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US4142860A Expired / Lapsed US ⏱️ 0.0 years remaining

Apparatus for producing a calibration sample for analytical instrumentation

Assignee: Individual
•
Filing: 1976-06-23
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Granted: 1979-03-06
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Expires: 1996-06-23
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Abstract

Abstract Apparatus for and method of preparing reference mixture gas samples for use with analytical instrumentation and small scale chemical reactions and processes, having a motor-driven magnetic stirrer with the motor and driving magnet mounted externally of the mixing chamber. Such structure together with the mass of the mixing chamber, which is large in comparison to the mass of the samples, helps to stabilize the temperature of the mixing chamber.

Inventors

  • 👤 Donald P. Mayeaux

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-04 19:49
CPC Classifications
F; F17; F17D; F17D3/00; F17D3/12; B; B01; B01F; B01F23/00; B01F23/10; B01F23/19; B01F33/00; B01F33/45; B01F33/453; B01F33/4531; G; G01; G01N; G01N33/00; G01N33/0004; G01N33/0006; G01N30/00; G01N30/02; G01N30/04; G01N2030/042; G01N2030/047; Y; Y10; Y10T; Y10T137/00; Y10T137/2496; Y10T137/2499; Y10T137/8158; Y10T137/8326; Y10T137/8593; Y10T137/85954; Y10T137/86389; Y10T137/86445; Y10T137/86461; Y10T137/87571; Y10T137/87652; Y10T137/8766; Y10T137/87676; Y10T137/87684; Y10T436/00; Y10T436/10; Y10T436/100833

