Patent US4128672A successfully refreshed from Google Patents.
US4128672A
Expired / Lapsed
US
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Process of making a magnetic recording medium
Assignee: BASF SE
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Filing: 1975-10-24
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Granted: 1978-12-05
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Expires: 1995-10-24
Abstract
Abstract A process for the manufacture of rigid magnetic recording media by depositing a cobalt-containing ferromagnetic metal layer on a non-magnetic metallic base disc provided with a cured layer of binder which does not dissolve or swell in organic solvents and contains non-magnetic pigments, and which has been activated, before deposition of the ferromagnetic layer, by treatment with a solution of a palladium (O) complex in an organic solvent, followed by decomposition of this complex, to prepare it to receive the ferromagnetic metal layer which is produced by electroless deposition.
Inventors
- 👤 Gerd Wunsch
- 👤 Paul Deigner
- 👤 Roland Falk
- 👤 Karl Mahler
- 👤 Werner Loeser
- 👤 Friedrich Domas
- 👤 Peter Felleisen
- 👤 Werner Steck
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-30 22:27
CPC Classifications
G; G11; G11B; G11B5/00; G11B5/84; G11B5/62; G11B5/68; G11B5/70; G11B5/708; G11B5/7085; H; H01; H01F; H01F41/00; H01F41/14
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
221 words
In a process for the manufacture of rigid magnetic recording media in which a thin film of a cobalt-containing ferromagnetic metal having a coercivity of from 23 to 75k A/m is deposited by electroless deposition on an activated rigid base followed by the application of a less than 0.1 μ thick protective layer to the surface of the said thin film of cobalt-containing ferromagnetic metal and said rigid base includes a non-magnetic metallic base disc at least one surface of which carry a layer (S) from 2 to 100 μm thick, which layer (S) has been brought by machining to a peak-to-valley height R t of not more than 0.3 μ, is insoluble in, and virtually non-swellable by, organic solvents and consists of a dispersion of from 0.5 to 5 parts by weight of a finely divided non-magnetic pigment (P) of a Mohs' hardness of at least 6, per part by weight of a cured binder (B) which firmly bonds the pigments to the base disc, the improvement which comprises: activating the surface of the base disc by treatment with a solution of a palladium(O) complex in an organic solvent and decomposing the complex, and thereafter depositing a thin film of ferromagnetic metal of about 0.05 to 1 μ thickness on the so-activated surface of the base disc by electroless deposition.
Claim 2
Dependent Claim
221 words
In a process for the manufacture of rigid magnetic recording media in which a thin film of a cobalt-containing ferromagnetic metal having a coercivity of from 23 to 75k A/m is deposited by electroless deposition on an activated rigid base followed by the application of a less than 0.1 μ thick protective layer to the surface of the said thin film of cobalt-containing ferromagnetic metal and said rigid base includes a non-magnetic metallic base disc at least one surface of which carry a layer (S) from 2 to 100 μm thick, which layer (S) has been brought by machining to a peak-to-valley height R t of not more than 0.3 μ, is insoluble in, and virtually non-swellable by, organic solvents and consists of a dispersion of from 0.5 to 5 parts by weight of a finely divided non-magnetic pigment (P) of a Mohs' hardness of at least 6, per part by weight of a cured binder (B) which firmly bonds the pigments to the base disc, the improvement which comprises: activating the surface of the base disc by treatment with a solution of a palladium(O) complex in an organic solvent and decomposing the complex, and thereafter depositing a thin film of ferromagnetic metal of about 0.05 to 1 μ thickness on the so-activated surface of the base disc by electroless deposition.
Claim 3
Dependent Claim
22 words
A process as set forth in claim 1, wherein the magnetic thin film produced by electroless deposition is thickened by electrolytic deposition.
Claim 4
Dependent Claim
32 words
A process as set forth in claim 1, wherein the recording medium carrying the thin film of ferromagnetic metal is heated at from about 150° to 300° C. under an inert gas.
Claim 5
Dependent Claim
25 words
A process as set forth in claim 1, wherein the palladium(O) complexes are decomposed by heating in the course of activating the machined layer (S).
Claim 6
Dependent Claim
82 words
A process as set forth in claim 1, wherein a solution of a film-forming organic synthetic resin in a volatile solvent is applied to the thin film of cobalt-containing ferromagnetic metal in such an amount that the thickness of the layer of solution in the dried but not baked state is not more than 0.3 μ, and the applied layer is dried and baked for from about 1 to 15 hours in an oxygen-containing atmosphere at from about 200° to 300° C.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1981-12-04 | 1982-06-05 | 1982-12-05 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1985-12-04 | 1986-06-05 | 1986-12-05 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1989-12-04 | 1990-06-05 | 1990-12-05 | $7700.00 | Window Closed / Lapsed |