Patent US4132666A successfully refreshed from Google Patents.
US4132666A
Expired / Lapsed
US
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Process for preparing alkali metal dispersions
Assignee: JSR Corp
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Filing: 1977-07-27
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Granted: 1979-01-02
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Expires: 1997-07-27
Abstract
Abstract A process for preparing alkali metal dispersions comprises continuously feeding a molten alkali metal, a dispersing agent, and an inactive dispersion liquid to a multipass emulsifier to form an emulsion of the molten alkali metal, and rapidly cooling the emulsion to a temperature at least 10° C lower than the melting point of the alkali metal.
Inventors
- 👤 Tatsusuke Chikatsu
- 👤 Shinichi Shimokawa
- 👤 Takao Miura
- 👤 Taro Okumura
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-09 03:41
CPC Classifications
B; B01; B01F; B01F23/00; B01F23/40; B01F23/41; B01F23/4105; B01F23/43; B01F23/48; B01F23/482; B01F23/50; B01F23/51; B01F23/511; B01F27/00; B01F27/80; B01F27/91; B01J; B01J13/00; B01J13/0004; B01J13/0043; B01J13/0086; B01F27/05; B01F27/11; B01F27/15
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
172 words
A process for preparing alkali metal dispersions which comprises continuously feeding a molten alkali metal, a dispersing agent and an inactive dispersion liquid to a multipass emulsifier to form an emulsion of the molten alkali metal, and continuously transferring the resulting emulsion into a container containing a sufficient quantity of a liquid carrier under agitation thereby rapidly cooling the emulsion to a temperature at least 10° lower than the melting point of the alkali metal; the said emulsifier comprising a main cylinder having a cover on its upper end, an auxiliary cylinder located with upper and lower ends open in a middle lower part of the space inside the main cylinder, and a turbine mounted in the auxiliary cylinder to form an upward axial fluid flow, said main cylinder having an inlet formed in the portion facing the bottom of the auxiliary cylinder and also having an overflow gap provided between the entire upper periphery of the main cylinder and the cover and communicated with a discharge pipe surrounding the main cylinder.
Claim 2
Dependent Claim
172 words
A process for preparing alkali metal dispersions which comprises continuously feeding a molten alkali metal, a dispersing agent and an inactive dispersion liquid to a multipass emulsifier to form an emulsion of the molten alkali metal, and continuously transferring the resulting emulsion into a container containing a sufficient quantity of a liquid carrier under agitation thereby rapidly cooling the emulsion to a temperature at least 10° lower than the melting point of the alkali metal; the said emulsifier comprising a main cylinder having a cover on its upper end, an auxiliary cylinder located with upper and lower ends open in a middle lower part of the space inside the main cylinder, and a turbine mounted in the auxiliary cylinder to form an upward axial fluid flow, said main cylinder having an inlet formed in the portion facing the bottom of the auxiliary cylinder and also having an overflow gap provided between the entire upper periphery of the main cylinder and the cover and communicated with a discharge pipe surrounding the main cylinder.
Claim 3
Dependent Claim
171 words
A process for preparing alkali metal dispersions which comprises continuously feeding a molten alkali metal, a dispersing agent, and an inactive dispersion liquid to a multipass emulsifier to form an emulsion of the molten alkali metal, and causing the resulting emulsion to flow through a tubular cooler at a linear velocity up to 50 cm/second, thereby cooling it to a temperature at least 10° C lower than the melting point of the alkali metal; the said emulsifier comprising a main cylinder having a cover on its upper end, an auxiliary cylinder located with upper and lower ends open in a middle lower part of the space inside the main cylinder, and a turbine mounted in the auxiliary cylinder to form an upward axial fluid flow, said main cylinder having an inlet formed in the portion facing the bottom of the auxiliary cylinder and also having an overflow gap provided between the entire upper periphery of the main cylinder and the cover and communicated with a discharge pipe surrounding the main cylinder.
Claim 4
Dependent Claim
171 words
A process for preparing alkali metal dispersions which comprises continuously feeding a molten alkali metal, a dispersing agent, and an inactive dispersion liquid to a multipass emulsifier to form an emulsion of the molten alkali metal, and causing the resulting emulsion to flow through a tubular cooler at a linear velocity up to 50 cm/second, thereby cooling it to a temperature at least 10° C lower than the melting point of the alkali metal; the said emulsifier comprising a main cylinder having a cover on its upper end, an auxiliary cylinder located with upper and lower ends open in a middle lower part of the space inside the main cylinder, and a turbine mounted in the auxiliary cylinder to form an upward axial fluid flow, said main cylinder having an inlet formed in the portion facing the bottom of the auxiliary cylinder and also having an overflow gap provided between the entire upper periphery of the main cylinder and the cover and communicated with a discharge pipe surrounding the main cylinder.
Claim 5
Dependent Claim
30 words
A process as defined in claim 2, wherein said tubular cooler comprises an interior cooling pipe with an exterior jacket and is adapted to circulate a coolant through said jacket.
Claim 6
Dependent Claim
13 words
A process as defined in claim 1 wherein said alkali metal is sodium.
Claim 7
Dependent Claim
13 words
A process as defined in claim 1 wherein said alkali metal is lithium.
Claim 8
Dependent Claim
13 words
A process as defined in claim 2 wherein said alkali metal is sodium.
Claim 9
Dependent Claim
13 words
A process as defined in claim 2 wherein said alkali metal is lithium.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1982-01-01 | 1982-07-03 | 1983-01-02 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1986-01-01 | 1986-07-03 | 1987-01-02 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1990-01-01 | 1990-07-03 | 1991-01-02 | $7700.00 | Window Closed / Lapsed |