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Method for recovering palladium from spent palladium catalysts

Assignee: University of Chemistry and Technology
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Filing: 1976-12-17
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Granted: 1978-02-07
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Expires: 1996-12-17
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Abstract

Abstract A technique for recovering palladium from a spent palladium catalyst or ash thereof involves fluorinating the catalyst or ash at elevated temperatures to yield palladium fluoride and decomposing the fluoride with a mineral acid at a temperature ranging from 90° - 100° C.

Inventors

  • 👤 Ludek Vodicka
  • 👤 Ivo Peka
  • 👤 Voktor Suchy

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 12:38
CPC Classifications
C; C01; C01G; C01G55/00; C01G55/005; C22; C22B; C22B11/00

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 60 words
A method for recovering palladium values from spent palladium catalysts and ash thereof which comprises the steps of fluorinating the spent catalyst and ash at a temperature which increases gradually from 200° - 500° C and decomposing palladium fluorides so obtained with a mineral acid at a temperature ranging from 90° - 100° C to obtain palladium values in solution.
Claim 2
Independent Claim 60 words
A method for recovering palladium values from spent palladium catalysts and ash thereof which comprises the steps of fluorinating the spent catalyst and ash at a temperature which increases gradually from 200° - 500° C and decomposing palladium fluorides so obtained with a mineral acid at a temperature ranging from 90° - 100° C to obtain palladium values in solution.
Claim 3
Dependent Claim 13 words
Method in accordance with claim 1, wherein fluorination is effected with elemental fluorine.
Claim 4
Dependent Claim 18 words
Method in accordance with claim 1, wherein fluorination is effected with a mixture of fluorine and hydrogen fluoride.
Claim 5
Dependent Claim 13 words
Method in accordance with claim 1, wherein the mineral acid is hydrochloric acid.
Claim 6
Dependent Claim 13 words
Method in accordance with claim 3, wherein the mineral acid is hydrochloric acid.

References Cited (Backward Citations)

US3969267A Cited
US3958985A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-02-06 1981-08-08 1982-02-07 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-02-06 1985-08-08 1986-02-07 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-02-06 1989-08-08 1990-02-07 $7700.00 Window Closed / Lapsed

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