Claims Analysis
Total Claims: 15
Claim 1
Independent Claim
392 words
A method for preparing a soluble instant coffee composition from roast and ground coffee comprising the steps of: (a) uniformly wetting a semi-bed of roast and ground coffee while the coffee is in a state of mechanical fluidization, with from about 0.1 to about 0.9 parts water per part of roast and ground coffee, said water being at a temperature of from about 32° F. to about 110° F., said roast and ground coffee having a particle size of from about 5 to about 800 microns; (b) contacting the mechanically fluidized roast and ground coffee with from about 0.005 to about 0.05 parts steam, per part of roast and ground coffee, thereby to provide volatiles-laden steam and devolatilized roast and ground coffee, said contact being conducted under an absolute pressure of from about 5 to about 100 mm of mercury, the steam having a temperature of from about 32° F. to about 110° F., said roast and ground coffee making contact with said steam for about 0.1 to about 45 minutes; (c) collecting the volatiles-laden steam as a frost by condensation at a temperature of from about -100° F. to about -320° F. and at an absolute pressure of from about 4 to about 80 mm of mercury; (d) melting the frost to form a volatiles-laden extract by contacting the frost with at least an equal weight of an aqueous coffee extract having a solids content of from about 25% to about 65%; (e) forming an aqueous slurry of the devolatilized roast and ground coffee and from about 2 parts to about 10 parts of water by dry weight of coffee, said slurry having a temperature of from about 80° F. to about 200° F., and gently agitating the slurry with a low shear agitation system so as to provide a substantially uniform suspension and an extract having a soluble coffee solids content of about 4% to about 15%, and wherein said soluble coffee solids are about 18% to about 27% of said roast and ground coffee on a dry weight basis, said low shear agitation system maintaining a substantially emulsion-free slurry, separating the aqueous extract from released coffee oil and extracted coffee grounds; and (f) drying the aqueous extracts of steps (d) and (e) to dry and soluble coffee powders; and (g) combining said powders to provide said instant coffee composition.
Claim 2
Independent Claim
392 words
A method for preparing a soluble instant coffee composition from roast and ground coffee comprising the steps of: (a) uniformly wetting a semi-bed of roast and ground coffee while the coffee is in a state of mechanical fluidization, with from about 0.1 to about 0.9 parts water per part of roast and ground coffee, said water being at a temperature of from about 32° F. to about 110° F., said roast and ground coffee having a particle size of from about 5 to about 800 microns; (b) contacting the mechanically fluidized roast and ground coffee with from about 0.005 to about 0.05 parts steam, per part of roast and ground coffee, thereby to provide volatiles-laden steam and devolatilized roast and ground coffee, said contact being conducted under an absolute pressure of from about 5 to about 100 mm of mercury, the steam having a temperature of from about 32° F. to about 110° F., said roast and ground coffee making contact with said steam for about 0.1 to about 45 minutes; (c) collecting the volatiles-laden steam as a frost by condensation at a temperature of from about -100° F. to about -320° F. and at an absolute pressure of from about 4 to about 80 mm of mercury; (d) melting the frost to form a volatiles-laden extract by contacting the frost with at least an equal weight of an aqueous coffee extract having a solids content of from about 25% to about 65%; (e) forming an aqueous slurry of the devolatilized roast and ground coffee and from about 2 parts to about 10 parts of water by dry weight of coffee, said slurry having a temperature of from about 80° F. to about 200° F., and gently agitating the slurry with a low shear agitation system so as to provide a substantially uniform suspension and an extract having a soluble coffee solids content of about 4% to about 15%, and wherein said soluble coffee solids are about 18% to about 27% of said roast and ground coffee on a dry weight basis, said low shear agitation system maintaining a substantially emulsion-free slurry, separating the aqueous extract from released coffee oil and extracted coffee grounds; and (f) drying the aqueous extracts of steps (d) and (e) to dry and soluble coffee powders; and (g) combining said powders to provide said instant coffee composition.
Claim 3
Dependent Claim
24 words
The method of claim 1 wherein said roast and ground coffee was ground at a temperature of about -110° F to about -320° F.
Claim 4
Dependent Claim
25 words
The method of claim 1 wherein said devolatilized roast and ground coffee has a slurry extraction residence time of about 3 to about 120 minutes.
Claim 5
Dependent Claim
12 words
The method of claim 1 wherein said method is a continuous process.
Claim 6
Dependent Claim
24 words
The method of claim 4 wherein said roast and ground coffee has an average particle size of from about 10 to about 400 microns.
Claim 7
Dependent Claim
24 words
The method of claim 4 wherein said roast and ground coffee is in contact with said steam for about 0.5 to about 10 minutes.
Claim 8
Dependent Claim
36 words
The method of claim 4 wherein the temperature of said slurry is between 90° F and 160° F, and said roast and ground coffee has a slurry extraction residence time of about 15 to 30 minutes.
Claim 9
Dependent Claim
22 words
The method of claim 4 wherein said slurry has a water:coffee ratio of from about 2:1 to about 5:1 parts by weight.
Claim 10
Dependent Claim
15 words
The method of claim 8 wherein said coffee:water ratio is from about 2.25:1 to 3.0:1.
Claim 11
Dependent Claim
15 words
The method of claim 1 wherein said aqueous coffee extract is freeze-concentrated and then freeze-dried.
Claim 12
Dependent Claim
17 words
The method of claim 1 wherein said aqueous coffee extract is concentrated by evaporation and then freeze-dried.
Claim 13
Dependent Claim
43 words
The method of claim 1 wherein said volatiles are recovered by melting said frost by contacting the frost with a 27% to 50% solids aqueous extract wherein the weight ratio of this extract to said frost is from about 1:1 to about 10:1.
Claim 14
Dependent Claim
17 words
The method of claim 1 wherein said aqueous coffee extract is concentrated by evaporation and then spray-dried.
Claim 15
Dependent Claim
25 words
The method of claim 1 wherein sad separated aqueous extract has a coffee oil content of less than 0.004 parts per part of soluble solids.