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US4069175A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for producing dimensionally stable urea-formaldehyde foams

Assignee: Waverly Chemical Co
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Filing: 1977-01-21
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Granted: 1978-01-17
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Expires: 1997-01-21
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Abstract

Abstract Method of producing a dimensionally stabilized urea-formaldehyde foam which comprises preparing a neutral concentrated partially cured aqueous urea-formaldehyde resin, combining said neutral resin with a froth produced by forcing air through a dilute acidic aqueous surfactant solution to activate the urea-formaldehyde foam cure, immediately thereafter combining the curing urea-formaldehyde foam with a substantially non-ionic liquid additive containing dissolved urea and suspended linearly shaped refractory solid particles, completing the acid catalyzed foam cure, and drying. Foam dimensional stability is maximized when the non-ionic liquid additive contains 10-20% by weight dissolved urea and 10-20% by weight suspended attapulgite clay.

Inventors

  • 👤 William Percy Moore

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 08:35
CPC Classifications
C; C08; C08J; C08J9/00; C08J9/30; C08J2361/00; C08J2361/20; C08J2361/22; C08J2361/24; Y; Y10; Y10S; Y10S521/00; Y10S521/911; Y10S521/917

Claims Analysis

Total Claims: 2
Claim 1
Independent Claim 127 words
A method for producing dimensionally stable urea-formaldehyde foam which comprises an aqueous neutral urea-formaldehyde resin having a formaldehyde to urea mol ratio of about 2, a viscosity of about 40 centipoise and a solids content between 40 and 65%, combining the said resin with frothed curing solution containing about 1% sulfuric acid and about 2% surfactant and having an electrical conductivity of at least 0.1 ohm -1 centimeter -1 , continuously blending the combined resin and curing solution foam with a substantially un-ionized liquid suspension having an electrical conductivity lower than 0.00001 ohms -1 centimeter -1 and containing between 10 and 25% attapulgite clay sized to pass through a 325 mesh Tyler Screen, curing and drying the combined foam at temperatures between 0° C and 35° C.
Claim 2
Independent Claim 127 words
A method for producing dimensionally stable urea-formaldehyde foam which comprises an aqueous neutral urea-formaldehyde resin having a formaldehyde to urea mol ratio of about 2, a viscosity of about 40 centipoise and a solids content between 40 and 65%, combining the said resin with frothed curing solution containing about 1% sulfuric acid and about 2% surfactant and having an electrical conductivity of at least 0.1 ohm -1 centimeter -1 , continuously blending the combined resin and curing solution foam with a substantially un-ionized liquid suspension having an electrical conductivity lower than 0.00001 ohms -1 centimeter -1 and containing between 10 and 25% attapulgite clay sized to pass through a 325 mesh Tyler Screen, curing and drying the combined foam at temperatures between 0° C and 35° C.

References Cited (Backward Citations)

US2273367A Cited
US2947647A Cited
US3457199A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1981-01-16 1981-07-18 1982-01-17 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1985-01-16 1985-07-18 1986-01-17 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1989-01-16 1989-07-18 1990-01-17 $7700.00 Window Closed / Lapsed

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