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US4026819A Expired / Lapsed US ⏱️ 0.0 years remaining

Production of hydrous pentavalent antimony oxide sol composition, dry powder prepared therefrom, and production of said dry powder

Assignee: COOKSON MINERALS Ltd UTTOXETER ROAD MEIR STOKE-ON-TRENT ST3 7XS UNITED KINGDOM A Co OF UNITED KINGDOM
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Filing: 1976-04-09
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Granted: 1977-05-31
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Expires: 1996-04-09
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Abstract

Abstract An aqueous antimony pentoxide sol composition, comprising from 10% to 50% antimony pentoxide and the remainder water has been prepared. This sol composition also may contain up to 5.0% of an amine if desired. When this sol composition contains the amine, a dried composition may be obtained from this sol composition. This dried powder contains from 85% to 95% antimony pentoxide and from 2.5% to 10% of an amine, the remainder being absorbed and combined water. This dried composition when added to water or an organic solvent readily forms the stabilized sol composition originally obtained.

Inventors

  • 👤 Ronald Francis Langere
  • 👤 Otto Ernest Loeffler
  • 👤 Thomas Francis Santini

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 11:02
CPC Classifications
C; C01; C01G; C01G30/00; C01G30/004; C01G30/005; B; B82; B82Y; B82Y30/00; C08; C08K; C08K3/00; C08K3/18; C08K3/20; C08K3/22; C08K3/2279; C08K9/00; C08K9/02; D; D06; D06M; D06M11/00; D06M11/32; D06M11/36; D06M11/47; C01P; C01P2004/00; C01P2004/60; C01P2004/64; C01P2006/00; C01P2006/22; C01P2006/80

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 98 words
A process for producing a stable aqueous antimony pentoxide sol comprising from 10% to 50% antimony pentoxide and the remainder water, said sol prepared by admixing antimony trioxide, hydrogen peroxide and water in amounts such that there are from 0.7 to 9.4 parts of water and from 0.65 to 0.68 parts of hydrogen peroxide for each part of antimony trioxide present in said mixture and refluxing the mixture for a period of 1 to 10 hours then cooling the mixture, thus forming the stable antimony pentoxide sol, all of the percentages and parts expressed on a weight basis.
Claim 2
Dependent Claim 98 words
A process for producing a stable aqueous antimony pentoxide sol comprising from 10% to 50% antimony pentoxide and the remainder water, said sol prepared by admixing antimony trioxide, hydrogen peroxide and water in amounts such that there are from 0.7 to 9.4 parts of water and from 0.65 to 0.68 parts of hydrogen peroxide for each part of antimony trioxide present in said mixture and refluxing the mixture for a period of 1 to 10 hours then cooling the mixture, thus forming the stable antimony pentoxide sol, all of the percentages and parts expressed on a weight basis.
Claim 3
Dependent Claim 140 words
Process for producing a stable aqueous antimony pentoxide sol comprising from 10% to 50% antimony pentoxide, an amine in amount up to 5.0% and the remainder water, said sol prepared by admixing antimony trioxide, hydrogen peroxide and water in amounts such that there are from 0.7 to 9.4 parts of water and from 0.65 to 0.68 parts of hydrogen peroxide for each part of antimony trioxide present in said mixture and refluxing the mixture for a period of 1 to 10 hours then cooling the mixture, and to the mixture adding an amine in amount up to 5.0%, all of the percentages and parts expressed on a weight basis, said amine being selected from the group consisting of secondary and tertiary aliphatic amines having from 1 to 5 carbon atoms and cyclicamines, said sol capable of remaining stable upon drying.
Claim 4
Dependent Claim 140 words
Process for producing a stable aqueous antimony pentoxide sol comprising from 10% to 50% antimony pentoxide, an amine in amount up to 5.0% and the remainder water, said sol prepared by admixing antimony trioxide, hydrogen peroxide and water in amounts such that there are from 0.7 to 9.4 parts of water and from 0.65 to 0.68 parts of hydrogen peroxide for each part of antimony trioxide present in said mixture and refluxing the mixture for a period of 1 to 10 hours then cooling the mixture, and to the mixture adding an amine in amount up to 5.0%, all of the percentages and parts expressed on a weight basis, said amine being selected from the group consisting of secondary and tertiary aliphatic amines having from 1 to 5 carbon atoms and cyclicamines, said sol capable of remaining stable upon drying.
Claim 5
Dependent Claim 134 words
A dry powder comprising from 85% to 95% antimony pentoxide, from 2.5% to 10% of an amine and the remainder water, said powder prepared by admixing antimony trioxide, hydrogen peroxide and water in amounts such that there are from 0.7 to 9.4 parts of water and from 0.65 to 0.68 parts of hydrogen peroxide for each part of antimony trioxide present in said mixture and refluxing the mixture for a period of 1 to 10 hours, then cooling the mixture and adding an amine to said mixture in amount up to 5.0%, all of the percentages and parts expressed on a weight basis, said amine being selected from the group consisting of secondary and tertiary aliphatic amines having from 1 to 5 carbon atoms and cyclicamines, and drying the mixture to form said powder.
Claim 6
Dependent Claim 134 words
A dry powder comprising from 85% to 95% antimony pentoxide, from 2.5% to 10% of an amine and the remainder water, said powder prepared by admixing antimony trioxide, hydrogen peroxide and water in amounts such that there are from 0.7 to 9.4 parts of water and from 0.65 to 0.68 parts of hydrogen peroxide for each part of antimony trioxide present in said mixture and refluxing the mixture for a period of 1 to 10 hours, then cooling the mixture and adding an amine to said mixture in amount up to 5.0%, all of the percentages and parts expressed on a weight basis, said amine being selected from the group consisting of secondary and tertiary aliphatic amines having from 1 to 5 carbon atoms and cyclicamines, and drying the mixture to form said powder.
Claim 7
Dependent Claim 136 words
Process for producing a dry powder comprising from 85% to 95% antimony pentoxide, from 2.5% to 10% of an amine and the remainder water which comprises admixing antimony trioxide, hydrogen peroxide and water in amounts such that there are from 0.7 to 9.4 parts of water and from 0.65 to 0.68 parts of hydrogen peroxide for each part of antimony trioxide present in said mixture and refluxing the mixture for a period of 1 to 10 hours, then cooling the mixture and adding an amine to said mixture in amount from 2.5% to 10.0%, all of the percentages and parts expressed on a weight basis, said amine being selected from the group consisting of secondary and tertiary aliphatic amines having from 1 to 5 carbon atoms and cyclicamines, and drying the mixture to form said powder.
Claim 8
Dependent Claim 136 words
Process for producing a dry powder comprising from 85% to 95% antimony pentoxide, from 2.5% to 10% of an amine and the remainder water which comprises admixing antimony trioxide, hydrogen peroxide and water in amounts such that there are from 0.7 to 9.4 parts of water and from 0.65 to 0.68 parts of hydrogen peroxide for each part of antimony trioxide present in said mixture and refluxing the mixture for a period of 1 to 10 hours, then cooling the mixture and adding an amine to said mixture in amount from 2.5% to 10.0%, all of the percentages and parts expressed on a weight basis, said amine being selected from the group consisting of secondary and tertiary aliphatic amines having from 1 to 5 carbon atoms and cyclicamines, and drying the mixture to form said powder.

References Cited (Backward Citations)

US3281216A Cited
US3676362A Cited
US3860523A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-05-30 1980-11-29 1981-05-31 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-05-30 1984-11-29 1985-05-31 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-05-30 1988-11-29 1989-05-31 $7700.00 Window Closed / Lapsed

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