Patent US3206448A successfully refreshed from Google Patents.
Patent US4145187A successfully refreshed from Google Patents.
US4145187A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Treatment of material with hydrogen chloride
Assignee: Matthey Rustenburg Refiners Pty Ltd
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Filing: 1976-12-02
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Granted: 1979-03-20
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Expires: 1996-12-02
Abstract
Abstract This invention relates to apparatus for refining platinum group metal concentrates and the separation therefrom of silver and of the majority of base metals which are present with them. In more detail, the apparatus comprises means for reacting together gaseous hydrogen and chlorine so as to produce a flame and means for passing into the reaction zone of the said flame the said mineral concentrate in finely divided particulate form.
Inventors
- 👤 Raymond E. Oliver
- 👤 George McGuire
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 19:39
CPC Classifications
C; C22; C22B; C22B11/00; C22B11/02; B; B01; B01D; B01D47/00; B01D47/06; C22B1/00; C22B1/02; C22B1/08
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
186 words
Apparatus for separating base metal and silver from precious metal components in a mineral concentrate containing the same which comprises: (a) a tubular member made of heat resistant material and forming a reaction zone, (b) a tubular assembly including at least one tube having an end opening into said reaction zone and means for passing hydrogen and chlorine through said assembly to said end to form a hydrogen-chlorine flame at said end extending into said reaction zone, (c) a supply of mineral concentrate in particulate form and means communicating with said supply and including a venturi intermediate the ends of said tube for inducting said concentrate in particulate form into said tube and for feeding the thus inducted concentrate through said tube to the end thereof and then into said flame, (d) heat insulation means for maintaining said reaction zone at a temperature between 900° C. and 2500° C., (e) means for removing the resulting reaction mixture from said reaction zone, and (f) means including a high turbulence zone for scrubbing the thus removed reaction mixture by contact with a high velocity concurrent aqueous scrubbing solution.
Claim 2
Dependent Claim
186 words
Apparatus for separating base metal and silver from precious metal components in a mineral concentrate containing the same which comprises: (a) a tubular member made of heat resistant material and forming a reaction zone, (b) a tubular assembly including at least one tube having an end opening into said reaction zone and means for passing hydrogen and chlorine through said assembly to said end to form a hydrogen-chlorine flame at said end extending into said reaction zone, (c) a supply of mineral concentrate in particulate form and means communicating with said supply and including a venturi intermediate the ends of said tube for inducting said concentrate in particulate form into said tube and for feeding the thus inducted concentrate through said tube to the end thereof and then into said flame, (d) heat insulation means for maintaining said reaction zone at a temperature between 900° C. and 2500° C., (e) means for removing the resulting reaction mixture from said reaction zone, and (f) means including a high turbulence zone for scrubbing the thus removed reaction mixture by contact with a high velocity concurrent aqueous scrubbing solution.
Claim 3
Dependent Claim
13 words
Apparatus according to claim 1 in which the heat resistant material comprises ceramic.
Claim 4
Dependent Claim
24 words
Apparatus according to claim 2 in which the ceramic is selected from the group consisting of alumina, silica, alumina-silica, titania, zirconia, hafnia and thoria.
Claim 5
Dependent Claim
11 words
Apparatus according to claim 2 in which the ceramic is lagged.
Claim 6
Dependent Claim
17 words
Apparatus according to claim 1 wherein said assembly includes separate concentric tubes for supplying hydrogen and chlorine.
Claim 7
Dependent Claim
19 words
Apparatus according to claim 5 including means for supplying a carrier gas to feed said concentrate through said tube.
Claim 8
Dependent Claim
22 words
Apparatus according to claim 6 in which the particulate mineral concentrate is fed to the carrier gas by means of a Vibrofeeder.
Claim 9
Dependent Claim
26 words
Apparatus according to claim 6 in which means are provided for controlling the rate of flow of hydrogen, chlorine and carrier gas to the said flame.
Claim 10
Dependent Claim
17 words
Apparatus according to claim 1 including an expansion zone between the reaction zone and the scrubbing means.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1982-03-19 | 1982-09-18 | 1983-03-20 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1986-03-19 | 1986-09-18 | 1987-03-20 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1990-03-19 | 1990-09-18 | 1991-03-20 | $7700.00 | Window Closed / Lapsed |