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US4043507A Expired / Lapsed US ⏱️ 0.0 years remaining

Apparatus for the formation of liquid droplets

Assignee: United Kingdom Atomic Energy Authority
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Filing: 1974-11-01
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Granted: 1977-08-23
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Expires: 1994-11-01
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Abstract

Abstract There is disclosed an apparatus and method for the production of particles wherein liquid droplets, to be formed into particles, are produced by the ejection of liquid out of the orifices of a spinnerette which is vibrated.

Inventors

  • 👤 Peter Frederick Wace

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 12:02
CPC Classifications
B; B01; B01J; B01J2/00; B01J2/02; B01J2/06; B01J2/08; C; C01; C01G; C01G43/00; C01G43/01; C01G43/025; C01P; C01P2004/00; C01P2004/30; C01P2004/32

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 97 words
Apparatus for the formation of liquid droplets comprising: ejection means for ejecting downwardly a plurality of continuously moving jets of liquid, said ejection means comprising a lightweight dropping head in the form of a spinnerette having a plurality of orifices of highly uniform and accurate orifice size and position, and break-up means for breaking up the continuously moving jets leaving the orifices, into short lengths which then form into droplets subsequent to their formation into short lengths, said break-up means comprising a means for vibrating the spinnerette as the said continuously moving liquid jets are issuing therefrom.
Claim 2
Dependent Claim 97 words
Apparatus for the formation of liquid droplets comprising: ejection means for ejecting downwardly a plurality of continuously moving jets of liquid, said ejection means comprising a lightweight dropping head in the form of a spinnerette having a plurality of orifices of highly uniform and accurate orifice size and position, and break-up means for breaking up the continuously moving jets leaving the orifices, into short lengths which then form into droplets subsequent to their formation into short lengths, said break-up means comprising a means for vibrating the spinnerette as the said continuously moving liquid jets are issuing therefrom.
Claim 3
Dependent Claim 45 words
Apparatus according to claim 1, wherein the orifices are located in an essentially horizontal plane, and wherein said means for vibrating comprises means for vibrating the spinnerette linearly transversely or axially with respect to the plane of the orifices while maintaining said plane essentially horizontal.
Claim 4
Dependent Claim 21 words
Apparatus according to claim 1, wherein the means for vibrating the spinnerette is an electromagnetic vibrator mechanically connected to the spinnerette.
Claim 5
Dependent Claim 154 words
Apparatus for the production of particles of uniform size by gelling of droplets of liquid, comprising: ejection means for ejecting downwardly a plurality of continuously moving jets of liquid, said ejection means comprising a lightweight dropping head in the form of a spinnerette having a plurality of orifices of highly uniform and accurate orifice size and position, and including break-up means for breaking up the continuously moving jets leaving the orifices, into short lengths, said break-up means comprising a means for vibrating the spinnerette as the said continuously moving liquid jets issue therefrom, and including means for supplying a liquid to be gelled to the spinnerette and, in association with the spinnerette, a column for containing a reagent capable of causing the liquid to be gelled to gel, the column being spaced downwardly from the spinnerette a sufficient distance to permit the said short lengths to form into droplets before passing into the column.
Claim 6
Dependent Claim 154 words
Apparatus for the production of particles of uniform size by gelling of droplets of liquid, comprising: ejection means for ejecting downwardly a plurality of continuously moving jets of liquid, said ejection means comprising a lightweight dropping head in the form of a spinnerette having a plurality of orifices of highly uniform and accurate orifice size and position, and including break-up means for breaking up the continuously moving jets leaving the orifices, into short lengths, said break-up means comprising a means for vibrating the spinnerette as the said continuously moving liquid jets issue therefrom, and including means for supplying a liquid to be gelled to the spinnerette and, in association with the spinnerette, a column for containing a reagent capable of causing the liquid to be gelled to gel, the column being spaced downwardly from the spinnerette a sufficient distance to permit the said short lengths to form into droplets before passing into the column.
Claim 7
Dependent Claim 19 words
Apparatus according to claim 4, wherein the column is arranged to contain a gaseous reagent and a liquid reagent.
Claim 8
Dependent Claim 21 words
Apparatus according to claim 4, wherein the means for vibrating the spinnerette is an electromagnetic vibrator mechanically connected to the spinnerette.
Claim 9
Dependent Claim 23 words
Apparatus according to claim 4, wherein said column comprises means for inhibiting the release of reagent gas from the top of the column.
Claim 10
Independent Claim 73 words
A method for forming liquid droplets comprising: ejecting downwardly a plurality of jets of liquid by passing the liquid continuously through a plurality of orifices of a light-weight dropping head in the form of a spinnerette, and breaking up the continuously moving liquid jets into short lengths by vibrating the spinnerette to vibrate the jets passing therethrough, and subsequently forming the short lengths into droplets by falling downwardly after said breaking up step.
Claim 11
Independent Claim 73 words
A method for forming liquid droplets comprising: ejecting downwardly a plurality of jets of liquid by passing the liquid continuously through a plurality of orifices of a light-weight dropping head in the form of a spinnerette, and breaking up the continuously moving liquid jets into short lengths by vibrating the spinnerette to vibrate the jets passing therethrough, and subsequently forming the short lengths into droplets by falling downwardly after said breaking up step.
Claim 12
Dependent Claim 54 words
A method according to claim 8, wherein the liquid is a liquid to be gelled, and including the step of supplying said liquid to the spinnerette for said ejection into liquid jets, and including contacting the droplets thus formed with a reagent capable of gelling the liquid to thus cause the droplets to gel.
Claim 13
Dependent Claim 33 words
A method according to claim 9, wherein the droplets are partially gelled by contacting a gaseous reagent and are then contacted with a liquid reagent wherein the gelling of the droplets is completed.
Claim 14
Dependent Claim 20 words
A method according to claim 10, wherein ammonia gas is the gaseous reagent and ammonium hydroxide is the liquid reagent.
Claim 15
Dependent Claim 18 words
A method according to claim 9, wherein the liquid droplets to be gelled contain a nuclear fuel material.

References Cited (Backward Citations)

US3085749A Cited
GB977128A Cited
US3361352A Cited
US3256677A Cited
US3458135A Cited
US3709432A Cited
US3739393A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-08-22 1981-02-21 1981-08-23 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-08-22 1985-02-21 1985-08-23 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-08-22 1989-02-21 1989-08-23 $7700.00 Window Closed / Lapsed

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