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US4073729A Expired / Lapsed US ⏱️ 0.0 years remaining

Filtering process using inorganic synthetically prepared filter sand

Assignee: Wasag Chemie AG
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Filing: 1973-12-12
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Granted: 1978-02-14
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Expires: 1993-12-12
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Abstract

Abstract A process for removing solids from a liquid wherein the liquid is passed through a bed of filter media comprising discrete, inorganic, artificially produced filter sand, and wherein the artificially produced filter sand has grain densities of between about 1.0 to 2.2 grams per cubic centimeter and grain diameters of between about 0.3 and 10 mm and the grain density decreases with increasing grain diameter.

Inventors

  • 👤 Stefan Kraemer
  • 👤 Michael Seger
  • 👤 Alois Seidl

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 09:17
CPC Classifications
B; B01; B01D; B01D39/00; B01D39/02; B01D39/06; B01D2239/00; B01D2239/10; B01D2239/12; B01D2239/1241

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 244 words
In a process for removing solids from a liquid wherein said liquid is passed through a bed of filter media consisting of discrete, inorganic, artifically produced filter sand having the same chemical composition, the improvement comprising passing said liquid over artifically produced filter sand having grain densities of between about 1.0 and 2.2 grams per cubic centimeter, and grain diameters of between about 0.3 and 10 mm, wherein the grain density decreases with increasing grain diameter, backwashing said artifically produced filter sand and settling said artifically produced filter sand with sand grain diameters distributed from the largest to the smallest in the direction of liquid passage, said discrete, inorganic artifically produced filter sand consists essentially of a preliminary product mixed with a powder selected from the group consisting of amorphous particles, crystalline materials, and mixtures thereof, granulated with addition of water, dried, expanded at a temperature up to about 400° C, melting the outside at a temperature of about 700° C, and cooling to form spheres, said preliminary product produced by: (a) forming a solution containing in parts by weight about 1 part sodium silicate, having a molar ratio of Na 2 O:SiO 2 of 1:2.5 to 1:4.5, 0.02 parts to 0.8 parts of inorganic fibrous silicate or finely powdered silicate and 2-10 parts of water; (b) adding means for producing foaming gas to the solution; and (c) heating the solution to about 140° - 360° C to drive off any free water phase.
Claim 2
Dependent Claim 244 words
In a process for removing solids from a liquid wherein said liquid is passed through a bed of filter media consisting of discrete, inorganic, artifically produced filter sand having the same chemical composition, the improvement comprising passing said liquid over artifically produced filter sand having grain densities of between about 1.0 and 2.2 grams per cubic centimeter, and grain diameters of between about 0.3 and 10 mm, wherein the grain density decreases with increasing grain diameter, backwashing said artifically produced filter sand and settling said artifically produced filter sand with sand grain diameters distributed from the largest to the smallest in the direction of liquid passage, said discrete, inorganic artifically produced filter sand consists essentially of a preliminary product mixed with a powder selected from the group consisting of amorphous particles, crystalline materials, and mixtures thereof, granulated with addition of water, dried, expanded at a temperature up to about 400° C, melting the outside at a temperature of about 700° C, and cooling to form spheres, said preliminary product produced by: (a) forming a solution containing in parts by weight about 1 part sodium silicate, having a molar ratio of Na 2 O:SiO 2 of 1:2.5 to 1:4.5, 0.02 parts to 0.8 parts of inorganic fibrous silicate or finely powdered silicate and 2-10 parts of water; (b) adding means for producing foaming gas to the solution; and (c) heating the solution to about 140° - 360° C to drive off any free water phase.
Claim 3
Dependent Claim 65 words
The process of claim 1, wherein said powder is finely ground with said preliminary product in a ratio by weight of about 2 to 6:1; granulated with the addition of water, dried, expanded at a temperature of up to about 400° C and melted above 700° C to form spheres having a density of between about 1.0 and 2.2 g/cm 3 in one operating step.
Claim 4
Dependent Claim 25 words
The process of claim 2, further comprising the addition of a separating agent to said fine grinding step to produce spheres with a rough surface.
Claim 5
Dependent Claim 25 words
The process of claim 3, wherein said separating agent is selected from the group consisting of chalk, kieselguhr, ground slag, ground limestone and dolomite meal.
Claim 6
Dependent Claim 39 words
The process of claim 2, further comprising the addition of about 0.1 to 5 percent by weight of a binder selected from the group consisting of sodium silicate and polyvinyl alcohol to the water added before the granulation step.
Claim 7
Dependent Claim 44 words
The process of claim 2, wherein said granulated material is dried at temperatures between about 400° C and 700° C to expand the granulated material to spheres and melted above about 700° C to contract the spheres with partial loss of the porous structure.
Claim 8
Dependent Claim 22 words
The process of claim 1, wherein said crystalline materials are selected from the group consisting of ground quartz and crushed natural silicate.
Claim 9
Dependent Claim 27 words
The process of claim 1, wherein said amorphous materials are selected from the group consisting of ground slag, fly ash, ground pumice, ground basalt and crushed lava.
Claim 10
Dependent Claim 189 words
In a process for removing solids from a liquid wherein said liquid is passed through a bed of filter media consisting of discrete, inorganic, artificially produced filter sand having the same chemical composition, the improvement comprising passing said liquid over artifically produced filter sand having grain densities of between about 1.0 and 2.2 grams per cubic centimeter, and grain diameters of between about 0.3 and 10 mm, wherein the grain density decreases with increasing grain diameter, backwashing said artificially produced filter sand and settling said artificially produced filter sand with said grain diameters distributed from the largest to the smallest in the direction of liquid passage said discrete, inorganic, artifically produced filter sand consists essentially of a preliminary product mixed with a powder selected from the group consisting ofamorphous particles, crystalline materials and mixtures thereof, granulated with addition of water, dried, expanded at a temperature up to about 400° C, melting the outisde at a temperature above 700° C, cooling to form spheres, said preliminary product produced by finely grinding a window glass composition and mixing therewith about 0.3 to 1.5 percent by weight of a carbonaceous foaming agent.
Claim 11
Dependent Claim 189 words
In a process for removing solids from a liquid wherein said liquid is passed through a bed of filter media consisting of discrete, inorganic, artificially produced filter sand having the same chemical composition, the improvement comprising passing said liquid over artifically produced filter sand having grain densities of between about 1.0 and 2.2 grams per cubic centimeter, and grain diameters of between about 0.3 and 10 mm, wherein the grain density decreases with increasing grain diameter, backwashing said artificially produced filter sand and settling said artificially produced filter sand with said grain diameters distributed from the largest to the smallest in the direction of liquid passage said discrete, inorganic, artifically produced filter sand consists essentially of a preliminary product mixed with a powder selected from the group consisting ofamorphous particles, crystalline materials and mixtures thereof, granulated with addition of water, dried, expanded at a temperature up to about 400° C, melting the outisde at a temperature above 700° C, cooling to form spheres, said preliminary product produced by finely grinding a window glass composition and mixing therewith about 0.3 to 1.5 percent by weight of a carbonaceous foaming agent.

References Cited (Backward Citations)

US293745A Cited
US3184371A Cited
US3235635A Cited
US3343680A Cited
US3471025A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-02-13 1981-08-15 1982-02-14 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-02-13 1985-08-15 1986-02-14 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-02-13 1989-08-15 1990-02-14 $7700.00 Window Closed / Lapsed

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