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US4154869A Expired / Lapsed US ⏱️ 0.0 years remaining

Electroless plating method with inspection for an unbroken layer of water prior to plating

Assignee: Aura Systems Inc
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Filing: 1977-12-30
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Granted: 1979-05-15
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Expires: 1997-12-30
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Abstract

Abstract Improvements are disclosed in the method of electroless deposition of a metal on a nonconductive surface wherein the surface is sequentially contacted with a tin salt solution, a palladium salt solution, and an electroless plating bath containing said metal. The improvement relates to preparing the surface to produce an unbroken layer of water adhering thereto upon dipping said surface in deionized water. The improvement further contemplates removing the surface from the electroless plating bath after formation of the visible amount of metal, inspecting the surface for imperfections, removing the metal, and recleaning the surface to remove imperfections. Finally, the activation steps are repeated followed by contacting the surface with an electroless plating bath to plate the desired quantity of metal thereon in a manner wherein uniformity and adhesion are improved.

Inventors

  • 👤 Victor Luft

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 07:09
CPC Classifications
C; C23; C23C; C23C18/00; C23C18/16; C23C18/18; C23C18/20; C23C18/28; H; H05; H05K; H05K3/00; H05K3/10; H05K3/18; H05K3/181

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 91 words
A method of plating metal on nonconductive surfaces, comprising the steps of: a. Cleaning a nonconductive surface to remove impurities; b. Contacting said cleaned surface with a tin salt to sensitize said surface, followed by contacting said sensitized surface with a palladium salt to catalyze said surface; c. Rinsing said surface in deionized water to inspect for an unbroken layer of water adhering to said surface, and repeating step b. above until said unbroken layer of water is found; and d. Electrolessly plating said surface with a desired amount of metal.
Claim 2
Independent Claim 91 words
A method of plating metal on nonconductive surfaces, comprising the steps of: a. Cleaning a nonconductive surface to remove impurities; b. Contacting said cleaned surface with a tin salt to sensitize said surface, followed by contacting said sensitized surface with a palladium salt to catalyze said surface; c. Rinsing said surface in deionized water to inspect for an unbroken layer of water adhering to said surface, and repeating step b. above until said unbroken layer of water is found; and d. Electrolessly plating said surface with a desired amount of metal.
Claim 3
Dependent Claim 134 words
The method of claim 1, which further includes the steps of: a. Cleaning a nonconductive surface to remove impurities; b. Contacting said cleaned surface with a tin salt to sensitize said surface, followed by contacting said sensitized surface with a palladium salt to catalyze said surface; c. Rinsing said surface in deionized water to inspect for an unbroken layer of water adhering to said surface, and repeating step b. above until said unbroken layer of water is found; d. Electrolessly plating said surface with said metal for sufficient time to plate a visible amount of metal thereon; e. Inspecting said surface for plating imperfections, removing said plating, and recleaning said areas of imperfections; f. Repeating said steps in b. and c. above; and g. Electrolessly plating said surface with a desired amount of metal.
Claim 4
Dependent Claim 18 words
The method of claim 1, wherein said deionized water has a resistivity of at least one megohm centimeter.
Claim 5
Dependent Claim 12 words
The method of claim 1, wherein said tin salt is stannous chloride.
Claim 6
Dependent Claim 12 words
The method of claim 1, wherein said palladium salt is palladium chloride.

References Cited (Backward Citations)

US3442683A Cited
US3639143A Cited
US3798050A Cited
US4072772A Cited
US4002779A Cited
JPS5149130A Cited
US4042730A Cited
US4066809A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1982-05-14 1982-11-13 1983-05-15 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1986-05-14 1986-11-13 1987-05-15 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1990-05-14 1990-11-13 1991-05-15 $7700.00 Window Closed / Lapsed

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