Patent US4073856A successfully refreshed from Google Patents.
US4073856A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method of fabricating welded PFA-to-PTFE structures
Assignee: Crane Co
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Filing: 1976-01-16
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Granted: 1978-02-14
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Expires: 1996-01-16
Abstract
Abstract A method is described whereby perfluoroalkoxy (PFA) fluorocarbon resin is fusion bonded to polytetrafluoroethylene (PTFE) resin to provide united sections thereof and to provide a bonded or welded interconnection between separate sections of PTFE resin. The welds are obtained under minimal positive pressure, generally below about 40 psi, at a temperature above the gel point of the PTFE resin, generally between 635° F. and 710° F., with subsequent slow cooling under pressures somewhat higher and generally ranging between about 59 psi and 150 psi.
Inventors
- 👤 Edward J. Chu
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-28 13:35
CPC Classifications
B; B29; B29C; B29C70/00; B29C70/68; B29C70/74; B29C70/76; B29C70/766; B29C35/00; B29C35/02; B29C35/04; B29C43/00; B29C43/02; B29C43/18; B29C63/00; B29C63/26; B29C63/34; B29C63/346; B29C65/00; B29C65/02; B29C66/00; B29C66/01; B29C66/05; B29C66/10; B29C66/11; B29C66/112; B29C66/1122; B29C66/50; B29C66/51; B29C66/52; B29C66/522; B29C66/5227; B29C66/52271; B29C66/52272; B29C66/70; B29C66/71; B29C66/80; B29C66/82; B29C66/824; B29C66/8248; B29C66/83; B29C66/832; B29C66/8322; B29C66/90; B29C66/91; B29C66/912; B29C66/9121; B29C66/91221; B29C66/914; B29C66/9141; B29C66/91411; B29C66/91431; B29C65/10; B29C65/18; B29C66/9161; B29C66/91641; B29C66/91643; B29C66/91645; B29K; B29K2027/00; B29K2027/12; B29K2027/18; B29K2105/00; B29K2105/25; B29K2105/251; B29L; B29L2023/00; B29L2023/22
Claims Analysis
Total Claims: 17
Claim 1
Independent Claim
291 words
A method of forming a fluorocarbon resin structure in which a body of PFA resin is fused to a body of sintered PTFE resin which comprises the steps of confining a quantity of particulate PGA resin in a zone contiguous to said body of sintered PTFE resin, heating said quantity of PFA resin and at least the PTFE resin which is adjacent said zone to a temperature above the gel point of said PTFE resin and above the melting point of said PFA resin to melt said PFA resin, maintaining said elevated temperature while compacting said PFA resin against said PTFE resin under positive pressure just sufficient to urge said PFA resin melt at a very slow rate without fault producing flow therein into intimate surface contact with said PTFE resin until said former wets the surface of said latter over an area to be fused, after establishing said intimate contact, maintaining the conditions static at the fusing interface by increasing the pressure applied to said PFA resin to a predetermined level at a rate which is sufficiently slow so that there is a minimum tendency for said PFA resin to flow along the surface of said mating PTFE resin, and permitting said resins to cool slowly without force cooling toward ambient temperature while maintaining said pressure near said predetermined level where said predetermined level is chosen sufficient to prevent the formation of sinks and voids in said PFA resin while cooling but below the level at which noticeable flow is induced in said PFA resin, and continuing said cooling at least until said PFA has solidified, thereafter completing said cooling and removing said pressure, whereby said PFA resin becomes fused to said body of PTFE resin at the interface therebetween.
Claim 2
Independent Claim
291 words
A method of forming a fluorocarbon resin structure in which a body of PFA resin is fused to a body of sintered PTFE resin which comprises the steps of confining a quantity of particulate PGA resin in a zone contiguous to said body of sintered PTFE resin, heating said quantity of PFA resin and at least the PTFE resin which is adjacent said zone to a temperature above the gel point of said PTFE resin and above the melting point of said PFA resin to melt said PFA resin, maintaining said elevated temperature while compacting said PFA resin against said PTFE resin under positive pressure just sufficient to urge said PFA resin melt at a very slow rate without fault producing flow therein into intimate surface contact with said PTFE resin until said former wets the surface of said latter over an area to be fused, after establishing said intimate contact, maintaining the conditions static at the fusing interface by increasing the pressure applied to said PFA resin to a predetermined level at a rate which is sufficiently slow so that there is a minimum tendency for said PFA resin to flow along the surface of said mating PTFE resin, and permitting said resins to cool slowly without force cooling toward ambient temperature while maintaining said pressure near said predetermined level where said predetermined level is chosen sufficient to prevent the formation of sinks and voids in said PFA resin while cooling but below the level at which noticeable flow is induced in said PFA resin, and continuing said cooling at least until said PFA has solidified, thereafter completing said cooling and removing said pressure, whereby said PFA resin becomes fused to said body of PTFE resin at the interface therebetween.
Claim 3
Dependent Claim
21 words
A method according to claim 1, wherein said temperature above the gel point is between about 635° F. and 710° F.
Claim 4
Dependent Claim
15 words
A method according to claim 2, wherein said positive pressure is below about 40 psi.
Claim 5
Dependent Claim
21 words
A method according to claim 3, wherein said predetermined level lies within the range of about 59 psi to 150 psi.
Claim 6
Dependent Claim
15 words
A method according to claim 4, wherein said predetermined level is above about 130 psi.
Claim 7
Dependent Claim
15 words
A method according to claim 1, wherein said positive pressure is below about 340 psi.
Claim 8
Dependent Claim
21 words
A method according to claim 6, wherein said predetermined level lies within the range of about 59 psi to 150 psi.
Claim 9
Dependent Claim
15 words
A method according to claim 7, wherein said predetermined level is above about 130 psi.
Claim 10
Dependent Claim
21 words
A method according to claim 1, wherein said predetermined level lies within the range of about 59 psi to 150 psi.
Claim 11
Dependent Claim
21 words
A method according to claim 9, wherein said temperature above the gel point is between about 635° F. and 710° F.
Claim 12
Dependent Claim
15 words
A method according to claim 10, wherein said predetermined level is above about 130 psi.
Claim 13
Dependent Claim
15 words
A method according to claim 9, wherein said predetermined level is above about 130 psi.
Claim 14
Dependent Claim
14 words
A method according to claim 1, wherein said predetermined level is about 130 psi.
Claim 15
Dependent Claim
21 words
A method according to claim 13, wherein said temperature above the gel point is between about 635° F. and 710° F.
Claim 16
Dependent Claim
15 words
A method according to claim 13, wherein said positive pressure is below about 40 psi.
Claim 17
Dependent Claim
47 words
A method according to claim 1, wherein said temperature above the gel point is between about 675° F. and 685° F., said positive pressure is between about 22 psi and 37 psi, and said predetermined level lies within the range of about 131 psi to 48 psi.
References Cited (Backward Citations)
US3206344A
Cited
US3946136A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1981-02-13 | 1981-08-15 | 1982-02-14 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1985-02-13 | 1985-08-15 | 1986-02-14 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1989-02-13 | 1989-08-15 | 1990-02-14 | $7700.00 | Window Closed / Lapsed |