the acid-neutralizer component comprises imidazole derivatives of a specific formula.
Inventors
- 👤 John M. Winslow
- 👤 Gary E. LaBelle
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-02 21:11
CPC Classifications
G; G03; G03C; G03C1/00; G03C1/52; G03C1/60
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
158 words
A heat reactive diazotype sheet having a supporting substrate having at least two layers thereon, one of said layers comprising a heat-softenable binder material and an acid-stabilized light sensitive diazonium salt capable of reacting with an azo-coupler compound to form a dye, and the other of said layers comprising a heat-softenable binder material and an acid-neutralizer component capable of providing basic equivalents in an amount at least sufficient to neutralize said acid stabilization of said diazonium salt so as to provide a weakly basic environment for the diazonium salt in the sheet and to render said acid-stabilized diazonium salt reactive with said azo-coupler compound, and at least one of said layers containing an azo-coupler, said diazotype sheet being characterized by said acid-neutralizer component being comprised of at least 25% by weight imidazole acid-neutralizer compound is selected from the group consisting of 2-isopropyl imidazole, 2-phenyl imidazole, 2-benzyl imidazole, 4-phenyl imidazole, 4-methyl imidazole, 2,4-dimethyl imidazole, 2-phenyl-4-methyl imidazole, and 2,4,5-trimethyl imidazole.
Claim 2
Dependent Claim
158 words
A heat reactive diazotype sheet having a supporting substrate having at least two layers thereon, one of said layers comprising a heat-softenable binder material and an acid-stabilized light sensitive diazonium salt capable of reacting with an azo-coupler compound to form a dye, and the other of said layers comprising a heat-softenable binder material and an acid-neutralizer component capable of providing basic equivalents in an amount at least sufficient to neutralize said acid stabilization of said diazonium salt so as to provide a weakly basic environment for the diazonium salt in the sheet and to render said acid-stabilized diazonium salt reactive with said azo-coupler compound, and at least one of said layers containing an azo-coupler, said diazotype sheet being characterized by said acid-neutralizer component being comprised of at least 25% by weight imidazole acid-neutralizer compound is selected from the group consisting of 2-isopropyl imidazole, 2-phenyl imidazole, 2-benzyl imidazole, 4-phenyl imidazole, 4-methyl imidazole, 2,4-dimethyl imidazole, 2-phenyl-4-methyl imidazole, and 2,4,5-trimethyl imidazole.
Claim 3
Dependent Claim
24 words
The heat reactive diazotype sheet of claim 1 wherein at least 50% by weight of said acid neutralizer component is an imidazole acid-neutralizer compound.
Claim 4
Dependent Claim
24 words
The heat reactive diazotype sheet of claim 1 wherein at least 75% by weight of said acid neutralizer component is an imidazole acid-neutralizer compound.
Claim 5
Dependent Claim
27 words
The heat reactive diazotype sheet of claim 1 wherein said imidazole acid-neutralizer component is selected from the group consisting of 2-isopropyl imidazole, 2-phenyl imidazole, and 2-benzyl imidazole.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1982-09-17 | 1983-03-19 | 1983-09-18 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1986-09-17 | 1987-03-19 | 1987-09-18 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1990-09-17 | 1991-03-19 | 1991-09-18 | $7700.00 | Window Closed / Lapsed |