US3940498A
Expired / Lapsed
US
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Chill-proofing with synthetic magnesium silicates
Assignee: CELITE Corp
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Filing: 1974-09-03
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Granted: 1976-02-24
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Expires: 1994-09-03
Abstract
Abstract Undesirable protein and polyphenol molecules are removed from aqueous liquids or suspensions, such as wort, wine, or beer, by contacting the liquid with acid-treated synthetic magnesium silicates containing less than about 14% magnesium oxide. The resultant liquid is more resistant to chill haze formation. Even better results are obtained if a polyamide is blended with the acid-treated synthetic silicate prior to contact with the liquid. A filter aid, such as diatomite, can also be combined with the acid-treated synthetic magnesium silicate and/or the blends containing the polyamide.
Inventors
- 👤 Elbert Roy Butterworth
- 👤 Willard John Duensing
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 03:34
CPC Classifications
C; C12; C12C; C12C7/00; C12C7/20; A; A23; A23L; A23L2/00; A23L2/70; A23L2/80; C12C7/26; C12H; C12H1/00; C12H1/02; C12H1/04; C12J; C12J1/00
Claims Analysis
Total Claims: 21
Claim 1
Independent Claim
74 words
A method of stabilizing aqueous liquids or aqueous liquid suspensions against chill haze formation comprising contacting said liquid or said suspension with an acid-treated synthetic magnesium silicate containing 13% or less by weight of magnesium, on an oxide basis, in an amount effective to eliminate or reduce said chill haze and seperating said silicate from said liquid or liquid suspension to provide an aqueous liquid or aqueous liquid suspension resistant to chill haze formation.
Claim 2
Independent Claim
74 words
A method of stabilizing aqueous liquids or aqueous liquid suspensions against chill haze formation comprising contacting said liquid or said suspension with an acid-treated synthetic magnesium silicate containing 13% or less by weight of magnesium, on an oxide basis, in an amount effective to eliminate or reduce said chill haze and seperating said silicate from said liquid or liquid suspension to provide an aqueous liquid or aqueous liquid suspension resistant to chill haze formation.
Claim 3
Dependent Claim
21 words
The method of claim 1 wherein said acid is an acid that forms a water-soluble compound upon reaction with magnesium oxide.
Claim 4
Dependent Claim
12 words
The method of claim 2 wherein the acid is a mineral acid.
Claim 5
Dependent Claim
23 words
The method of claim 3 wherein the mineral acid is a sulfuric acid and the magnesium oxide content is less than about 12%.
Claim 6
Dependent Claim
11 words
The method of claim 1 wherein the liquid suspension is wort.
Claim 7
Dependent Claim
23 words
The method of claim 1 wherein the liquid or suspension is selected from the group consisting of vinegar, beer, malt liquor, and ale.
Claim 8
Dependent Claim
12 words
The method of claim 1 wherein the liquid or suspension is wine.
Claim 9
Dependent Claim
11 words
The method of claim 4 wherein the liquid suspension is wort.
Claim 10
Dependent Claim
23 words
The method of claim 4 wherein the liquid or suspension is selected from the group consisting of vinegar, beer, malt liquor and ale.
Claim 11
Dependent Claim
31 words
The method of claim 1 wherein in addition to the acid-treated synthetic magnesium silicate there is also added a conventional filter aid material which is later removed in a filtering step.
Claim 12
Dependent Claim
26 words
The method of claim 1 wherein in addition to the acid-treated synthetic magnesium silicate there is also added one or more conventional chill haze control agents.
Claim 13
Dependent Claim
31 words
The method of claim 10 wherein in addition to the acid-treated synthetic magnesium silicate and a filter aid material there is also added one or more conventional chill haze control agents.
Claim 14
Dependent Claim
15 words
The method of claim 11 wherein the conventional chill haze control agent is polyvinyl polypyrrolidone.
Claim 15
Independent Claim
82 words
A method of stabilizing an aqueous liquid or aqueous liquid suspension selected from the group consisting of wort, beer and wine against chill haze formation comprising contacting said liquid or suspension with particles of acid-treated synthetic magnesium silicate, having a magnesium content of 13% or less by weight in an amount effective to stabilize said liquid or suspension against chill haze formation and separating said particles from said liquid or suspension to provide a liquid or suspension resistant to chill haze formation.
Claim 16
Independent Claim
82 words
A method of stabilizing an aqueous liquid or aqueous liquid suspension selected from the group consisting of wort, beer and wine against chill haze formation comprising contacting said liquid or suspension with particles of acid-treated synthetic magnesium silicate, having a magnesium content of 13% or less by weight in an amount effective to stabilize said liquid or suspension against chill haze formation and separating said particles from said liquid or suspension to provide a liquid or suspension resistant to chill haze formation.
Claim 17
Dependent Claim
19 words
The method of claim 14 wherein said acid contains sulfur as one of the constituents of the acid molecule.
Claim 18
Dependent Claim
12 words
The method of claim 15 wherein the acid is a mineral acid.
Claim 19
Dependent Claim
24 words
The method of claim 16 wherein the acid is sulfuric acid and the magnesium content, on an oxide basis is less than about 12%.
Claim 20
Dependent Claim
34 words
The method of claim 14 wherein the acid-treated magnesium silicate is added in an amount to provide a concentration of at least 2 pounds of acid-treated synthetic magnesium silicate per 100 barrels of beer.
Claim 21
Dependent Claim
24 words
The method of claim 18 wherein polyvinyl polypyrrolidone is also added in an amount less than the amount of acid-treated synthetic magnesium silicate added.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1979-02-23 | 1979-08-25 | 1980-02-24 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1983-02-23 | 1983-08-25 | 1984-02-24 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1987-02-23 | 1987-08-25 | 1988-02-24 | $7700.00 | Window Closed / Lapsed |