← Back to Patent Explorer
US3798050A Expired / Lapsed US ⏱️ 0.0 years remaining

Catalytic sensitization of substrates for metallization

Assignee: PPG Industries Inc
•
Filing: 1971-05-28
•
Granted: 1974-03-19
•
Expires: 1991-05-28
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract Metal films of improved uniformity are formed on substrates having their surfaces sensitized by the deposition of palladium on tin by buffering the palladium salt solution in contact with the glass at a pH from 6 to 9. Buffering is preferably accomplished by contacting the substrate with an aqueous buffering solution and an acidic palladium salt solution.

Inventors

  • 👤 H Franz
  • 👤 R Crissman

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 22:36
CPC Classifications
C; C23; C23C; C23C18/00; C23C18/16; C23C18/18; C23C18/20; C23C18/28; C23C18/30

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 127 words
In the method of coating a non-conductive substrate surface with a metal-containing deposit comprising the steps of: first, contacting the substrate with a solution of tin salt and then rinsing the same; second, contacting the substrate with a solution of palladium salt and thereafter contacting the substrate with a solution containing the desired metal to be deposited and reducing agent for such metal, whereby a non-uniform metal-containing deposit is formed, the improvement comprising the steps of: rinsing the tin salt contacted substrate with a rinse of water containing an alkaline buffering compound in an effective amount to provide a pH of about 7 to about 9 in the mixture of palladium salt solution and remaining rinse in contact with the substrate whereby a uniform metal-containing deposit results.
Claim 2
Dependent Claim 14 words
The method of claim 2 wherein the contacting solutions are sprayed against the substrate.
Claim 3
Dependent Claim 36 words
The method of claim 2 wherein the alkaline buffer is selected from the group consisting of ammonium hydroxide, ammonium borate and water-soluble ammonium, alkali metal and alkaline earth metal carbonates, bicarbonates and phosphates and mixtures thereof.
Claim 4
Dependent Claim 28 words
The method of claim 4 wherein the rinse contains as an esential ingredient from about 0.01 to about 7 percent by weight of the aqueous rinse, sodium bicarbonate.

References Cited (Backward Citations)

US3266929A Cited
US3403035A Cited
US3296012A Cited
US3438798A Cited
US3370974A Cited
US3418143A Cited
US3672939A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-03-18 1977-09-17 1978-03-19 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-03-18 1981-09-17 1982-03-19 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-03-18 1985-09-17 1986-03-19 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag