US4069310A — Method for the manufacture of clear dentifrices

Claim 1

Independent Claim 161 words

A method for the manufacture of a visually clear, bubble-free dentifrice comprising a vacuum deareated synthetic inorganic complex silicate clay gelling agent of the formula [Si.sub.8 Mg.sub.5.1 Li.sub.0.6 H.sub.7.6 O.sub.24 ].sup.0.6.spsp.- Na.sup.+.sub.0.6 , a dentally acceptable substantially water-insoluble polishing agent having a refractive index of about 1.44 to 1.48, water, sorbitol and glycerine, with the proportion of such dentifrice components being about 1 to 5% of such gelling agent, about 5 to 50% of such polishing agent, about 5 to 30% of water, about 20 to 75% of sorbitol and at least 5% of glycerine, with the total of water, sorbitol and glycerine being about 30 to 94%, which comprises high shear mixing said deaerated gelling agent, heated to about 90° C. for about 15 minutes, 40° C. for one hour or unheated at room temperature for 16 hours, with water and sorbitol to produce a clear gel and admixing glycerine with the clear gel to make a clear water-sorbitol-glycerine gel.

Claim 2

Independent Claim 161 words

A method for the manufacture of a visually clear, bubble-free dentifrice comprising a vacuum deareated synthetic inorganic complex silicate clay gelling agent of the formula [Si.sub.8 Mg.sub.5.1 Li.sub.0.6 H.sub.7.6 O.sub.24 ].sup.0.6.spsp.- Na.sup.+.sub.0.6 , a dentally acceptable substantially water-insoluble polishing agent having a refractive index of about 1.44 to 1.48, water, sorbitol and glycerine, with the proportion of such dentifrice components being about 1 to 5% of such gelling agent, about 5 to 50% of such polishing agent, about 5 to 30% of water, about 20 to 75% of sorbitol and at least 5% of glycerine, with the total of water, sorbitol and glycerine being about 30 to 94%, which comprises high shear mixing said deaerated gelling agent, heated to about 90° C. for about 15 minutes, 40° C. for one hour or unheated at room temperature for 16 hours, with water and sorbitol to produce a clear gel and admixing glycerine with the clear gel to make a clear water-sorbitol-glycerine gel.

Claim 3

Independent Claim 132 words

A method for the manufacture of a visually clear dentifrice comprising a synthetic inorganic complex silicate clay gelling agent of the formula [Si.sub.8 Mg.sub.5.1 Li.sub.0.6 H.sub.7.6 O.sub.24 ].sup.0.6.spsp.- Na.sup.+.sub.0.6, a dentally acceptable substantially water-insoluble polishing agent having a refractive index of about 1.44 to 1.48, water, sorbitol and glycerine, with the proportion of such dentifrice components being about 1 to 5% of such gelling agent, about 5 to 50% of such polishing agent, about 5 to 30% of water, about 20 to 75% of sorbitol and at least 5% of glycerine, with the total of water, sorbitol and glycerine being about 30 to 94%, which comprises mixing said gelling agent with water and sorbitol to produce a clear gel and admixing glycerine with the clear gel to make a clear water-sorbitol-glycerine gel.

Claim 4

Independent Claim 132 words

A method for the manufacture of a visually clear dentifrice comprising a synthetic inorganic complex silicate clay gelling agent of the formula [Si.sub.8 Mg.sub.5.1 Li.sub.0.6 H.sub.7.6 O.sub.24 ].sup.0.6.spsp.- Na.sup.+.sub.0.6, a dentally acceptable substantially water-insoluble polishing agent having a refractive index of about 1.44 to 1.48, water, sorbitol and glycerine, with the proportion of such dentifrice components being about 1 to 5% of such gelling agent, about 5 to 50% of such polishing agent, about 5 to 30% of water, about 20 to 75% of sorbitol and at least 5% of glycerine, with the total of water, sorbitol and glycerine being about 30 to 94%, which comprises mixing said gelling agent with water and sorbitol to produce a clear gel and admixing glycerine with the clear gel to make a clear water-sorbitol-glycerine gel.

Claim 5

Dependent Claim 126 words

A method according to claim 2 wherein the dentifrice composition commprises 1 to 3% of the gelling agent, 10 to 30% of the polishing agent, 5 to 20% of water, 25 to 50% of sorbitol, 15 to 35% of glycerine and 0.05 to 5% or organic surface active agent, the polishing agent is selected from the group consisting of colloidal silica, amorphous silicic anhydride and amorphous complex aluminosilicates, and mixtures thereof, and has a refractive index in the range of 1.44 to 1.48, and the gelling agent is mixed with an aqueous solution of sorbitol to produce the clear gel, after which glycerine is admixed with the clear gel and with the product resulting there are subsequently admixed the polishing agent and organic surface active agent.

Claim 6

Dependent Claim 69 words

A method according to claim 3 wherein the polishing agent is a mixture of amorphous silicic anhydride and synthetic amorphous complex sodium aluminosilicate, the gel comprising gelling agent, water, sorbitol and glycerine is subjected to vacuum to deaerate it and subsequently a deaerated mixture of the amorphous silicic anhydride and synthetic amorphous complex sodium aluminosilicate is vigorously mixed with the other dental gel components to produce a clear gel.

Claim 7

Dependent Claim 34 words

A method according to claim 3 wherein the clear gel of sorbitol, water and gelling agent is made by high shear mixing and the clear gel produced is deaerated by mixing thereof under vacuum.

Claim 8

Dependent Claim 51 words

A method according to claim 4 wherein the gelling agent is free of gelation-promoting electrolyte, the surface active agent is a sodium N-higher fatty acyl sarcoside, sodium saccharin is present as a sweetener and there is present in the sarcoside and saccharin sufficient electrolyte to promote gelation of the gelling agent.

Annuity Stage	Window Opens	Payment Deadline	Surcharge Period Until	Estimated Fee	Status
3.5 Years (Year 4)	1981-01-16	1981-07-18	1982-01-17	$2000.00	Window Closed / Lapsed
7.5 Years (Year 8)	1985-01-16	1985-07-18	1986-01-17	$3760.00	Window Closed / Lapsed
11.5 Years (Year 12)	1989-01-16	1989-07-18	1990-01-17	$7700.00	Window Closed / Lapsed

Method for the manufacture of clear dentifrices

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