Patent US4133854A successfully refreshed from Google Patents.
US4133854A
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Method for producing small hollow spheres
Assignee: United States Department of Energy
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Filing: 1977-06-16
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Granted: 1979-01-09
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Expires: 1997-06-16
Abstract
Abstract Method for producing small hollow spheres of glass, metal or plastic, wherein the sphere material is mixed with or contains as part of the composition a blowing agent which decomposes at high temperature (T ≳ 600° C). As the temperature is quickly raised, the blowing agent decomposes and the resulting gas expands from within, thus forming a hollow sphere of controllable thickness. The thus produced hollow spheres (20 to 10 3 μm) have a variety of application, and are particularly useful in the fabrication of targets for laser implosion such as neutron sources, laser fusion physics studies, and laser initiated fusion power plants.
Inventors
- 👤 Charles D. Hendricks
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-26 16:17
CPC Classifications
C; C03; C03B; C03B19/00; C03B19/10; C03B19/1005; C03B19/1055; B; B01; B01J; B01J2/00; B01J2/02; B01J2/04; B22; B22F; B22F1/00; B22F1/06; B22F1/065; B22F1/0655; C03B19/107; C03B19/1075; C03C; C03C11/00; C03C11/002; Y; Y02; Y02P; Y02P40/00; Y02P40/50; Y02P40/57; Y10; Y10S; Y10S376/00; Y10S376/916; Y10T; Y10T428/00; Y10T428/29; Y10T428/2982; Y10T428/2991; Y10T428/2993; Y10T428/2996
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
158 words
A method for producing small hollow spheres of uniform wall thickness and diameter comprising the steps of: forming drops from a solution of selected materials composed of sphere forming material and a blowing agent which decomposes at a certain temperature producing a gas agent, placing an electrical charge on at least a portion of the thus formed drops, passing the thus formed drops along a flow path through deflection electrode means wherein the drops having a certain electric charge are deflected from the flow path and separated from the remaining drops, passing the remaining drops through a multiple zone oven having an increasing temperature in each subsequent zone causing drying of the drops and forming same into hollow spheres by melting of the thus dried drops and thermal decomposing of the blowing agent such that a bubble is formed therein and expanded to form the sphere forming material into hollow spheres of substantially uniform wall thickness upon cooling.
Claim 2
Independent Claim
158 words
A method for producing small hollow spheres of uniform wall thickness and diameter comprising the steps of: forming drops from a solution of selected materials composed of sphere forming material and a blowing agent which decomposes at a certain temperature producing a gas agent, placing an electrical charge on at least a portion of the thus formed drops, passing the thus formed drops along a flow path through deflection electrode means wherein the drops having a certain electric charge are deflected from the flow path and separated from the remaining drops, passing the remaining drops through a multiple zone oven having an increasing temperature in each subsequent zone causing drying of the drops and forming same into hollow spheres by melting of the thus dried drops and thermal decomposing of the blowing agent such that a bubble is formed therein and expanded to form the sphere forming material into hollow spheres of substantially uniform wall thickness upon cooling.
Claim 3
Dependent Claim
29 words
The method defined in claim 1, additionally including the step of forming the solution of selected materials by mixing selected amounts of sodium silicate, potassium tetraborate, water and urea.
Claim 4
Dependent Claim
78 words
The method defined in claim 1, wherein the step of drying the drops is carried out in a first zone of the multiple zone oven maintained at a first temperature and wherein the step of forming the materials into a hollow sphere is carried out in a plurality of subsequent zones of the multiple zone oven maintained at a plurality of different temperatures, each of the subsequent zones having a respectively higher temperature than the previous zone temperature.
Claim 5
Dependent Claim
51 words
The method defined in claim 3, wherein the temperature of the first zone is about 200° C to 500° C, wherein the temperature of a first of the subsequent zones is 300° C to 900° C, and wherein the temperature of the remaining subsequent zones is 500° C to 1350° C.
Claim 6
Dependent Claim
66 words
The method defined in claim 1, additionally including the step of forming the sphere forming material of the solution of selected materials by dissolving 100 grams of sodium silicate, 21.3 grams of potassium tetraborate, 5.2 grams of potassium hydroxide, and 4.9 grams of sodium hydroxide in water to make 1 liter of solution, and wherein the blowing agent of the solution of selected materials is urea.
References Cited (Backward Citations)
US3347798A
Cited
US3975194A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1982-01-08 | 1982-07-10 | 1983-01-09 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1986-01-08 | 1986-07-10 | 1987-01-09 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1990-01-08 | 1990-07-10 | 1991-01-09 | $7700.00 | Window Closed / Lapsed |