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US4148129A
Expired / Lapsed
US
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Aluminum-stabilized multifilamentary superconductor and method of its manufacture
Assignee: Airco Inc
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Filing: 1976-11-01
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Granted: 1979-04-10
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Expires: 1996-11-01
Abstract
Abstract A multifilamentary superconductor having a large number fo NbTi filaments in an aluminum alloy matrix which is stabilized by a high-purity aluminum sheath is disclosed, together with the method of its manufacture. An Al alloy billet having a number of NbTi rods disposed therein is extruded. A superpure Al sheath is added; this product is then enclosed in copper and wiredrawn after which the copper is etched off.
Inventors
- 👤 Morris S. Young
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 10:50
CPC Classifications
H; H10; H10N; H10N60/00; H10N60/20; H10N60/01; H10N60/0156; Y; Y10; Y10S; Y10S505/00; Y10S505/825; Y10S505/876; Y10S505/877; Y10S505/917; Y10S505/918; Y10S505/928; Y10S505/929; Y10S505/93; Y10T; Y10T29/00; Y10T29/49; Y10T29/49002; Y10T29/49014
Claims Analysis
Total Claims: 14
Claim 1
Independent Claim
142 words
A method for manufacturing an aluminum-stabilized multifilamentary superconductor, which comprises: (a) preparing a cylindrical billet of aluminum alloy having a plurality of holes spaced apart from one another in an essentially circular and symmetric array extending therethrough parallel to the axis of the cylinder; (b) inserting rods of superconductive material into said holes; (c) extruding said billet such that it is elongated in the direction of its axis; (d) enclosing said extruded billet in a tube consisting essentially of aluminum not less than 99.999% pure; (e) further enclosing said enclosed extruded billet in a metallic sheath of a metal substantially harder than the aluminum of the tube; (f) working the assembly thus produced to a desired final cross sectional size not more than half its size prior to said working; and (g) removing the metallic sheath from the outside of the assembly.
Claim 2
Independent Claim
142 words
A method for manufacturing an aluminum-stabilized multifilamentary superconductor, which comprises: (a) preparing a cylindrical billet of aluminum alloy having a plurality of holes spaced apart from one another in an essentially circular and symmetric array extending therethrough parallel to the axis of the cylinder; (b) inserting rods of superconductive material into said holes; (c) extruding said billet such that it is elongated in the direction of its axis; (d) enclosing said extruded billet in a tube consisting essentially of aluminum not less than 99.999% pure; (e) further enclosing said enclosed extruded billet in a metallic sheath of a metal substantially harder than the aluminum of the tube; (f) working the assembly thus produced to a desired final cross sectional size not more than half its size prior to said working; and (g) removing the metallic sheath from the outside of the assembly.
Claim 3
Dependent Claim
20 words
The method of claim 1 wherein the assembly has been heat treated at an intermediate stage of the drawing process.
Claim 4
Dependent Claim
20 words
The method of claim 2 wherein the heat treatment is at approximately 350° C. for between 24 and 72 hours.
Claim 5
Dependent Claim
13 words
The method of claim 1 in which the metallic sheath is of copper.
Claim 6
Dependent Claim
16 words
The method of claim 4 in which the copper is removed by etching with nitric acid.
Claim 7
Dependent Claim
23 words
The method of claim 1 wherein there are 55 holes in the billet prior to the insertion of the rods of superconducting material.
Claim 8
Dependent Claim
16 words
The method of claim 1 wherein the superconductive material is an alloy of niobium and titanium.
Claim 9
Dependent Claim
17 words
The method of claim 1 wherein the assembly is heat treated after the drawing operation is completed.
Claim 10
Dependent Claim
18 words
The method of claim 8 wherein the heat treatment is at roughly 340° C. for approximately 60 hours.
Claim 11
Dependent Claim
16 words
The method of claim 8 wherein the copper sheath has been removed prior to heat treatment.
Claim 12
Dependent Claim
31 words
The method of claim 8 wherein said heat treatment is preceded by a warmup extended over approximately eight hours to approximately 280° C., which temperature is held for approximately one hour.
Claim 13
Independent Claim
132 words
A method for making a multifilamentary superconductor, stabilized with aluminum not less than 99.999% pure, comprising the steps of: preparing and extruding an aluminum alloy billet having a number of rods of superconductive alloy disposed therein in a symmetric and essentially circular pattern such that the rods are not in contact with one another to an intermediate size; enclosing the extruded billet in a tube of aluminum not less than 99.999% pure, and in a further metallic tube of a metal harder than the aluminum of said tube; working this assembly by wire drawing to a final size such that its diameter is at least halved; removing the further metallic tube; and heat-treating the product at a temperature of between 300° and 400° C. for a time between 24 and 72 hours.
Claim 14
Independent Claim
132 words
A method for making a multifilamentary superconductor, stabilized with aluminum not less than 99.999% pure, comprising the steps of: preparing and extruding an aluminum alloy billet having a number of rods of superconductive alloy disposed therein in a symmetric and essentially circular pattern such that the rods are not in contact with one another to an intermediate size; enclosing the extruded billet in a tube of aluminum not less than 99.999% pure, and in a further metallic tube of a metal harder than the aluminum of said tube; working this assembly by wire drawing to a final size such that its diameter is at least halved; removing the further metallic tube; and heat-treating the product at a temperature of between 300° and 400° C. for a time between 24 and 72 hours.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1982-04-09 | 1982-10-09 | 1983-04-10 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1986-04-09 | 1986-10-09 | 1987-04-10 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1990-04-09 | 1990-10-09 | 1991-04-10 | $7700.00 | Window Closed / Lapsed |