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US4151325A Expired / Lapsed US ⏱️ 0.0 years remaining

Titanium nitride thin films for minimizing multipactoring

Assignee: United States Department of Energy
•
Filing: 1976-10-22
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Granted: 1979-04-24
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Expires: 1996-10-22
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Abstract

Abstract Applying a thin film coating to the surface of a workpiece, in particular, applying a coating of titanium nitride to a klystron window by means of a crossed-field diode sputtering array. The array is comprised of a cohesive group of numerous small hollow electrically conducting cylinders and is mounted so that the open ends of the cylinders on one side of the group are adjacent a titanium cathode plate. The workpiece is mounted so as to face the open ends of the other side of the group. A magnetic field is applied to the array so as to be coaxial with the cylinders and a potential is applied across the cylinders and the cathode plate, the cylinders as an anode being positive with respect to the cathode plate. The cylinders, the cathode plate and the workpiece are situated in an atmosphere of nitrogen which becomes ionized such as by field emission because of the electric field between the cylinders and cathode plate, thereby establishing an anode-cathode discharge that results in sputtering of the titanium plate. The sputtered titanium coats the workpiece and chemically combines with the nitrogen to form a titanium nitride coating on the workpiece. Gas pressure, gas mixtures, cathode material composition, voltages applied to the cathode and anode, the magnetic field, cathode, anode and workpiece spacing, and the aspect ratio (ratio of length to inner diameter) of the anode cylinders, all may be controlled to provide consistent optimum thin film coatings of various compositions and thicknesses. Another facet of the disclosure is the coating of microwave components per se with titanium nitride to reduce multipactoring under operating conditions of the components.

Inventors

  • 👤 Kimo M. Welch

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 18:15
CPC Classifications
C; C23; C23C; C23C14/00; C23C14/22; C23C14/34; C23C14/35; H; H01; H01J; H01J37/00; H01J37/32; H01J37/34; H01J9/00; H01J9/20; Y; Y10; Y10S; Y10S505/00; Y10S505/80; Y10S505/815; Y10S505/816; Y10S505/825; Y10S505/866

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 24 words
A microwave circuit component having a thin film coating of titanium nitride on the surface thereof to reduce multipactoring in operation of the component.
Claim 2
Dependent Claim 24 words
A microwave circuit component having a thin film coating of titanium nitride on the surface thereof to reduce multipactoring in operation of the component.
Claim 3
Dependent Claim 14 words
The microwave circuit component of claim 1 wherein the component is a klystron window.
Claim 4
Dependent Claim 20 words
The microwave circuit component of claim 1, wherein said coating is of a thickness ranging down to one molecular layer.
Claim 5
Dependent Claim 14 words
The microwave circuit component of claim 1, wherein said coating is a sputtered coating.

References Cited (Backward Citations)

GB773702A Cited
US3309302A Cited
US3891884A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1982-04-23 1982-10-23 1983-04-24 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1986-04-23 1986-10-23 1987-04-24 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1990-04-23 1990-10-23 1991-04-24 $7700.00 Window Closed / Lapsed

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