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US4046846A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of producing hard foamed materials

Assignee: Individual
•
Filing: 1974-08-14
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Granted: 1977-09-06
•
Expires: 1994-08-14
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Abstract

Abstract A hard foamed material having a small specific gravity and a high mechanical strength is produced by mixing vinyl chloride resin with a large amount of inorganic powdery substances and a solvent, heating and kneading the resulting mixture in a closed kneader at a given temperature, adding a liquefied butane with a solvent thereto, and heating and foaming the resulting mixture in a mold.

Inventors

  • 👤 Tokuzo Fujimori

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 15:18
CPC Classifications
C; C08; C08J; C08J9/00; C08J9/04; C08J9/12; C08J9/127; C08J9/0066; C08K; C08K3/00; C08K3/18; C08K3/20; C08K3/22; C08K3/24; C08K3/26; C08K3/34; C08K7/00; C08K7/22; C08K7/24; C08K7/26; C08J2203/00; C08J2203/14; C08J2327/00; C08J2327/02; C08J2327/04; C08J2327/06; Y; Y10; Y10S; Y10S264/00; Y10S264/05; Y10S264/13; Y10S264/17; Y10S521/00; Y10S521/907

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 226 words
In the method of producing hard foamed objects of expanded vinyl chloride resin which comprises forming a mixture comprised of said vinyl chloride resin and a blowing agent; introducing the mixture into a mold; pressurizing the mold while heating the mold to cause the blowing agent to partially expand the resulting resin mixture to fill said mold; cooling said mold; removing the resulting object from said mold and then heating the object to further expand its size without changing its shape, the improvement which comprises: forming a dry mixture of said resin with about 0.4 to about 40 times by weight of the resin of a powdery inorganic filler, adding to the dry mixture at least about 30 parts by weight of said mixture of a solvent selected from toluene and xylene, kneading the solvent, resin and inorganic filler containing mixture in a closed kneader at about 40° to about 100° C. until the outer surfaces of the particles of said inorganic filler are covered with said resin and are adhered to each other by said resin, adding a blowing agent comprised of liquid butane, and an additional amount of about 30 to about 40 parts by weight of said solvent, thoroughly mixing the resulting mixture so that all the ingredients including the liquid butane are thoroughly dispersed and then introducing said mixture into said mold.
Claim 2
Dependent Claim 226 words
In the method of producing hard foamed objects of expanded vinyl chloride resin which comprises forming a mixture comprised of said vinyl chloride resin and a blowing agent; introducing the mixture into a mold; pressurizing the mold while heating the mold to cause the blowing agent to partially expand the resulting resin mixture to fill said mold; cooling said mold; removing the resulting object from said mold and then heating the object to further expand its size without changing its shape, the improvement which comprises: forming a dry mixture of said resin with about 0.4 to about 40 times by weight of the resin of a powdery inorganic filler, adding to the dry mixture at least about 30 parts by weight of said mixture of a solvent selected from toluene and xylene, kneading the solvent, resin and inorganic filler containing mixture in a closed kneader at about 40° to about 100° C. until the outer surfaces of the particles of said inorganic filler are covered with said resin and are adhered to each other by said resin, adding a blowing agent comprised of liquid butane, and an additional amount of about 30 to about 40 parts by weight of said solvent, thoroughly mixing the resulting mixture so that all the ingredients including the liquid butane are thoroughly dispersed and then introducing said mixture into said mold.
Claim 3
Dependent Claim 29 words
The method of claim 1 wherein the inorganic filler is selected from carbonates, sulfates, silicates, oxides and hydroxides of calcium, magnesium and aluminum; talc, bentonite, clay and mixtures thereof.
Claim 4
Dependent Claim 25 words
The method of claim 1 wherein not less than 90% of the inorganic filler has a particle size which passes through a 200 mesh sieve.
Claim 5
Dependent Claim 28 words
The method of claim 1 in which about 2% to about 15% by weight of the total mixture of a fireproofing agent is added to the dry mixture.
Claim 6
Dependent Claim 33 words
The method of claim 1 wherein the liquid butane is added in an amount of about 10 to about 20 parts by weight of the mixture of vinyl chloride resin and inorganic filler.

References Cited (Backward Citations)

US2525965A Cited
US2525880A Cited
US2498074A Cited
US2692863A Cited
FR1321630A Cited
US3306960A Cited
US3812225A Cited
US3846523A Cited
US3812224A Cited
US3773873A Cited
US3912667A Cited
US3911070A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-09-05 1981-03-07 1981-09-06 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-09-05 1985-03-07 1985-09-06 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-09-05 1989-03-07 1989-09-06 $7700.00 Window Closed / Lapsed

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