Patent US4155755A successfully refreshed from Google Patents.
US4155755A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Oxidation resistant porous abradable seal member for high temperature service
Assignee: Graftech International Holdings Inc
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Filing: 1978-07-07
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Granted: 1979-05-22
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Expires: 1998-07-07
Abstract
Abstract Porous abradable sintered metal structures suitable for use as abradable seals are rendered oxidation resistant and thus suitable for high temperature service by introducing into the porous structure an intermetallic compound of aluminum with one of chromium, titanium, cobalt and nickel, which compound is then thermally reacted with the porous metal structures to form an aluminum alloy in the structure.
Inventors
- 👤 Raymond V. Sara
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-03 13:16
CPC Classifications
B; B22; B22F; B22F3/00; B22F3/10; B22F3/11; B22F3/114; B22F3/1143; C; C22; C22C; C22C1/00; C22C1/08; B22F2998/00; B22F2998/10
Claims Analysis
Total Claims: 16
Claim 1
Independent Claim
191 words
Method of rendering a porous, abradable, sintered metal structure comprising a base alloy of chromium with nickel or cobalt sufficiently oxidation resistant to be used at temperatures up to about 1050° C. without substantial loss of strength, porosity or abradability which comprises immersing said porous sintered metal structure briefly in a suspension in an anhydrous organic fluid of at least one powdered intermetallic compound of aluminum and an element selected from the group consisting of chromium, titanium, cobalt and nickel, the particles of said intermetallic compound powder being substantially smaller than the average pore size of said porous sintered metal structure, drying said porous sintered metal after removal from said slurry, repeating said steps of immersion and drying as often as necessary until the desired weight percent of intermetallic compound has been added to said porous sintered metal structure and then heating said porous sintered metal structure at a sufficiently elevated temperature and for a sufficient time to form a structural alloy of aluminum and chromium with at least one metal selected from the group consisting of nickel, cobalt and titanium, which structure alloy is substantially all beta and gamma phases.
Claim 2
Dependent Claim
191 words
Method of rendering a porous, abradable, sintered metal structure comprising a base alloy of chromium with nickel or cobalt sufficiently oxidation resistant to be used at temperatures up to about 1050° C. without substantial loss of strength, porosity or abradability which comprises immersing said porous sintered metal structure briefly in a suspension in an anhydrous organic fluid of at least one powdered intermetallic compound of aluminum and an element selected from the group consisting of chromium, titanium, cobalt and nickel, the particles of said intermetallic compound powder being substantially smaller than the average pore size of said porous sintered metal structure, drying said porous sintered metal after removal from said slurry, repeating said steps of immersion and drying as often as necessary until the desired weight percent of intermetallic compound has been added to said porous sintered metal structure and then heating said porous sintered metal structure at a sufficiently elevated temperature and for a sufficient time to form a structural alloy of aluminum and chromium with at least one metal selected from the group consisting of nickel, cobalt and titanium, which structure alloy is substantially all beta and gamma phases.
Claim 3
Dependent Claim
14 words
A method according to claim 1 wherein said anhydrous organic fluid is isopropyl alcohol.
Claim 4
Dependent Claim
49 words
A method according to claim 1 wherein said steps of immersion and drying are repeated until said dried porous sintered metal structure has had introduced into it said intermetallic compound in a quantity equal to at least 7 weight percent of said porous sintered metal structure before said introduction.
Claim 5
Dependent Claim
48 words
A method according to claim 1 wherein said steps of immersion and drying are repeated until the dried porous sintered metal structure has had introduced into it said intermetallic compound in a quantity equal to about 14 weight percent of said porous sintered metal structure before said introduction.
Claim 6
Dependent Claim
14 words
A method according to claim 1 wherein said base alloy comprises nickel and chromium.
Claim 7
Dependent Claim
14 words
A method according to claim 1 wherein said base alloy comprises cobalt and chromium.
Claim 8
Dependent Claim
15 words
A method according to claim 1 wherein said intermetallic compound is an aluminum chromium compound.
Claim 9
Dependent Claim
15 words
A method according to claim 1 wherein said intermetallic compound is an aluminum titanium compound.
Claim 10
Dependent Claim
15 words
A method according to claim 1 wherein said intermetallic compound is an aluminum cobalt compound.
Claim 11
Dependent Claim
15 words
A method according to claim 1 wherein said intermetallic compound is an aluminum nickel compound.
Claim 12
Dependent Claim
76 words
A method according to claim 1 wherein said intermetallic compound is at least one selected from the group consisting of Al 7 Cr, Al 11 Cr 2 , Al 4 Cr, Al 3 Cr, Al 9 Cr 4 , Al 8 Cr 5 , AlCr 2 , Al 3 Ti, AlTi, Al 9 Co 2 , Al 13 Co 4 , Al 5 Co 2 , AlCo, Al 3 Ni, Al 3 Ni 2 and AlNi.
Claim 13
Dependent Claim
24 words
A method according to claim 1 wherein said heating of said porous sintered metal structure is at a temperature of at least 1050° C.
Claim 14
Dependent Claim
23 words
A method according to claim 1 wherein said heating of said porous sintered metal structure is at a temperature of about 1150° C.
Claim 15
Dependent Claim
24 words
A method according to claim 1 wherein said heating of said porous sintered metal structure is for a period of at least 15 minutes.
Claim 16
Dependent Claim
23 words
A method according to claim 1 wherein said heating of said porous sintered metal structure is for a period of about 2 hours.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1982-05-21 | 1982-11-20 | 1983-05-22 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1986-05-21 | 1986-11-20 | 1987-05-22 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1990-05-21 | 1990-11-20 | 1991-05-22 | $7700.00 | Window Closed / Lapsed |