Patent US4036694A successfully refreshed from Google Patents.
US4036694A
Expired / Lapsed
US
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Process for beet sugar production
Assignee: Hokkaido Sugar Co Ltd
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Filing: 1975-09-23
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Granted: 1977-07-19
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Expires: 1995-09-23
Abstract
Abstract Beet juice is purified, then concentrated and treated in several steps for boiling and centrifugal separation to effect recovery of sucrose therefrom. The molasses remaining after the separation of sucrose from massecuite is treated with alpha -galactosidase to effect hydrolysis of raffinose present in the molasses. The resultant raffinose hydrolyzate is introduced into a calcium saccharate-forming step, wherein quicklime is continuously added to the hydrolyzate to form saccharate within the hydrolyzate. From the calcium saccharate-forming step, nearly the same volume of the saccharate-containing solution as that of the raffinose hydrolyzate fed therein is forwarded to a filtering and washing step. The resultant saccharate cake is sent back to the step for purification. From said calcium saccharate-forming step, the same saccharate-containing solution is also withdrawn in a volume of from three to ten times that of said raffinose hydrolyzate fed therein, is cooled and thereafter returned to the calcium saccharate-forming step. The saccharate-containing solution is circulated several times through this step so that discharge of waste molasses is eliminated and the sucrose contained in the beet juice is efficiently recovered substantially in its entire amount.
Inventors
- 👤 Shinichi Meguro
- 👤 Shinsaku Imafuku
- 👤 Kazuo Kawamura
- 👤 Shigeki Hashimoto
- 👤 Shigeyoshi Narita
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 12:37
CPC Classifications
C; C13; C13B; C13B35/00; C13B35/005; C13B20/00; C13B20/02; Y; Y02; Y02P; Y02P40/00; Y02P40/40
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
210 words
In a process for manufacturing beet sugar comprising purifying diffused beet juice, concentrating the purified beet juice, recovering sucrose from the concentrated beet juice in a boiling and centrifugal separation step, adding quicklime to the molasses remaining after the centrifugal separation of sucrose from the massecuite to produce calcium saccharate and returning the resultant saccharate cake to the diffused beet juice-purifying step, the improvement which comprises a. adding α-galactosidase to the molasses remaining after the centrifugal separation of sucrose thereby hydrolyzing the raffinose present in the molasses into sucrose and galactose before said quicklime addition; b. continuously adding quicklime to the resultant raffinose hydrolyzate to produce calcium saccharate; c. continuously withdrawing from the calcium saccharate-forming step substantially the same amount of the saccharate-containing solution as the amount of raffinose hydrolyzate being fed into the calcium saccharate-forming step and forwarding the saccharate cake obtained by filtering and washing said saccharate-containing solution to the diffused beet juice-purifying step; and d. at the same time, continuously withdrawing from the calcium saccharate-forming step a second volume of the saccharate-containing solution which is three to ten times the volume of the raffinose hydrolyzate being fed into the calcium saccharate-forming step, cooling said second withdrawn solution and returning the cooled solution to the calcium saccharate-forming step.
Claim 2
Dependent Claim
210 words
In a process for manufacturing beet sugar comprising purifying diffused beet juice, concentrating the purified beet juice, recovering sucrose from the concentrated beet juice in a boiling and centrifugal separation step, adding quicklime to the molasses remaining after the centrifugal separation of sucrose from the massecuite to produce calcium saccharate and returning the resultant saccharate cake to the diffused beet juice-purifying step, the improvement which comprises a. adding α-galactosidase to the molasses remaining after the centrifugal separation of sucrose thereby hydrolyzing the raffinose present in the molasses into sucrose and galactose before said quicklime addition; b. continuously adding quicklime to the resultant raffinose hydrolyzate to produce calcium saccharate; c. continuously withdrawing from the calcium saccharate-forming step substantially the same amount of the saccharate-containing solution as the amount of raffinose hydrolyzate being fed into the calcium saccharate-forming step and forwarding the saccharate cake obtained by filtering and washing said saccharate-containing solution to the diffused beet juice-purifying step; and d. at the same time, continuously withdrawing from the calcium saccharate-forming step a second volume of the saccharate-containing solution which is three to ten times the volume of the raffinose hydrolyzate being fed into the calcium saccharate-forming step, cooling said second withdrawn solution and returning the cooled solution to the calcium saccharate-forming step.
Claim 3
Dependent Claim
44 words
The process of claim 1, wherein the molasses remaining after the centrifugal separation of sucrose is diluted to 20° to 50° Brix and the α-galactosidase is added thereto under a pH of 4.5 - 7 and a reaction temperature of 20° - 55° C.
Claim 4
Dependent Claim
29 words
The process of claim 2, wherein the α-galactosidase is added to the molasses at a rate of 1,000,000 ˜ 16,000,000,000 units per g of raffinose contained in the molasses.
Claim 5
Dependent Claim
29 words
The process of claim 1, wherein the raffinose hydrolyzate is separated from the α-galactosidase contained therein and then is fed with the concentration unchanged, to the calcium saccharate-forming step.
Claim 6
Dependent Claim
38 words
The process of claim 4, wherein the molasses subjected to the treatment for raffinose hydrolysis has a polarization of 12 ˜ 20% and the resultant raffinose hydrolyzate is fed, with the concentration unchanged, to the calcium saccharate-forming step.
Claim 7
Dependent Claim
36 words
The process of claim 1, wherein said second saccharate-containing solution withdrawn from the calcium saccharate-forming step is cooled to a temperature such that the reaction solution in the calcium saccharate-forming step is maintained below 20° C.
References Cited (Backward Citations)
US3844835A
Cited
US3767526A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-07-18 | 1981-01-17 | 1981-07-19 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-07-18 | 1985-01-17 | 1985-07-19 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-07-18 | 1989-01-17 | 1989-07-19 | $7700.00 | Window Closed / Lapsed |