Patent US385069A successfully refreshed from Google Patents.
US4020199A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for producing acrylic fibers having animal hair-like hand
Assignee: Japan Exlan Co Ltd
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Filing: 1975-09-24
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Granted: 1977-04-26
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Expires: 1995-09-24
Abstract
Abstract Process for imparting an animal hairlike hand to acrylic fibers by mixing a silicone resin and a polyoxyethylene alkylphenyl phosphate while adding water thereto to form an emulsion of weak acidity, applying the emulsion to swollen gelly acrylic fibers, drying the resultant fibers and applying a spinning oil to the dried fibers.
Inventors
- 👤 Katsuaki Nomura
- 👤 Masaaki Fujimatsu
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 12:21
CPC Classifications
D; D06; D06M; D06M15/00; D06M15/19; D06M15/37; D06M15/643; D06M13/00; D06M13/244; D06M13/282; D06M13/292; D06M15/6436; Y; Y10; Y10T; Y10T428/00; Y10T428/29; Y10T428/2913; Y10T428/2933; Y10T428/2962; Y10T428/2964; Y10T428/2967
Claims Analysis
Total Claims: 2
Claim 1
Independent Claim
201 words
A process for preparing acrylic fibers having an animal hairlike hand which comprises preparing an emulsion of pH 5.5 to 6.8 consisting essentially of (1) a silicone resin of the formula ##STR2## wherein R is R'NH 2 , R'NHR" or R'NR" 2 , R' is (CH 2 ) n , n is 1 to 3, R" is C m H 2m +1 , m is 1 to 3, x and y are positive integers and the molecular weight of the silicone resin is less than 100,000 and (2) an emulsifier selected from the group consisting of polyoxyethylene (n') monoalkylphenyl phosphates, wherein n' is the number of ethylene oxide groups and is a value of 5 to 15, and the alkyl group contains 8 to 12 carbon atoms, and (3) water, depositing said emulsion on undried wet-spun swollen gelly acrylic fibers containing 40 to 100% by weight of water based on the dry weight of the fibers, in an amount of 0.1 to 3.0% by weight of the silicone resin based on the dry weight of the fibers, immediately drying the resultant fibers to fix said silicone resin on the fiber surfaces and applying a spinning oil agent to the dried fibers.
Claim 2
Dependent Claim
201 words
A process for preparing acrylic fibers having an animal hairlike hand which comprises preparing an emulsion of pH 5.5 to 6.8 consisting essentially of (1) a silicone resin of the formula ##STR2## wherein R is R'NH 2 , R'NHR" or R'NR" 2 , R' is (CH 2 ) n , n is 1 to 3, R" is C m H 2m +1 , m is 1 to 3, x and y are positive integers and the molecular weight of the silicone resin is less than 100,000 and (2) an emulsifier selected from the group consisting of polyoxyethylene (n') monoalkylphenyl phosphates, wherein n' is the number of ethylene oxide groups and is a value of 5 to 15, and the alkyl group contains 8 to 12 carbon atoms, and (3) water, depositing said emulsion on undried wet-spun swollen gelly acrylic fibers containing 40 to 100% by weight of water based on the dry weight of the fibers, in an amount of 0.1 to 3.0% by weight of the silicone resin based on the dry weight of the fibers, immediately drying the resultant fibers to fix said silicone resin on the fiber surfaces and applying a spinning oil agent to the dried fibers.
References Cited (Backward Citations)
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-04-25 | 1980-10-25 | 1981-04-26 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-04-25 | 1984-10-25 | 1985-04-26 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-04-25 | 1988-10-25 | 1989-04-26 | $7700.00 | Window Closed / Lapsed |