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US4039828A Expired / Lapsed US ⏱️ 0.0 years remaining

Quadrupole mass spectrometer

Assignee: Uranit GmbH
•
Filing: 1974-12-13
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Granted: 1977-08-02
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Expires: 1994-12-13
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Abstract

Abstract In a quadrupole mass spectrometer enclosed by a high vacuum container and including an ionization chamber, a molecular beam radiator passing through the container and having an output opening for supplying the gas to be analyzed, and a cryopump arranged for receiving the molecular beam exiting from the output opening and serving as a radiation trap, the output opening of the radiator and the cryopump are disposed at the periphery of the ionization chamber preferably diametrically opposite one another.

Inventors

  • 👤 Jochen Pokar
  • 👤 Horst Putter

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 14:27
CPC Classifications
H; H01; H01J; H01J49/00; H01J49/02; H01J49/04; H01J49/0468

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 166 words
In a quadrupole mass spectrometer enclosed by a high vacuum container and including an ionization chamber enclosing an ionization region in which gas molecules are ionized, an ion source located outside of the ionization chamber and separated from the ionization region, a molecular beam radiator passing through the container and having an output opening for supplying the gas to be ionized in the ionization region and to be analyzed, and a cryopump arranged for receiving the molecular beam exiting from the output opening and serving as a radiation trap, the improvement wherein said output opening of said radiator and said cryopump are disposed at the periphery of said ionization chamber and said cryopump is located in line with the molecular beam exiting from said output opening, and said spectrometer further comprises a second cryopump enclosing said molecular beam radiator, a cathode, and a coolable heat shield between said cathode and said ionization chamber and kept at a low temperature level by connecting it with said cryopumps.
Claim 2
Dependent Claim 166 words
In a quadrupole mass spectrometer enclosed by a high vacuum container and including an ionization chamber enclosing an ionization region in which gas molecules are ionized, an ion source located outside of the ionization chamber and separated from the ionization region, a molecular beam radiator passing through the container and having an output opening for supplying the gas to be ionized in the ionization region and to be analyzed, and a cryopump arranged for receiving the molecular beam exiting from the output opening and serving as a radiation trap, the improvement wherein said output opening of said radiator and said cryopump are disposed at the periphery of said ionization chamber and said cryopump is located in line with the molecular beam exiting from said output opening, and said spectrometer further comprises a second cryopump enclosing said molecular beam radiator, a cathode, and a coolable heat shield between said cathode and said ionization chamber and kept at a low temperature level by connecting it with said cryopumps.
Claim 3
Dependent Claim 46 words
A system as defined in claim 1 wherein said molecular beam radiator and the said cryopump are disposed diametrically opposite one another, and the longitudinal axis of said molecular beam radiator is approximately perpendicular to the longitudinal axis of the quadrupole rod system of said spectrometer.
Claim 4
Dependent Claim 25 words
A system as defined in claim 2 further comprising means defining a molecular beam aperture disposed between said molecular beam radiator and said ionization chamber.
Claim 5
Dependent Claim 35 words
A system as defined in claim 1 further comprising means maintaining said output opening of said molecular beam radiator at the same electrical potential as the portions of said system which border said ionization chamber.
Claim 6
Dependent Claim 41 words
A system as defined in claim 4 wherein said radiator is made of a plastic material which is resistant to the medium to be analyzed or of a ceramic material, and said output opening is provided with an electrically conductive layer.
Claim 7
Dependent Claim 24 words
A system as defined in claim 5 wherein said radiator is made of plastic material selected from the group consisting of polytrifluorochloroethylene and polytetrafluoroethylene.
Claim 8
Dependent Claim 15 words
A system as defined in claim 5 wherein said radiator is made of aluminum oxide.
Claim 9
Dependent Claim 29 words
A system as defined in claim 5 wherein said molecular beam radiator is fastened to said container to be adjustable in its position with respect to said ionization chamber.

References Cited (Backward Citations)

US3142752A Cited
US3418513A Cited
US3313935A Cited
US3553451A Cited
US3770954A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-08-01 1981-01-31 1981-08-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-08-01 1985-01-31 1985-08-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-08-01 1989-01-31 1989-08-02 $7700.00 Window Closed / Lapsed

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