Patent US4017290A successfully refreshed from Google Patents.
US4017290A
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Method and apparatus for making uniform pellets for fusion reactors
Assignee: KMS Fusion Inc
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Filing: 1974-04-15
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Granted: 1977-04-12
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Expires: 1994-04-15
Abstract
Abstract A method and apparatus for making uniform pellets for laser driven fusion reactors which comprises selection of a quantity of glass frit which has been accurately classified as to size within a few micrometers and contains an occluded material, such as urea, which gasifies and expands when heated. The sized particles are introduced into an apparatus which includes a heated vertical tube with temperatures ranging from 800° C to 1300° C. The particles are heated during the drop through the tube to molten condition wherein the occluded material gasifies to form hollow microspheres which stabilize in shape and plunge into a collecting liquid at the bottom of the tube. The apparatus includes the vertical heat resistant tube, heaters for the various zones of the tube and means for introducing the frit and collecting the formed microspheres.
Inventors
- 👤 Ronald G. Budrick
- 👤 Frank T. King
- 👤 Alfred J. Martin
- 👤 Robert L. Nolen, Jr.
- 👤 David E. Solomon
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-27 20:07
CPC Classifications
G; G21; G21B; G21B1/00; G21B1/11; G21B1/19; C; C03; C03B; C03B19/00; C03B19/10; C03B19/107; C03B19/1075; Y; Y02; Y02E; Y02E30/00; Y02E30/10
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
123 words
A method of forming sized microspheres which comprises: a. separating glass frit into a plurality of quantities of predetermined selected sizes in the range of 50 to 90 micrometers, b. heating a vertical drop tube from outside the tube to temperature ranges between 800° and 1300° C, c. closing the top of the tube with a closure and the bottom of said tube with a quantity of receiving liquid to prevent down or updraft, d. feeding a quantity of a selected size of frit into the top of said heated tube and recovering said frit as microspheres in said liquid, and e. repeating said feeding step with a different selected size in each instance to provide a plurality of microspheres of differing sizes.
Claim 2
Independent Claim
123 words
A method of forming sized microspheres which comprises: a. separating glass frit into a plurality of quantities of predetermined selected sizes in the range of 50 to 90 micrometers, b. heating a vertical drop tube from outside the tube to temperature ranges between 800° and 1300° C, c. closing the top of the tube with a closure and the bottom of said tube with a quantity of receiving liquid to prevent down or updraft, d. feeding a quantity of a selected size of frit into the top of said heated tube and recovering said frit as microspheres in said liquid, and e. repeating said feeding step with a different selected size in each instance to provide a plurality of microspheres of differing sizes.
Claim 3
Independent Claim
152 words
A method of forming sized microspheres which comprises: a. separating glass frit into a plurality of quantities of predetermined selected sizes in the range of 50 to 90 micrometers, b. heating a vertical drop tube from outside the tube into a series of three temperature ranges from top to bottom, including a first range of 900° to 100° C, a second range from 1100° to 1300° C, and a third range from 800 to 1000° C, c. closing the top of the tube with a closure and the bottom of said tube with a quantity of receiving liquid to prevent down or updraft, d. feeding a quantity of a selected size of frit into the top of said heated tube and recovering said frit as microspheres in said liquid, and e. repeating said feeding step with a different selected size in each instance to provide a plurality of microspheres of differing sizes.
Claim 4
Independent Claim
152 words
A method of forming sized microspheres which comprises: a. separating glass frit into a plurality of quantities of predetermined selected sizes in the range of 50 to 90 micrometers, b. heating a vertical drop tube from outside the tube into a series of three temperature ranges from top to bottom, including a first range of 900° to 100° C, a second range from 1100° to 1300° C, and a third range from 800 to 1000° C, c. closing the top of the tube with a closure and the bottom of said tube with a quantity of receiving liquid to prevent down or updraft, d. feeding a quantity of a selected size of frit into the top of said heated tube and recovering said frit as microspheres in said liquid, and e. repeating said feeding step with a different selected size in each instance to provide a plurality of microspheres of differing sizes.
Claim 5
Independent Claim
108 words
An apparatus for forming glass microspheres in relatively large quantities which comprises: a. a vertical refractory tube formed of aligned sections, b. means to support said tube in vertical position, c. means comprising electrical heating elements surrounding said tube to heat said tube from the outside to temperatures ranging from 800° to 1000° C, d. means to close said tube at the top end, e. means including a liquid body and retainer therefor for closing the bottom end of the tube, and f. means adjacent the top of the tube to feed a quantity of glass frit at a point where it will fall through the heated zone.
Claim 6
Independent Claim
108 words
An apparatus for forming glass microspheres in relatively large quantities which comprises: a. a vertical refractory tube formed of aligned sections, b. means to support said tube in vertical position, c. means comprising electrical heating elements surrounding said tube to heat said tube from the outside to temperatures ranging from 800° to 1000° C, d. means to close said tube at the top end, e. means including a liquid body and retainer therefor for closing the bottom end of the tube, and f. means adjacent the top of the tube to feed a quantity of glass frit at a point where it will fall through the heated zone.
Claim 7
Dependent Claim
78 words
An apparatus as defined in claim 3 in which said heating elements surrounding said tube are divided into three zone sections, and means to control the heating of said zones to provide a preheat section near the top with a temperature of 900° to 1100° C, an intermediate expansion section with a temperature in the range of 1100° to 1300° C, and a shape stabilizing section near the bottom heated to a range of 800° to 1000° C.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-04-11 | 1980-10-11 | 1981-04-12 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-04-11 | 1984-10-11 | 1985-04-12 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-04-11 | 1988-10-11 | 1989-04-12 | $7700.00 | Window Closed / Lapsed |