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US4020199A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing acrylic fibers having animal hair-like hand

Assignee: Japan Exlan Co Ltd
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Filing: 1975-09-24
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Granted: 1977-04-26
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Expires: 1995-09-24
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Abstract

Abstract Process for imparting an animal hairlike hand to acrylic fibers by mixing a silicone resin and a polyoxyethylene alkylphenyl phosphate while adding water thereto to form an emulsion of weak acidity, applying the emulsion to swollen gelly acrylic fibers, drying the resultant fibers and applying a spinning oil to the dried fibers.

Inventors

  • 👤 Katsuaki Nomura
  • 👤 Masaaki Fujimatsu

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 12:34
CPC Classifications
D; D06; D06M; D06M15/00; D06M15/19; D06M15/37; D06M15/643; D06M13/00; D06M13/244; D06M13/282; D06M13/292; D06M15/6436; Y; Y10; Y10T; Y10T428/00; Y10T428/29; Y10T428/2913; Y10T428/2933; Y10T428/2962; Y10T428/2964; Y10T428/2967

Claims Analysis

Total Claims: 2
Claim 1
Independent Claim 201 words
A process for preparing acrylic fibers having an animal hairlike hand which comprises preparing an emulsion of pH 5.5 to 6.8 consisting essentially of (1) a silicone resin of the formula ##STR2## wherein R is R'NH 2 , R'NHR" or R'NR" 2 , R' is (CH 2 ) n , n is 1 to 3, R" is C m H 2m +1 , m is 1 to 3, x and y are positive integers and the molecular weight of the silicone resin is less than 100,000 and (2) an emulsifier selected from the group consisting of polyoxyethylene (n') monoalkylphenyl phosphates, wherein n' is the number of ethylene oxide groups and is a value of 5 to 15, and the alkyl group contains 8 to 12 carbon atoms, and (3) water, depositing said emulsion on undried wet-spun swollen gelly acrylic fibers containing 40 to 100% by weight of water based on the dry weight of the fibers, in an amount of 0.1 to 3.0% by weight of the silicone resin based on the dry weight of the fibers, immediately drying the resultant fibers to fix said silicone resin on the fiber surfaces and applying a spinning oil agent to the dried fibers.
Claim 2
Dependent Claim 201 words
A process for preparing acrylic fibers having an animal hairlike hand which comprises preparing an emulsion of pH 5.5 to 6.8 consisting essentially of (1) a silicone resin of the formula ##STR2## wherein R is R'NH 2 , R'NHR" or R'NR" 2 , R' is (CH 2 ) n , n is 1 to 3, R" is C m H 2m +1 , m is 1 to 3, x and y are positive integers and the molecular weight of the silicone resin is less than 100,000 and (2) an emulsifier selected from the group consisting of polyoxyethylene (n') monoalkylphenyl phosphates, wherein n' is the number of ethylene oxide groups and is a value of 5 to 15, and the alkyl group contains 8 to 12 carbon atoms, and (3) water, depositing said emulsion on undried wet-spun swollen gelly acrylic fibers containing 40 to 100% by weight of water based on the dry weight of the fibers, in an amount of 0.1 to 3.0% by weight of the silicone resin based on the dry weight of the fibers, immediately drying the resultant fibers to fix said silicone resin on the fiber surfaces and applying a spinning oil agent to the dried fibers.

References Cited (Backward Citations)

US3281260A Cited
US3366584A Cited
US3455771A Cited
US3488217A Cited
US3619278A Cited
US3655420A Cited
US3855776A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-04-25 1980-10-25 1981-04-26 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-04-25 1984-10-25 1985-04-26 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-04-25 1988-10-25 1989-04-26 $7700.00 Window Closed / Lapsed

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