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 229 words
Apparatus for producing a calibration gas mixture of known composition from a plurality of component gases separately introduced therein and blended together for use with analytical instrumentation, including: a pressure vessel forming a gas mixing chamber of mass large relative to the mass of the gaseous contents introduced therein to provide a sufficient heat sink to hold the gas temperature substantially stable during the blending of the gases; a stirring element movably disposed in said gas mixing chamber for homogenizing the mixture of gases introduced into, and retained within, said chamber while the gases are homogenized; exhaust valve means operatively communicated with said chamber for controlling flow from said gas mixing chamber; vacuum means communicating with said exhaust valve means of said gas mixing chamber for substantially exhausting said gas mixing chamber when desired; pressure transducer means for measuring the absolute pressure of the gases in said mixing chamber and producing a usable output signal in response to the absolute pressure present in said mixing chamber; pressure indicator means operatively connected with said pressure transducer means for displaying the absolute pressure measured by said pressure transducer means; and a plurality of inlet valves, each of which is in fluid communication with said mixing chamber and with a supply of a component gas of the gas mixture for controlling the introduction of the desired component gases into said mixing chamber.
Claim 2
Dependent Claim 229 words
Apparatus for producing a calibration gas mixture of known composition from a plurality of component gases separately introduced therein and blended together for use with analytical instrumentation, including: a pressure vessel forming a gas mixing chamber of mass large relative to the mass of the gaseous contents introduced therein to provide a sufficient heat sink to hold the gas temperature substantially stable during the blending of the gases; a stirring element movably disposed in said gas mixing chamber for homogenizing the mixture of gases introduced into, and retained within, said chamber while the gases are homogenized; exhaust valve means operatively communicated with said chamber for controlling flow from said gas mixing chamber; vacuum means communicating with said exhaust valve means of said gas mixing chamber for substantially exhausting said gas mixing chamber when desired; pressure transducer means for measuring the absolute pressure of the gases in said mixing chamber and producing a usable output signal in response to the absolute pressure present in said mixing chamber; pressure indicator means operatively connected with said pressure transducer means for displaying the absolute pressure measured by said pressure transducer means; and a plurality of inlet valves, each of which is in fluid communication with said mixing chamber and with a supply of a component gas of the gas mixture for controlling the introduction of the desired component gases into said mixing chamber.
Claim 3
Dependent Claim 73 words
The apparatus as set forth in claim 1, wherein said stirring element has magnetic properties; a movable drive magnet disposed exteriorly of said pressure vessel and in such near proximity of the stirring element to effect a sufficient magnetic force between the drive magnet and the stirring element to effect movement of said stirring element when said drive magnet moves; and means operatively connected with said drive magnet for moving said drive magnet.
Claim 4
Dependent Claim 20 words
The apparatus as set forth in claim 2, wherein: said means for moving said drive magnet is an electric motor.
Claim 5
Dependent Claim 30 words
The apparatus as set forth in claim 2, including: said stirring element is rotatably mounted in said mixing chamber; and said drive magnet is rotated to rotate said stirring element.
Claim 6
Dependent Claim 20 words
The apparatus as set forth in claim 4, wherein: said means for rotating said drive magnet is an electric motor.
Claim 7
Dependent Claim 43 words
The apparatus as set forth in claim 1, wherein said vacuum means further includes: a vacuum pump means for exhausting to an absolute pressure of substantially zero; and vacuum conduit means for fluidly connecting said vacuum pump means and said exhaust valve means.
Claim 8
Dependent Claim 227 words
Apparatus for producing a calibration gas mixture of known composition for use with analytical instrumentation, including: a pressure vessel forming a gas mixing chamber; mixing means for homogenizing the mixture of gases introduced into said chamber; vacuum means communicating with said gas mixing chamber for substantially exhausting said gas mixing chamber when desired; pressure transducer means for measuring the absolute pressure of the gases in said mixing chamber and producing a usable output signal in response to the absolute pressure present in said mixing chamber; pressure indicator means operably connected with said pressure transducer means for displaying the absolute pressure measured by said pressure transducer means; a plurality of inlet valves, each of which is in fluid communication with said mixing chamber and with a supply of a component gas of the gas mixture for controlling the introduction of the desired component gases into said mixing chamber; a vacuum pump means for exhausting to an absolute pressure of substantially zero; exhaust valve means for controlling flow from said mixing chamber to said vacuum pump means; vacuum conduit means for fluidly connecting said vacuum pump means and said exhaust valve means; a branch connection means for forming a passageway for transferring the mixture of gases in said mixing chamber into a sample container; and a sample valve in said branch connection for controlling flow through said branch connection.
Claim 9
Dependent Claim 227 words
Apparatus for producing a calibration gas mixture of known composition for use with analytical instrumentation, including: a pressure vessel forming a gas mixing chamber; mixing means for homogenizing the mixture of gases introduced into said chamber; vacuum means communicating with said gas mixing chamber for substantially exhausting said gas mixing chamber when desired; pressure transducer means for measuring the absolute pressure of the gases in said mixing chamber and producing a usable output signal in response to the absolute pressure present in said mixing chamber; pressure indicator means operably connected with said pressure transducer means for displaying the absolute pressure measured by said pressure transducer means; a plurality of inlet valves, each of which is in fluid communication with said mixing chamber and with a supply of a component gas of the gas mixture for controlling the introduction of the desired component gases into said mixing chamber; a vacuum pump means for exhausting to an absolute pressure of substantially zero; exhaust valve means for controlling flow from said mixing chamber to said vacuum pump means; vacuum conduit means for fluidly connecting said vacuum pump means and said exhaust valve means; a branch connection means for forming a passageway for transferring the mixture of gases in said mixing chamber into a sample container; and a sample valve in said branch connection for controlling flow through said branch connection.
Claim 10
Dependent Claim 55 words
The apparatus as set forth in claim 1, wherein: said pressure transducer is one producing a direct current or voltage output signal that increases linearly with increased pressure in the mixing chamber; and said pressure indicator means is one having a digital display of the voltage output signal of the pressure in said mixing chamber.
Claim 11
Dependent Claim 25 words
The apparatus as set forth in claim 1, wherein: each of said inlet valves is a right angled type valve mounted with the pressure vessel.

References Cited (Backward Citations)

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US3071447A Cited
US3249413A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1982-03-05 1982-09-04 1983-03-06 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1986-03-05 1986-09-04 1987-03-06 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1990-03-05 1990-09-04 1991-03-06 $7700.00 Window Closed / Lapsed

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