Patent US4130669A successfully refreshed from Google Patents.
US4130669A
Expired / Lapsed
US
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Method of making an improved tea volatiles concentrate
Assignee: Procter and Gamble Co
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Filing: 1977-06-22
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Granted: 1978-12-19
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Expires: 1997-06-22
Abstract
Abstract A method of steam-stripping and recovering desirable volatiles from ground tea leaves by subjecting them to conditions which preserve the freshness of the tea volatiles as well as the freshness of the soluble solids remaining in the devolatilized tea. A bed of mechanically fluidized ground tea leaves is sprayed with 32°-160° F. water and contacted with steam in free space for devolatilization under an absolute pressure of 5-250 mm of Hg and a temperature of 32°-160° F. The resulting volatiles-laden steam is then freeze-condensed under an absolute pressure of about 0-80 mm Hg and under super-cold conditons to provide a frost. A tea volatiles-containing concentrate is prepared by contacting the frozen condensate, the frost, with an aqueous tea extract.
Inventors
- 👤 Richard Gregg
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-09 23:00
CPC Classifications
A; A23; A23F; A23F3/00; A23F3/40; A23F3/42; A23F3/426
Claims Analysis
Total Claims: 8
Claim 1
Independent Claim
284 words
A method for preparing a tea volatiles concentrate from ground tea leaves comprising the steps of: (a) uniformly wetting said ground tea with from about 0.1 to about 3.0 parts water per part of ground tea, said water being at a temperature of from about 32° F. to about 160° F.; (b) contacting said ground tea while, in a state of fluidization in free space, with from about 0.005 to about 0.20 parts steam, per part of ground tea, thereby to provide volatiles-laden steam and devolatilized ground tea; said contact being conducted under an absolute pressure of from about 5 to about 250 mm of mercury, the steam having a temperature of from about 32° F. to about 160° F., said ground tea making contact with said steam for about 0.1 to about 45 minutes; (c) collecting the volatiles-laden steam as a frost by freeze condensation at a temperature of from about -100° F. to about -320° F. and at an absolute pressure of from about 0 to about 80 mm of mercury; (d) melting the frost to form a tea volatiles concentrate by contacting the frost with at least an equal weight of an aqueous tea extract having a solids content of from about 15% to about 65%; and wherein said fluidization is mechanically induced within a horizontal mixing shell by mixing tools which rotate within said shell at high speeds sufficient to impart rapid hurling-and-whirling motion to the ground tea leaves, said mixing tools being so designed such as to lift, drop and push the ground tea leaves from the walls of said shell into free space so that intimate steam contact takes place without adverse effect on said ground tea leaves.
Claim 2
Independent Claim
284 words
A method for preparing a tea volatiles concentrate from ground tea leaves comprising the steps of: (a) uniformly wetting said ground tea with from about 0.1 to about 3.0 parts water per part of ground tea, said water being at a temperature of from about 32° F. to about 160° F.; (b) contacting said ground tea while, in a state of fluidization in free space, with from about 0.005 to about 0.20 parts steam, per part of ground tea, thereby to provide volatiles-laden steam and devolatilized ground tea; said contact being conducted under an absolute pressure of from about 5 to about 250 mm of mercury, the steam having a temperature of from about 32° F. to about 160° F., said ground tea making contact with said steam for about 0.1 to about 45 minutes; (c) collecting the volatiles-laden steam as a frost by freeze condensation at a temperature of from about -100° F. to about -320° F. and at an absolute pressure of from about 0 to about 80 mm of mercury; (d) melting the frost to form a tea volatiles concentrate by contacting the frost with at least an equal weight of an aqueous tea extract having a solids content of from about 15% to about 65%; and wherein said fluidization is mechanically induced within a horizontal mixing shell by mixing tools which rotate within said shell at high speeds sufficient to impart rapid hurling-and-whirling motion to the ground tea leaves, said mixing tools being so designed such as to lift, drop and push the ground tea leaves from the walls of said shell into free space so that intimate steam contact takes place without adverse effect on said ground tea leaves.
Claim 3
Dependent Claim
42 words
The method of claim 1 wherein said aqueous tea extract has a solids content of from about 27% to about 50% solids and wherein the weight ratio of said aqueous tea extract to said frost is from about 1.1 to about 10.1.
Claim 4
Dependent Claim
12 words
The method of claim 1 wherein said method is a continuous process.
Claim 5
Dependent Claim
22 words
The method of claim 3 wherein said ground tea has an average particle size of from about 25 to about 1000 microns.
Claim 6
Dependent Claim
22 words
The method of claim 3 wherein said ground tea is in contact with said steam for about 0.5 to about 10 minutes.
Claim 7
Dependent Claim
12 words
The method of claim 1 wherein said tea volatiles concentrate is freeze-dried.
Claim 8
Dependent Claim
23 words
The method of claim 1 wherein said wetting is conducted while the ground tea leaves are mechanically hurled and whirled in free space.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1981-12-18 | 1982-06-19 | 1982-12-19 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1985-12-18 | 1986-06-19 | 1986-12-19 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1989-12-18 | 1990-06-19 | 1990-12-19 | $7700.00 | Window Closed / Lapsed |