Patent US4159357A successfully refreshed from Google Patents.
US4159357A
Expired / Lapsed
US
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Process for surface treating parts made of ceramic material
Assignee: MTU Aero Engines AG
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Filing: 1977-10-03
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Granted: 1979-06-26
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Expires: 1997-10-03
Abstract
Abstract A process for surface treating ceramic parts so as to increase their resistance to oxidation when exposed to high temperatures. The process includes applying a metal coating to the ceramic part, and thereafter heating the part to form a glass surface layer with the metal oxide built into the lattice of the glass layer. The metals employed may be aluminum, magnesium, titanium, lead, zinc, cadmium, or rare-earth elements. The heat treatment is performed in more than one stage.
Inventors
- 👤 Richard Grunke
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-30 23:30
CPC Classifications
C; C04; C04B; C04B41/00; C04B41/45; C04B41/50; C04B41/5022; F; F01; F01D; F01D5/00; F01D5/12; F01D5/28; F01D5/284; F01D5/288
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
169 words
A process for surface treating parts made of silicon-base ceramic material so as to increase the resistance of such parts to oxidation when they are exposed to high temperatures, the process comprising the steps of: (a) applying a single layer metal coating to the surface of a silicon-base ceramic part, the metal being one whose oxide can be built into the lattice of Si O 2 , and (b) thereafter subjecting the ceramic part to a two-stage heat treatment, (I) the first stage of the heat treatment comprising heating the coated ceramic part at a temperature just below the melting point of the coating metal for at least about two hours so as to oxidize the metal, and (II) the second stage of the heat treatment comprising heating the part at a temperature of about 1300° C. for at least about one day, so as to form an Si O 2 glass surface layer on the part with a metal oxide built into the lattice of the glass layer.
Claim 2
Dependent Claim
169 words
A process for surface treating parts made of silicon-base ceramic material so as to increase the resistance of such parts to oxidation when they are exposed to high temperatures, the process comprising the steps of: (a) applying a single layer metal coating to the surface of a silicon-base ceramic part, the metal being one whose oxide can be built into the lattice of Si O 2 , and (b) thereafter subjecting the ceramic part to a two-stage heat treatment, (I) the first stage of the heat treatment comprising heating the coated ceramic part at a temperature just below the melting point of the coating metal for at least about two hours so as to oxidize the metal, and (II) the second stage of the heat treatment comprising heating the part at a temperature of about 1300° C. for at least about one day, so as to form an Si O 2 glass surface layer on the part with a metal oxide built into the lattice of the glass layer.
Claim 3
Dependent Claim
20 words
A process as defined in claim 1 wherein the metal coating is applied to the ceramic part by vapor deposition.
Claim 4
Dependent Claim
16 words
A process as defined in claim 2 wherein the vapor deposition is performed in a vacuum.
Claim 5
Dependent Claim
27 words
A process as defined in claim 1 wherein the first stage of heat treatment is performed at a temperature lower than the temperature of the second stage.
Claim 6
Dependent Claim
27 words
A process as defined in claim 1 wherein the metal used to coat the ceramic part is selected from the group consisting of aluminum, magnesium, and titanium.
Claim 7
Dependent Claim
32 words
A process as defined in claim 1 wherein the metal used to coat the ceramic part is selected from the group consisting of aluminum, magnesium, titanium, lead, zinc, cadmium, and rare-earth elements.
References Cited (Backward Citations)
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1982-06-25 | 1982-12-25 | 1983-06-26 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1986-06-25 | 1986-12-25 | 1987-06-26 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1990-06-25 | 1990-12-25 | 1991-06-26 | $7700.00 | Window Closed / Lapsed |