Patent US4097624A successfully refreshed from Google Patents.
US4097624A
Expired / Lapsed
US
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Method for the metallization of fibers
Assignee: University of Virginia
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Filing: 1977-09-30
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Granted: 1978-06-27
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Expires: 1997-09-30
Abstract
Abstract A method for decontaminating and subsequently metallizing a filament comprises:
Inventors
- 👤 Hermann J. Schladitz
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-27 16:43
CPC Classifications
C; C23; C23C; C23C16/00; C23C16/02; C23C16/0209; C03; C03C; C03C25/00; C03C25/002; C03C25/10; C03C25/12; C03C25/22; C03C25/223; C03C25/42; C03C25/46; C03C25/70; C23C16/44; C23C16/54; C23C16/545; D; D01; D01F; D01F11/00; D01F11/10; D01F11/12; D01F11/127; D06; D06M; D06M11/00; D06M11/83; D06M7/00; D06M7/005; F; F27; F27B; F27B9/00; F27B9/28
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
258 words
A method for decontaminating and subsequently metallizing a filament which comprises passing the filament through the inner tube of a first chamber for decontamination which comprises two concentric tubes having an annular space therebetween, the inner tube of which has a series of fine holes therein; wherein said inner tube is heated and said annular space contains an inert gas such that said gas flows through said holes in heated jet streams which impinge upon said filament, thereby heating and decontaminating said filament; passing said heated and decontaminated filament into a second chamber for metallization also comprising two concentric tubes having an annular space therebetween, the inner tube of which has a series of fine holes therein; wherein said inner tube of said second chamber is heated and said annular space of said second chamber contains a gaseous, thermally decomposable metal compound such that said gaseous metal compound flows through said holes in heated jet streams and impinges upon said heated and decontaminated filament, thereby thermally decomposing said metal compound and metallizing said filament; disposing an intermediate chamber in alignment with and with ends in sealing relationship with the respective ends of said decontamination and metallization chambers and having a membrane disposed intermediately and transversely thereof; communicating each said inner tube with its associated section of the intermediate chamber drawing off gaseous material entering each said section from said inner tubes; and passing said heated and decontaminated filament through said intermediate chamber and through a pinhole aperture in said membrane prior to said passing through the metallization chamber.
Claim 2
Independent Claim
258 words
A method for decontaminating and subsequently metallizing a filament which comprises passing the filament through the inner tube of a first chamber for decontamination which comprises two concentric tubes having an annular space therebetween, the inner tube of which has a series of fine holes therein; wherein said inner tube is heated and said annular space contains an inert gas such that said gas flows through said holes in heated jet streams which impinge upon said filament, thereby heating and decontaminating said filament; passing said heated and decontaminated filament into a second chamber for metallization also comprising two concentric tubes having an annular space therebetween, the inner tube of which has a series of fine holes therein; wherein said inner tube of said second chamber is heated and said annular space of said second chamber contains a gaseous, thermally decomposable metal compound such that said gaseous metal compound flows through said holes in heated jet streams and impinges upon said heated and decontaminated filament, thereby thermally decomposing said metal compound and metallizing said filament; disposing an intermediate chamber in alignment with and with ends in sealing relationship with the respective ends of said decontamination and metallization chambers and having a membrane disposed intermediately and transversely thereof; communicating each said inner tube with its associated section of the intermediate chamber drawing off gaseous material entering each said section from said inner tubes; and passing said heated and decontaminated filament through said intermediate chamber and through a pinhole aperture in said membrane prior to said passing through the metallization chamber.
Claim 3
Dependent Claim
12 words
The method of claim 1, wherein said filament has a fibrous structure.
Claim 4
Dependent Claim
19 words
The method of claim 1, wherein each said fine holes have a diameter of from 0.1 to 0.5 mm.
Claim 5
Dependent Claim
19 words
The method of claim 3, wherein said fine holes are arranged in a spiral configuration on said inner tubes.
Claim 6
Dependent Claim
39 words
The method of claim 4, wherein said inner tubes are heated by means of insulated heating wires arranged in spiral configurations on the outer surfaces of said inner tubes such that said spirally arranged fine holes are not covered.
Claim 7
Dependent Claim
28 words
The method of claim 1, wherein said inert gas is He, Ar, CO 2 , H 2 , CO, N 2 , inert organic vapors or mixtures thereof.
Claim 8
Dependent Claim
17 words
The method of claim 1, wherein said decomposable metal compound is a metal carbonyl, nitrosyl or ethylacetonate.
Claim 9
Dependent Claim
21 words
The method of claim 1, wherein said filament is made of carbon, graphite, glass, quartz, asbestos, polycarbonate, polyacrylinitrile, polyester, or polyamide.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1981-06-26 | 1981-12-26 | 1982-06-27 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1985-06-26 | 1985-12-26 | 1986-06-27 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1989-06-26 | 1989-12-26 | 1990-06-27 | $7700.00 | Window Closed / Lapsed |