Patent US4046846A successfully refreshed from Google Patents.
US4046846A
Expired / Lapsed
US
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Method of producing hard foamed materials
Assignee: Individual
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Filing: 1974-08-14
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Granted: 1977-09-06
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Expires: 1994-08-14
Abstract
Abstract A hard foamed material having a small specific gravity and a high mechanical strength is produced by mixing vinyl chloride resin with a large amount of inorganic powdery substances and a solvent, heating and kneading the resulting mixture in a closed kneader at a given temperature, adding a liquefied butane with a solvent thereto, and heating and foaming the resulting mixture in a mold.
Inventors
- 👤 Tokuzo Fujimori
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-30 15:18
CPC Classifications
C; C08; C08J; C08J9/00; C08J9/04; C08J9/12; C08J9/127; C08J9/0066; C08K; C08K3/00; C08K3/18; C08K3/20; C08K3/22; C08K3/24; C08K3/26; C08K3/34; C08K7/00; C08K7/22; C08K7/24; C08K7/26; C08J2203/00; C08J2203/14; C08J2327/00; C08J2327/02; C08J2327/04; C08J2327/06; Y; Y10; Y10S; Y10S264/00; Y10S264/05; Y10S264/13; Y10S264/17; Y10S521/00; Y10S521/907
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
226 words
In the method of producing hard foamed objects of expanded vinyl chloride resin which comprises forming a mixture comprised of said vinyl chloride resin and a blowing agent; introducing the mixture into a mold; pressurizing the mold while heating the mold to cause the blowing agent to partially expand the resulting resin mixture to fill said mold; cooling said mold; removing the resulting object from said mold and then heating the object to further expand its size without changing its shape, the improvement which comprises: forming a dry mixture of said resin with about 0.4 to about 40 times by weight of the resin of a powdery inorganic filler, adding to the dry mixture at least about 30 parts by weight of said mixture of a solvent selected from toluene and xylene, kneading the solvent, resin and inorganic filler containing mixture in a closed kneader at about 40° to about 100° C. until the outer surfaces of the particles of said inorganic filler are covered with said resin and are adhered to each other by said resin, adding a blowing agent comprised of liquid butane, and an additional amount of about 30 to about 40 parts by weight of said solvent, thoroughly mixing the resulting mixture so that all the ingredients including the liquid butane are thoroughly dispersed and then introducing said mixture into said mold.
Claim 2
Dependent Claim
226 words
In the method of producing hard foamed objects of expanded vinyl chloride resin which comprises forming a mixture comprised of said vinyl chloride resin and a blowing agent; introducing the mixture into a mold; pressurizing the mold while heating the mold to cause the blowing agent to partially expand the resulting resin mixture to fill said mold; cooling said mold; removing the resulting object from said mold and then heating the object to further expand its size without changing its shape, the improvement which comprises: forming a dry mixture of said resin with about 0.4 to about 40 times by weight of the resin of a powdery inorganic filler, adding to the dry mixture at least about 30 parts by weight of said mixture of a solvent selected from toluene and xylene, kneading the solvent, resin and inorganic filler containing mixture in a closed kneader at about 40° to about 100° C. until the outer surfaces of the particles of said inorganic filler are covered with said resin and are adhered to each other by said resin, adding a blowing agent comprised of liquid butane, and an additional amount of about 30 to about 40 parts by weight of said solvent, thoroughly mixing the resulting mixture so that all the ingredients including the liquid butane are thoroughly dispersed and then introducing said mixture into said mold.
Claim 3
Dependent Claim
29 words
The method of claim 1 wherein the inorganic filler is selected from carbonates, sulfates, silicates, oxides and hydroxides of calcium, magnesium and aluminum; talc, bentonite, clay and mixtures thereof.
Claim 4
Dependent Claim
25 words
The method of claim 1 wherein not less than 90% of the inorganic filler has a particle size which passes through a 200 mesh sieve.
Claim 5
Dependent Claim
28 words
The method of claim 1 in which about 2% to about 15% by weight of the total mixture of a fireproofing agent is added to the dry mixture.
Claim 6
Dependent Claim
33 words
The method of claim 1 wherein the liquid butane is added in an amount of about 10 to about 20 parts by weight of the mixture of vinyl chloride resin and inorganic filler.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-09-05 | 1981-03-07 | 1981-09-06 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-09-05 | 1985-03-07 | 1985-09-06 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-09-05 | 1989-03-07 | 1989-09-06 | $7700.00 | Window Closed / Lapsed |