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US4097614A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of removing bitter substances from brewers yeast and brewers yeast autolysates

Assignee: Mondelez Australia Foods Ltd
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Filing: 1976-12-23
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Granted: 1978-06-27
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Expires: 1996-12-23
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Abstract

Abstract Bitter substances (isohumulones) are removed from brewers yeast suspensions or brewers yeast autolysates by contacting a yeast suspension or yeast autolysate with a composite adsorbent material containing an adsorbent and magnetic particles embedded in a porous matrix of organic polymeric material having a pore size within the range of 2-30nm, and separating the composite containing isohumulone molecules adsorbed thereto from the suspension or autolysate. The composite may be regenerated by removing the adsorbed isohumulone which can then be recovered.

Inventors

  • 👤 Simon Michael West

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 15:15
CPC Classifications
C; C12; C12F; C12F3/00; C12F3/06; C12C; C12C9/00; C12C9/02; C12C9/025; C12N; C12N1/00; C12N1/005; C12C3/00; C12C3/12

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 110 words
A method for removing isohumulones from suspensions of brewers yeast and from brewers yeast autolysates, wherein the suspensions or autolysates are brought into contact with a composite adsorbent material which comprises adsorbent carbon particles and magnetic particles embedded in a porous matrix of organic polymeric material, the pore size of such matrix being within the range 2-30nm and such as to allow molecules of the isohumulones to enter freely into the interstitial structure of the matrix, but to exclude larger molecules which are to be retained in the suspension or solution being treated, and wherein the loaded composite adsorbent material is subsequently separated from the suspension or solution being treated.
Claim 2
Independent Claim 110 words
A method for removing isohumulones from suspensions of brewers yeast and from brewers yeast autolysates, wherein the suspensions or autolysates are brought into contact with a composite adsorbent material which comprises adsorbent carbon particles and magnetic particles embedded in a porous matrix of organic polymeric material, the pore size of such matrix being within the range 2-30nm and such as to allow molecules of the isohumulones to enter freely into the interstitial structure of the matrix, but to exclude larger molecules which are to be retained in the suspension or solution being treated, and wherein the loaded composite adsorbent material is subsequently separated from the suspension or solution being treated.
Claim 3
Dependent Claim 35 words
A method as claimed in claim 1 wherein the loaded composite adsorbent material, after being separated from the suspension or solution being treated, is subjected to a regeneration treatment thereby producing a liquor containing isohumulones.
Claim 4
Dependent Claim 16 words
A method as claimed in claim 1 wherein the pore size is within the range 2-7nm.
Claim 5
Dependent Claim 21 words
A method as claimed in claim 2 wherein the regeneration treatment comprises treating the loaded composite material with an aqueous alkali.
Claim 6
Dependent Claim 24 words
A method as claimed in claim 2 wherein the regeneration treatment comprises treating the loaded composite material with an alkali in an alcohol/water mixture.
Claim 7
Dependent Claim 15 words
A method as claimed in claim 2 wherein the regeneration treatment comprises treatment with isobutylene.
Claim 8
Dependent Claim 23 words
A method as claimed in claim 2 wherein the said liquor is treated to recover the isohumulone by extraction with an immiscible solvent.
Claim 9
Dependent Claim 28 words
A method as claimed in claim 7 wherein the pH of the said liquor is adjusted to about pH 2 and the liquor is then extracted with iso-octane.

References Cited (Backward Citations)

US2149306A Cited
US3839588A Cited
US3862030A Cited
US3940498A Cited
US4018886A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-06-26 1981-12-26 1982-06-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-06-26 1985-12-26 1986-06-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-06-26 1989-12-26 1990-06-27 $7700.00 Window Closed / Lapsed

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