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Patent US4133691A successfully refreshed from Google Patents.
US4133691A
Expired / Lapsed
US
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Process for preparing inorganic foam materials
Assignee: WR Grace and Co
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Filing: 1978-01-18
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Granted: 1979-01-09
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Expires: 1998-01-18
Abstract
Abstract An inorganic foam formed by initially mixing particulate aluminum with an aqueous solution of an alkali metal base for a time sufficient to at least initially cause the formation of hydrogen gases therefrom, folding the mixture into an aqueous alkali metal silicate solution in a manner to substantially retain concentrated areas of the mixture in the silicate solution for a time sufficient to allow a substantial amount of the theoretical hydrogen gas to form, then thoroughly mixing the materials to form a solid inorganic foam.
Inventors
- 👤 Lawrence J. Kindt
- 👤 James M. Gaidis
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 12:45
CPC Classifications
C; C04; C04B; C04B28/00; C04B28/24; C04B28/26
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
147 words
A process for preparing an inorganic foam comprising: mixing particulate metallic aluminum with an aqueous basic solution formed from a water soluble base selected from an alkali metal oxide, alkali metal hydroxide or alkali metal aluminate or mixtures thereof for a time sufficient to form an Al/base mixture and to initiate the formation of hydrogen therefrom; said aluminum and base being present in an amount to cause the formation of sufficient gas to produce said foam; folding in the Al/base mixture into a separate aqueous alkali metal silicate solution at from about ambient temperatures to 40° C. and in a manner to substantially retain concentrated areas of said mixture in said silicate solution for a time to permit a substantial amount of hydrogen to be generated therein; and recovering an inorganic foam, said foam having a silica to alumina molar ratio of from about 1:1 to 10:1.
Claim 2
Dependent Claim
147 words
A process for preparing an inorganic foam comprising: mixing particulate metallic aluminum with an aqueous basic solution formed from a water soluble base selected from an alkali metal oxide, alkali metal hydroxide or alkali metal aluminate or mixtures thereof for a time sufficient to form an Al/base mixture and to initiate the formation of hydrogen therefrom; said aluminum and base being present in an amount to cause the formation of sufficient gas to produce said foam; folding in the Al/base mixture into a separate aqueous alkali metal silicate solution at from about ambient temperatures to 40° C. and in a manner to substantially retain concentrated areas of said mixture in said silicate solution for a time to permit a substantial amount of hydrogen to be generated therein; and recovering an inorganic foam, said foam having a silica to alumina molar ratio of from about 1:1 to 10:1.
Claim 3
Dependent Claim
41 words
The process according to claim 1 wherein the amount of base is from about 0.8 to 3 moles per mole of metallic aluminum; and the alkali metal silicate has an alkali metal oxide to silicon oxide ratio of 1:1 to 1:4.
Claim 4
Dependent Claim
20 words
The process according to claim 1 wherein the silica to alumina molar ratio is from about 2:1 to about 5:1.
Claim 5
Dependent Claim
39 words
The process according to claim 1 wherein the basic solution is formed from base material selected from an alkali metal oxide, an alkali metal hydroxide or mixtures of an alkali metal aluminate with an alkali metal oxide or hydroxide.
Claim 6
Dependent Claim
12 words
The process according to claim 1 wherein the alkali metal is sodium.
Claim 7
Dependent Claim
12 words
The process according to claim 4 wherein the alkali metal is sodium.
Claim 8
Dependent Claim
24 words
The process according to claim 1 wherein the particulate metallic aluminum and the basic solution is mixed together for up to about 5 seconds.
Claim 9
Dependent Claim
22 words
The process according to claim 1 wherein the particulate metallic aluminum is capable of passing through a 200 mesh (U.S. Standard) screen.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1982-01-08 | 1982-07-10 | 1983-01-09 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1986-01-08 | 1986-07-10 | 1987-01-09 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1990-01-08 | 1990-07-10 | 1991-01-09 | $7700.00 | Window Closed / Lapsed |