US4028135A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method of cleaning surfaces by irradiation with ultraviolet light
Assignee: United States Department of the Army
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Filing: 1976-04-22
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Granted: 1977-06-07
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Expires: 1996-04-22
Abstract
Abstract Contaminants are rapidly removed from surfaces by precleaning the surfaces in air, and then irradiating the surfaces with shortwave ultraviolet light in the presence of oxygen.
Inventors
- 👤 John R. Vig
- 👤 John W. LeBus
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-30 00:12
CPC Classifications
C; C23; C23G; C23G5/00; B; B08; B08B; B08B7/00; B08B7/0035; B08B7/0057; B08B7/04
Claims Analysis
Total Claims: 13
Claim 1
Independent Claim
107 words
Method of removing contaminants from surfaces including the steps of: A. precleaning the surfaces with solvents; then rinsing in running ultrapure water; and finally, spinning dry immediately after the running water rinse; said precleaning also being carried out under an atmosphere of air; B. placing the precleaned surfaces within about 5 millimeters of a lamp which emits short wavelength ultraviolet light that generates ozone in an oxygen containing atmosphere and that contains at least one wavelength between about 2000 angstroms and about 3000 angstroms; and irradiating the placed surfaces in an oxygen containing atmosphere with said short wavelength ultraviolet light from said lamp for about one minute.
Claim 2
Dependent Claim
107 words
Method of removing contaminants from surfaces including the steps of: A. precleaning the surfaces with solvents; then rinsing in running ultrapure water; and finally, spinning dry immediately after the running water rinse; said precleaning also being carried out under an atmosphere of air; B. placing the precleaned surfaces within about 5 millimeters of a lamp which emits short wavelength ultraviolet light that generates ozone in an oxygen containing atmosphere and that contains at least one wavelength between about 2000 angstroms and about 3000 angstroms; and irradiating the placed surfaces in an oxygen containing atmosphere with said short wavelength ultraviolet light from said lamp for about one minute.
Claim 3
Dependent Claim
34 words
Method according to claim 1 wherein the short wavelength ultraviolet light contains at least one wavelength shorter than about 2000 angstroms, and at least one wavelength between about 2000 angstroms and about 3000 angstroms.
Claim 4
Dependent Claim
21 words
Method according to claim 2 wherein the short wavelength ultraviolet light contains wavelengths of about 1849 angstroms and about 2537 angstroms.
Claim 5
Dependent Claim
20 words
Method according to claim 1 wherein the lamp is a low pressure mercury discharge lamp in a fused quartz envelope.
Claim 6
Dependent Claim
20 words
Method according to claim 1 wherein the surfaces to be cleaned and the lamp are enclosed in an aluminum box.
Claim 7
Dependent Claim
26 words
Method according to claim 1 wherein the short wavelength ultraviolet light used is about 2537 angstroms and wherein ozone is provided by a separate ozone generator.
Claim 8
Dependent Claim
98 words
Method according to claim 1 wherein the surface is a quartz resonator, wherein the contaminants removed are selected from the group consisting of human skin oils, a cutting oil used with a diamond saw, a beeswax and rosin mixture used to cement the crystals into a loaf during a rounding operation, a lapping vehicle, a mechanical vacuum pump oil, a silicone diffusion pump oil, an organic diffusion pump oil, a silicone vacuum grease, an acid flux, a rosin flux, and contamination absorbed during prolonged exposure to air, and wherein said contaminants are removed after 60 seconds of irradiation.
Claim 9
Dependent Claim
13 words
Method according to claim 1 wherein the surface to be cleaned is gold.
Claim 10
Dependent Claim
43 words
Method according to claim 5 wherein the surface to be cleaned is an oxide forming metal, and wherein the oxygen containing atmosphere is controlled to be free of impurities which can combine in the presence of ultraviolet radiation to produce a corrosive atmosphere.
Claim 11
Dependent Claim
19 words
Method according to claim 1 wherein the oxygen containing atmosphere is a mixture of pure oxygen and pure argon.
Claim 12
Dependent Claim
12 words
Method according to claim 1 wherein the oxygen containing atmosphere is air.
Claim 13
Dependent Claim
25 words
Method according to claim 5 wherein a second lamp is enclosed in said box which generates short wavelength ultraviolet light that does not generate ozone.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-06-06 | 1980-12-06 | 1981-06-07 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-06-06 | 1984-12-06 | 1985-06-07 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-06-06 | 1988-12-06 | 1989-06-07 | $7700.00 | Window Closed / Lapsed |