Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
220 words
A method of forming self-supporting compacts from metal powder, which formed compacts have green densities substantially equal to the tap density of the metal powder and being adapted for sintering without blistering or cracking by injection molding, comprising (1) mixing the metal powder with a plastic medium in an amount sufficient to substantially fill the entire void volume of the metal powder, thereby forming a plastic mixture, the plastic medium comprising an organic binder dissolved in a solvent in which it is soluble at room temperature but in which it is substantially less soluble at a higher temperature such that the plastic medium increases in viscosity at higher temperatures by rejection of the solvent, (2) injecting the plastic mixture under pressure at room temperature into a closed die preheated to that higher temperature, whereby solvent is rejected from the mixture and the rejection of solvent and increase in viscosity of the plastic medium produces a compact sufficiently self-supporting to hold its molded shape and to be ejected from a die cavity (3) removing the compact from which solvent has been rejected from the die and (4) drying the ejected compact to remove the remaining solvent therefrom and leave interconnecting pores in the compact for the escape of gases resulting from subsequent burning out of the binder during the sintering operation.
Claim 2
Independent Claim
220 words
A method of forming self-supporting compacts from metal powder, which formed compacts have green densities substantially equal to the tap density of the metal powder and being adapted for sintering without blistering or cracking by injection molding, comprising (1) mixing the metal powder with a plastic medium in an amount sufficient to substantially fill the entire void volume of the metal powder, thereby forming a plastic mixture, the plastic medium comprising an organic binder dissolved in a solvent in which it is soluble at room temperature but in which it is substantially less soluble at a higher temperature such that the plastic medium increases in viscosity at higher temperatures by rejection of the solvent, (2) injecting the plastic mixture under pressure at room temperature into a closed die preheated to that higher temperature, whereby solvent is rejected from the mixture and the rejection of solvent and increase in viscosity of the plastic medium produces a compact sufficiently self-supporting to hold its molded shape and to be ejected from a die cavity (3) removing the compact from which solvent has been rejected from the die and (4) drying the ejected compact to remove the remaining solvent therefrom and leave interconnecting pores in the compact for the escape of gases resulting from subsequent burning out of the binder during the sintering operation.
Claim 3
Dependent Claim
15 words
The method of claim 1 in which the metal powder is a high performance superalloy.
Claim 4
Dependent Claim
20 words
The method of claim 1 in which the plastic medium is composed of a binder, a solvent and binder modifiers.
Claim 5
Dependent Claim
17 words
The method of claim 3 in which the binder is methyl cellulose, and the solvent is water.
Claim 6
Dependent Claim
14 words
The method of claim 4 in which the modifiers are glycerin and boric acid.
Claim 7
Dependent Claim
20 words
The method of claim 3 in which the solvent is more than about 50% by weight of the plastic medium.
Claim 8
Dependent Claim
47 words
The method of claim 3 in which the metal powder is ball milled powder of -325 mesh and the plastic medium comprises, by weight of the metal powder, 1.5% to 3.5% methyl cellulose, 0.25% to 2.0% glycerin, 0.1% to 1.0% boric acid and 8% to 12% water.
Claim 9
Dependent Claim
49 words
The method of claim 3 in which the metal powder is atomized powder of between -30 and -325 mesh, and the plastic medium comprises, by weight of the metal powder, 1.5% to 3.5% methyl cellulose, 0.1% to 1.0% boric acid, 0.25% to 2.0% glycerin and 4.0% to 6.0% water.
Claim 10
Dependent Claim
32 words
The method of claim 8 in which the plastic medium comprises, by weight of the metal powder, about 2% methyl cellulose, about 0.5% boric acid, about 1.0% glycerin and about 4.5% water.