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US4048295A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for making extrudates from aluminum oxyhydrates

Assignee: Wintershall Dea International AG
•
Filing: 1975-12-16
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Granted: 1977-09-13
•
Expires: 1995-12-16
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Abstract

Abstract Formed products are made from aqueous aluminum oxyhydrate by peptizing the aqueous aluminum oxyhydrate with an acid and then subsequently adding a dilute solution of ammonia or an ammonia yielding compound following by extrusion, drying and calcining.

Inventors

  • 👤 Martin Wassermann
  • 👤 Arnold Meyer

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-06 16:28
CPC Classifications
B; B01; B01J; B01J37/00; B01J37/0009; B01J21/00; B01J21/02; B01J21/04; C; C01; C01F; C01F7/00; C01F7/02; C01F7/021; C01F7/025; C04; C04B; C04B35/00; C04B35/01; C04B35/10; C01P; C01P2004/00; C01P2004/60; C01P2004/61; C01P2006/00; C01P2006/11; C01P2006/12; C01P2006/14; C01P2006/16; C01P2006/17; C01P2006/21

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 145 words
A process consisting essentially of peptizing with an aqueous acid selected from the group consisting of nitric acid, acetic acid, citric acid, hydrochloric acid, sulfuric acid, formic acid, propionic acid, monochloracetic acid, dichloroacetic acid and trichloroacetic acid at a concentration of 0.3 to 10% a Boehmite aluminum oxyhydrate containing 65 to 85% by weight Al 2 O 3 , a bulk density of 500 to 700 g/l, a B.E.T. specific surface area of 140 to 300 m 2 /g and an average particle size below 100 microns, then adding an aqueous solution of ammonia or an ammonia liberating compound having a concentration of 0.1 to 3%, there being employed 50 to 70 parts of acid solution and 35 to 50 parts of ammonia solution per 100 parts of aluminum oxyhydrate, to form an extrudable mass, extruding said extrudable mass, drying and then calcining the extrudate.
Claim 2
Dependent Claim 145 words
A process consisting essentially of peptizing with an aqueous acid selected from the group consisting of nitric acid, acetic acid, citric acid, hydrochloric acid, sulfuric acid, formic acid, propionic acid, monochloracetic acid, dichloroacetic acid and trichloroacetic acid at a concentration of 0.3 to 10% a Boehmite aluminum oxyhydrate containing 65 to 85% by weight Al 2 O 3 , a bulk density of 500 to 700 g/l, a B.E.T. specific surface area of 140 to 300 m 2 /g and an average particle size below 100 microns, then adding an aqueous solution of ammonia or an ammonia liberating compound having a concentration of 0.1 to 3%, there being employed 50 to 70 parts of acid solution and 35 to 50 parts of ammonia solution per 100 parts of aluminum oxyhydrate, to form an extrudable mass, extruding said extrudable mass, drying and then calcining the extrudate.
Claim 3
Dependent Claim 24 words
The process of claim 1 wherein the ammonia liberating compound is selected from the group consisting of ammonium carbonate, ammonium bicarbonate, urea and hexamethylenetetramine.
Claim 4
Dependent Claim 10 words
The process of claim 1 wherein there is used ammonia.
Claim 5
Dependent Claim 11 words
The process of claim 3 wherein the acid is nitric acid.
Claim 6
Dependent Claim 19 words
The process of claim 1 wherein the aluminum oxyhydrate employed has been prepared by hydrolysis of an aluminum alkoxide.
Claim 7
Dependent Claim 17 words
The process of claim 1 wherein there is employed ammonia having a concentration of 0.1 to 3%.
Claim 8
Dependent Claim 11 words
The process of claim 6 wherein the ammonia concentration is 0.5%.
Claim 9
Dependent Claim 16 words
The process of claim 6 wherein the acid is nitric acid of 2 to 3% concentration.
Claim 10
Dependent Claim 16 words
The process of claim 6 wherein the acid is acetic acid of 0.5 to 1.5% concentration.
Claim 11
Dependent Claim 16 words
The process of claim 6 wherein the acid is citric acid of 1.5 to 2.5% concentration.

References Cited (Backward Citations)

US3385663A Cited
US3808153A Cited
US3945945A Cited
US3839230A Cited
US3975510A Cited
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US3975509A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-09-12 1981-03-14 1981-09-13 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-09-12 1985-03-14 1985-09-13 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-09-12 1989-03-14 1989-09-13 $7700.00 Window Closed / Lapsed

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